Drying device for medicament production
By setting up a heat exchanger and a cooling buffer box in the drying device for chemical production, the problems of excessive temperature difference and energy waste in the prior art are solved, the energy utilization rate and product performance are improved, and the temperature stability of the iron sulfate soaking tank is improved. .
Patent Information
- Application Number
- CN202422796115.8
- Authority / Receiving Office
- CN · China
- Patent Type
- Utility models(China)
- Current Assignee / Owner
- Filing Date
- 2024-11-18
- Publication Date
- 2024-12-13
- Estimated Expiration
- 2034-11-18
AI Technical Summary
During the drying process of lignin, the product performance is affected due to excessive temperature difference and energy waste. The high-temperature hot air of the quartz tube reactor is directly used in the drum drying box, which will destroy the microstructure of lignin.
After setting up a heat exchanger to cool down, the drum-type drying is performed using hot air, and the heated liquid phase is used to insulate the phosphoric acid soaking tank. At the same time, the high-temperature solid phase is cooled through the cooling buffer box and used to insulate the iron sulfate soaking tank.
It improves energy utilization and drying effect, improves product performance and temperature stability, and improves product quality.
Smart Images
Figure CN222165511U_ABST
Abstract
Description
Technical Field
[0001] The utility model relates to the technical field of defluorination agent production, in particular to a drying device for medicine production. Background Art
[0002] Modified lignin-based defluoridation agent is a new type of adsorbent obtained by chemically modifying lignin. Lignin is widely present in plants and is an aromatic polymer compound with abundant reserves in nature. Through modification, lignin can enhance its adsorption performance, especially in removing fluoride ions from water.
[0003] In actual production, lignin needs to be repeatedly soaked and dried, and reacted in a quartz tube reactor. In the processing process of existing equipment, the temperature of the quartz tube reactor is often 400-600℃, the temperature of the drum drying oven is 100-120℃, and the temperature of the washing tank and the iron sulfate soaking tank are both at room temperature. If the hot air from the quartz tube reactor is directly used in the drum drying oven, the microstructure of lignin will often be damaged due to excessive temperature, thus affecting product performance; and after the quartz tube reactor is processed, washing directly in the washing tank will also cause a large temperature difference, which will not only cause a decline in product performance, but also waste a lot of energy. Utility Model Content
[0004] In view of the above deficiencies in the prior art, the purpose of the utility model is to provide a drying device for pharmaceutical production. Through the setting of a heat exchanger, the hot air in the quartz tube reactor is cooled and used for drying in a drum drying box, and the liquid phase heated in the heat exchanger is used for heat preservation of a phosphoric acid soaking tank, which greatly improves the energy utilization and drying effect, thereby improving product performance; through the setting of a cooling buffer box, while cooling and buffering the high-temperature solid phase, the exchanged heat is used for heat preservation of the ferric sulfate soaking tank, which greatly improves the temperature stability in the ferric sulfate soaking tank and improves product quality.
[0005] The utility model is realized by adopting the following technical solutions:
[0006] The drying device for pharmaceutical production comprises a phosphoric acid soaking tank, which is connected to a quartz tube reactor through a drum drying box, the quartz tube reactor is connected to a washing tank through a cooling buffer box, the washing tank is connected to a ferric sulfate soaking tank through a stirring drying box, the ferric sulfate soaking tank is connected to a high-temperature drying box through a secondary water filter box, and a heat exchanger is connected to the quartz tube reactor.
[0007] The pipes used in the drying device for pharmaceutical production are all equipped with insulation layers, cooling liquid is installed in the heat exchanger, and a vibrator is installed on the wall of the secondary water filter box.
[0008] A primary water filter box is arranged between the phosphoric acid soaking tank and the drum drying box, and a conveyor belt is arranged between the primary water filter box and the drum drying box. A vibrator is arranged on the vertical wall of the primary water filter box, and the conveyor belt is a conveyor belt with a water filtering function.
[0009] The outer side of the phosphoric acid soaking tank is provided with a phosphoric acid soaking tank insulation jacket, and the heat exchanger is connected with the phosphoric acid soaking tank insulation jacket through a phosphoric acid soaking tank insulation jacket inlet pipe.
[0010] The washing tank is provided with a stirrer inside, a spray plate is provided above the stirrer, and a flushing water pipeline is connected to the spray plate. The washing tank is firstly flushed with hydrochloric acid and then with deionized water.
[0011] The cooling buffer box is provided with a cooling buffer box coil inside, and the outer side of the ferric sulfate soaking tank is provided with a ferric sulfate soaking tank insulation sleeve. The cooling buffer box coil is connected to the ferric sulfate soaking tank insulation sleeve through the ferric sulfate soaking tank insulation sleeve pipeline.
[0012] The high-temperature drying box is connected to the stirring drying box through a gas phase outlet high-temperature drying box pipeline; the heat exchanger is connected to the drum drying box through a gas phase inlet drum drying box pipeline.
[0013] The working principle of the utility model is:
[0014] After the crushing, the lignin enters the phosphoric acid soaking tank for soaking. After the soaking, it passes through the primary water filter box and the conveyor belt, enters the drum drying box, and is dried at 100-120°C. Then it enters the quartz tube reactor through the elevator and reacts at 400-600°C. After that, the gas phase enters the heat exchanger for cooling, and then enters the drum drying box. The heated liquid phase in the heat exchanger enters the phosphoric acid soaking tank insulation jacket through the phosphoric acid soaking tank insulation jacket pipe; the solid phase in the quartz tube reactor enters the cooling buffer box, and after cooling, it enters the stirring drying box after being treated in the washing tank, and then enters the high-temperature drying box for drying after passing through the iron sulfate soaking tank; the hot air of the high-temperature drying box enters the stirring drying box through the gas phase high-temperature drying box pipe for drying, and the liquid phase in the cooling buffer box coil enters the iron sulfate soaking tank insulation jacket through the iron sulfate soaking tank insulation jacket pipe to keep the iron sulfate soaking tank warm. Among them, the temperature of the high-temperature drying box is 100-120°C. The pipes used in the drying device for pharmaceutical production are all equipped with insulation layers, cooling liquid is installed in the heat exchanger, and a vibrator is installed on the wall of the secondary water filter box.
[0015] Compared with the prior art, the beneficial effects of the utility model are:
[0016] By adopting the drying device for pharmaceutical production of the utility model, the hot air in the quartz tube reactor is cooled by the setting of the heat exchanger and then used for drying in the drum drying box, and the liquid phase heated in the heat exchanger is used for heat preservation of the phosphoric acid soaking tank, which greatly improves the energy utilization rate and the drying effect, and thus improves the product performance; by setting the cooling buffer box, while the high-temperature solid phase is cooled and buffered, the exchanged heat is used for heat preservation of the ferric sulfate soaking tank, which greatly improves the temperature stability in the ferric sulfate soaking tank and improves the product quality. BRIEF DESCRIPTION OF THE DRAWINGS
[0017] Figure 1 This is a schematic diagram of the structure of the drying device for pharmaceutical production of the utility model;
[0018] In the figure: 1. phosphoric acid soaking tank; 2. primary water filter tank; 3. conveyor belt; 4. drum drying box; 5. quartz tube reactor; 6. cooling buffer tank; 7. washing tank; 8. stirring drying box; 9. ferric sulfate soaking tank; 10. secondary water filter tank; 11. high-temperature drying box; 12. phosphoric acid soaking tank insulation jacket; 13. heat exchanger; 14. cooling buffer tank coil; 15. spray plate; 16. ferric sulfate soaking tank insulation jacket; 17. pipe entering phosphoric acid soaking tank insulation jacket; 18. pipe entering ferric sulfate soaking tank insulation jacket; 19. gas phase exit high-temperature drying box pipe; 20. flushing water pipe; 21. gas phase enter drum drying box pipe. DETAILED DESCRIPTION
[0019] In order to make the purpose and technical solution of the utility model more clear, the utility model is further described in detail below in conjunction with the accompanying drawings.
[0020] Example 1
[0021] like Figure 1As shown, the drying device for pharmaceutical production includes a phosphoric acid soaking tank 1, which is connected to a quartz tube reactor 5 through a drum drying box 4, and the quartz tube reactor 5 is connected to a washing tank 7 through a cooling buffer box 6. The washing tank 7 is connected to a ferrous sulfate soaking tank 9 through a stirring drying box 8, and the ferrous sulfate soaking tank 9 is connected to a high-temperature drying box 11 through a secondary water filter box 10. A heat exchanger 13 is connected to the quartz tube reactor 5. The pipes used in the drying device for pharmaceutical production are all provided with a heat insulation layer, a cooling liquid is provided in the heat exchanger 13, and a vibrator is provided on the vertical wall of the secondary water filter box 10. A primary water filter box 2 is provided between the phosphoric acid soaking tank 1 and the drum drying box 4, and a conveyor belt 3 is provided between the primary water filter box 2 and the drum drying box 4. A phosphoric acid soaking tank insulation jacket 12 is provided on the outside of the phosphoric acid soaking tank 1, and the heat exchanger 13 is connected to the phosphoric acid soaking tank insulation jacket 12 through a phosphoric acid soaking tank insulation jacket inlet pipe 17. The washing tank 7 is provided with an agitator inside, and a spray plate 15 is provided above the agitator, and a flushing water pipe 20 is connected to the spray plate 15. The cooling buffer box 6 is provided with a cooling buffer box coil 14 inside, and the outer side of the iron sulfate soaking tank 9 is provided with an iron sulfate soaking tank insulation jacket 16, and the cooling buffer box coil 14 is connected to the iron sulfate soaking tank insulation jacket 16 through the iron sulfate soaking tank insulation jacket inlet pipe 18. The high-temperature drying box 11 is connected to the stirring drying box 8 through the gas phase high-temperature drying box outlet pipe 19; the heat exchanger 13 is connected to the drum drying box 4 through the gas phase drum drying box inlet pipe 21.
[0022] The above-mentioned drying device for pharmaceutical production, when in operation, comprises the following steps:
[0023] (1) After the pulverization, the lignin enters the phosphoric acid soaking tank 1 for soaking. After the soaking, it passes through the primary water filter box 2 and the conveyor belt 3, and then enters the drum drying box 4 for drying at 100-120°C. Then, it enters the quartz tube reactor 5 through the elevator and reacts at 400-600°C. After that, the gas phase enters the heat exchanger 13 for cooling, and then enters the drum drying box 4. The liquid phase heated in the heat exchanger 13 enters the phosphoric acid soaking tank insulation jacket 12 through the phosphoric acid soaking tank insulation jacket pipe 17; (2) The solid phase in the quartz tube reactor 5 enters the cooling buffer box 6, and after cooling, it is processed in the washing tank 7 and then enters the stirring and drying box 8. Then, it passes through the iron sulfate soaking tank 9 and enters the high-temperature drying box 11 for drying. (3) The hot air from the high-temperature drying box 11 enters the stirring and drying box 8 through the gas phase high-temperature drying box pipe 19 for drying, and the liquid phase in the cooling buffer box coil 14 enters the iron sulfate soaking tank insulation jacket 16 through the iron sulfate soaking tank insulation jacket pipe 18 to keep the iron sulfate soaking tank 9 warm.
Claims
1. A drying device for pharmaceutical production, characterized in that: The invention comprises a phosphoric acid soaking tank (1), wherein the phosphoric acid soaking tank (1) is connected to a quartz tube reactor (5) via a drum-type drying box (4), the quartz tube reactor (5) is connected to a washing tank (7) via a cooling buffer box (6), the washing tank (7) is connected to a ferric sulfate soaking tank (9) via a stirring drying box (8), the ferric sulfate soaking tank (9) is connected to a high-temperature drying box (11) via a secondary water filter box (10), and a heat exchanger (13) is connected to the quartz tube reactor (5).
2. The drying device for pharmaceutical production according to claim 1, characterized in that: A primary water filter box (2) is provided between the phosphoric acid soaking tank (1) and the drum-type drying box (4), and a conveyor belt (3) is provided between the primary water filter box (2) and the drum-type drying box (4).
3. The drying device for pharmaceutical production according to claim 1, characterized in that: The phosphoric acid soaking tank (1) is provided with a phosphoric acid soaking tank insulation jacket (12) on the outside, and the heat exchanger (13) is connected to the phosphoric acid soaking tank insulation jacket (12) via a phosphoric acid soaking tank insulation jacket inlet pipe (17).
4. The drying device for pharmaceutical production according to claim 1, characterized in that: The washing tank (7) is provided with an agitator inside, and a spray plate (15) is provided above the agitator, and a flushing water pipeline (20) is connected to the spray plate (15).
5. The drying device for pharmaceutical production according to claim 1, characterized in that: The cooling buffer box (6) is provided with a cooling buffer box coil (14) inside, the outer side of the ferric sulfate soaking tank (9) is provided with a ferric sulfate soaking tank insulation jacket (16), and the cooling buffer box coil (14) is connected to the ferric sulfate soaking tank insulation jacket (16) through a ferric sulfate soaking tank insulation jacket inlet pipe (18).
6. The drying device for pharmaceutical production according to claim 1, characterized in that: The high-temperature drying oven (11) is connected to the stirring drying oven (8) via a gas phase high-temperature drying oven outlet pipe (19); the heat exchanger (13) is connected to the drum drying oven (4) via a gas phase drum drying oven inlet pipe (21).