Preparation device of 1-ethynyl-1-cyclohexanol
By introducing agitating and filtration components into the 1-ethynyl-1-cyclohexanol preparation device, the problems of resource waste and pollution after solid-liquid separation are solved, and the recycling and utilization of resources are realized, and environmental pollution is reduced.
Patent Information
- Application Number
- CN202420970281.2
- Authority / Receiving Office
- CN · China
- Patent Type
- Utility models(China)
- Current Assignee / Owner
- Filing Date
- 2024-05-07
- Publication Date
- 2025-01-03
- Estimated Expiration
- 2034-05-07
AI Technical Summary
The existing 1-ethynyl-1-cyclohexanol preparation device usually directly discharges liquid after solid-liquid separation, resulting in waste of resources and environmental pollution.
A preparation device including a stirring assembly and a filter assembly is designed. The stirring rod and pulley are driven by the stirring assembly, and the threaded sleeve and scraper are combined to achieve solid recovery and further refining of liquid. The filter assembly is used for solid-liquid separation and collecting products. .
It effectively reduces resource waste and environmental pollution. Through the coordination of stirring and filtration components, resource recycling and utilization after solid-liquid separation is achieved.
Smart Images
Figure CN222286514U_ABST
Abstract
Description
Technical Field
[0001] The utility model belongs to the technical field of chemical engineering, and particularly relates to a preparation device for 1-ethynyl-1-cyclohexanol. Background Art
[0002] The preparation device of 1-ethynyl-1-cyclohexanol refers to a set of equipment and systems for synthesizing the organic compound, which includes components such as a reactor, a reaction control system, a separation device, and a storage and collection device. First, the reactor is the main place where the chemical reaction occurs, where appropriate raw materials are introduced for reaction. Secondly, the reaction control system is responsible for monitoring and adjusting the reaction conditions, such as temperature, pressure and the addition rate of reactants, to ensure that the formation of the target product is favorable. Thirdly, the separation device is used to separate the target product from the reaction mixture, usually by distillation, extraction or crystallization. Finally, the storage and collection device is used to store or collect the prepared 1-ethynyl-1-cyclohexanol for subsequent use or further processing. In summary, the preparation device of 1-ethynyl-1-cyclohexanol is a complete chemical synthesis system, covering key steps such as reaction, control, separation and storage, ensuring the efficient and safe preparation of the compound.
[0003] In the prior art, the preparation device of 1-ethynyl-1-cyclohexanol usually directly discharges the liquid after solid-liquid separation, but recyclable solvents and reactants will remain in the liquid, resulting in unnecessary waste of resources and pollution to the surrounding environment. To this end, we provide a preparation device of 1-ethynyl-1-cyclohexanol to solve the above problems. Utility Model Content
[0004] The utility model aims to provide a preparation device for 1-ethynyl-1-cyclohexanol. By coordinating a stirring component and a filtering component, the utility model solves the problem that the preparation device for 1-ethynyl-1-cyclohexanol in the prior art usually directly discharges the liquid after the solid-liquid separation, resulting in waste of resources and environmental pollution.
[0005] In order to solve the above technical problems, the utility model is realized by the following technical solutions:
[0006] The utility model discloses a preparation device for 1-ethynyl-1-cyclohexanol, comprising a filter box, a stirring box is fixedly connected to the bottom of the filter box, and a controller is fixedly connected to the front of the filter box;
[0007] A stirring assembly is arranged inside the stirring box, and the stirring assembly includes a support frame, the support frame is fixed to one side of the stirring box, a motor is fixedly connected to one side of the support frame, a stirring rod is fixedly connected to the output end of the motor, a stirring blade is fixedly connected to the surface of the stirring rod, and a transmission member is arranged on one side of the surface of the stirring rod;
[0008] The filter box is provided with a filter assembly inside, through which solid and liquid can be separated.
[0009] The utility model is further configured such that the filter assembly comprises a support rod, a filter plate is fixedly connected to the top of the support rod, and collection boxes are fixedly connected to both sides of the bottom of the inner cavity of the filter box.
[0010] The utility model is further configured such that the transmission member includes a first pulley, the first pulley is fixed to one side of the surface of the stirring rod, a reciprocating screw is movably connected to the rear side of the inner cavity of the filter box, a second pulley is fixedly connected to one side of the surface of the reciprocating screw, and the second pulley is connected to the first pulley through a belt.
[0011] The utility model is further configured that a threaded sleeve is threadedly connected to the surface of the reciprocating screw, a connecting rod is fixedly connected to the bottom of the threaded sleeve, and a scraper is fixedly connected to the bottom of the front side of the connecting rod.
[0012] The utility model is further configured that both sides of the bottom of the front side of the filter box are movably connected with box doors through hinges, and one side of the front side of the box door is fixedly connected with a handle.
[0013] The utility model is further configured that the bottom of the connecting rod is slidably connected to a guide plate, and the bottom of the guide plate is fixedly connected to the rear side of the top of the filter plate.
[0014] The utility model is further configured such that the top of the filter box is connected to a feed port, the bottom of the mixing box is connected to a discharge port, and a solenoid valve is arranged on the surface of the discharge port.
[0015] The utility model is further configured that heating plates are fixedly connected to both sides of the inner wall of the mixing box, and the number is four.
[0016] The utility model has the following beneficial effects:
[0017] 1. The utility model can drive the stirring rod and the first pulley to rotate through the rotation of the motor, and then the stirring rod drives the second pulley and the stirring blade to rotate, and then the reciprocating screw can be rotated through the drive of the second pulley, and then the movement of the threaded cylinder and the scraper can be combined to collect the fixed liquid into the collection box and recover the usable substances in the liquid.
[0018] 2. The utility model can further refine the filtered liquid through the setting of the stirring component, reduce the waste of resources and environmental pollution, and through the setting of the filtering component, the solid-liquid separation and collection of the reaction product can be carried out.
[0019] Of course, any product implementing the present invention does not necessarily need to achieve all of the advantages described above at the same time. BRIEF DESCRIPTION OF THE DRAWINGS
[0020] In order to more clearly illustrate the technical solutions of the embodiments of the utility model, the drawings required for describing the embodiments are briefly introduced below. Obviously, the drawings described below are only some embodiments of the utility model. For ordinary technicians in this field, other drawings can be obtained based on these drawings without creative work.
[0021] Figure 1 It is a structural stereogram of a device for preparing 1-ethynyl-1-cyclohexanol.
[0022] Figure 2 It is a left-side structural stereogram of a device for preparing 1-ethynyl-1-cyclohexanol.
[0023] Figure 3 for Figure 2 A is an enlarged view of the middle image.
[0024] Figure 4 The present invention is a schematic diagram of the internal structure of a filter box in a device for preparing 1-ethynyl-1-cyclohexanol.
[0025] Figure 5 The present invention is a schematic diagram of the internal structure of a stirring box in a device for preparing 1-ethynyl-1-cyclohexanol.
[0026] In the accompanying drawings, the components represented by the reference numerals are listed as follows:
[0027] 1. Filter box; 2. Mixing box; 3. Controller; 4. Support frame; 5. Motor; 6. Mixing rod; 7. Mixing blade; 8. Support rod; 9. Filter plate; 10. Collecting box; 11. First pulley; 12. Reciprocating screw; 13. Second pulley; 14. Threaded sleeve; 15. Connecting rod; 16. Scraper; 17. Box door; 18. Feed inlet; 19. Discharge outlet; 20. Solenoid valve; 21. Heating plate. DETAILED DESCRIPTION
[0028] The following will be combined with the drawings in the embodiments of the utility model to clearly and completely describe the technical solutions in the embodiments of the utility model. Obviously, the described embodiments are only part of the embodiments of the utility model, not all of the embodiments. Based on the embodiments of the utility model, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the utility model. Specific embodiment 1
[0030] See also Figure 1-5 The utility model is a preparation device for 1-ethynyl-1-cyclohexanol, comprising a filter box 1, a stirring box 2 is fixedly connected to the bottom of the filter box 1, and a controller 3 is fixedly connected to the front of the filter box 1;
[0031] A stirring assembly is arranged inside the stirring box 2, and the stirring assembly includes a support frame 4, the support frame 4 is fixed to one side of the stirring box 2, a motor 5 is fixedly connected to one side of the support frame 4, a stirring rod 6 is fixedly connected to the output end of the motor 5, a stirring blade 7 is fixedly connected to the surface of the stirring rod 6, and a transmission member is arranged on one side of the surface of the stirring rod 6;
[0032] A filter assembly is arranged inside the filter box 1, and solids and liquids can be separated by the filter assembly.
[0033] Specifically; the controller 3 is fixed at the center of the front of the filter box 1, the right side of the filter box is connected to a liquid filling port, the support frame 4 is fixed at the center of the left side of the mixing box 2, the motor 5 is fixed on the left side of the support frame 4, the stirring rod 6 is movably connected to the inside of the mixing box 2 through a bearing, and the left side is movably connected to the left side of the mixing box 2 through a bearing extension and extends to the outside of the mixing box 2, the stirring blade 7 is fixed on the right side of the surface of the stirring rod 6, and through the setting of the filtering component, solids and liquids can be separated, thereby increasing practicality during use. Specific embodiment 2
[0035] See also Figure 1-5 On the basis of the specific embodiment 1, the filter assembly includes a support rod 8, a filter plate 9 is fixedly connected to the top of the support rod 8, a collection box 10 is fixedly connected to both sides of the bottom of the inner cavity of the filter box 1, and the transmission member includes a first pulley 11, the first pulley 11 is fixed to one side of the surface of the stirring rod 6, a reciprocating screw 12 is movably connected to the rear side of the inner cavity of the filter box 1, a second pulley 13 is fixedly connected to one side of the surface of the reciprocating screw 12, the second pulley 13 is connected to the first pulley 11 through a belt, a threaded sleeve 14 is threadedly connected to the surface of the reciprocating screw 12, a connecting rod 15 is fixedly connected to the bottom of the threaded sleeve 14, and a scraper 16 is fixedly connected to the bottom of the front side of the connecting rod 15.
[0036] Specifically; the support rod 8 is fixed on both sides of the bottom of the inner cavity of the filter box 1, the filter plate 9 is fixed on the top of the support rod 8, there are two collecting boxes 10, which are symmetrically fixed on both sides of the bottom of the inner cavity of the filter box 1, the first pulley 11 is fixed on the left side of the surface of the stirring rod 6, and the reciprocating screw 12 is movably connected to the rear side of the inner cavity of the filter box 1 through a bearing. Two opposite threads are opened on the surface of the reciprocating screw 12, which can make the threaded sleeve 14 move back and forth. Specific embodiment three
[0038] See also Figure 1-5 On the basis of the specific embodiment 1 and the specific embodiment 2, both sides of the bottom of the front of the filter box 1 are movably connected with a box door 17 through hinges, a handle is fixedly connected to one side of the front of the box door 17, the bottom of the connecting rod 15 is slidably connected with a guide plate, and the bottom of the guide plate is fixedly connected to the rear side of the top of the filter plate 9. The top of the filter box 1 is connected to the feed port 18, and the bottom of the mixing box 2 is connected to the discharge port 19. The surface of the discharge port 19 is provided with a solenoid valve 20, and both sides of the inner wall of the mixing box 2 are fixedly connected with heating plates 21, and the number is four.
[0039] Specifically, there are two box doors 17, both of which are movably connected to the two sides of the bottom front of the filter box 1 through hinges, there are two handles, both of which are symmetrically fixed at the center of the right side of the front of the box door 17, and the guide plate is fixed to the top rear side of the filter plate 9. Through the setting of the guide plate, the connecting rod 15 can be limited to prevent displacement during movement. The feed port 18 is connected to the top center of the filter box 1, the solenoid valve 20 can control the switch of the discharge port 19, and there are four heating plates 21, which are symmetrically fixed at the bottom of both sides of the inner wall of the mixing box 2.
[0040] The working principle of the utility model is as follows: when it is necessary to separate the reactant and the liquid and extract the recyclable substance in the liquid, the user first adds the reactant into the filter box 1 through the feed port 18, and then after filtering through the filter plate 9, the solid will be filtered on the surface of the filter plate 9, and then the user starts the motor 5 through the controller 3, the motor 5 drives the stirring rod 6 and the first pulley 11 to rotate, the first pulley 11 drives the second pulley 13 to rotate, the second pulley 13 drives the reciprocating screw 12 to rotate, the reciprocating screw 12 drives the threaded sleeve 14 to move, the threaded sleeve 14 drives the connecting rod 15 to move, the connecting rod 15 drives the scraper 16 to move, the scraper 16 recovers the solid on the surface of the filter plate 9 to the inside of the collection box 10, and at the same time, the user adds the solvent into the stirring box 2 through the liquid adding port, and then the stirring rod 6 drives the stirring blade 7 to rotate, so that it is fully mixed and convenient for subsequent extraction work, so as to achieve the purpose of automatically collecting the fixed after solid-liquid separation and further recycling the liquid.
[0041] In the description of this specification, the description with reference to the terms "one embodiment", "example", "specific example", etc. means that the specific features, structures, materials or characteristics described in conjunction with the embodiment or example are included in at least one embodiment or example of the utility model. In this specification, the schematic representation of the above terms does not necessarily refer to the same embodiment or example. Moreover, the specific features, structures, materials or characteristics described can be combined in any one or more embodiments or examples in a suitable manner.
[0042] The preferred embodiments of the utility model disclosed above are only used to help explain the utility model. The preferred embodiments do not describe all the details in detail, nor do they limit the utility model to the specific implementation methods described. Obviously, many modifications and changes can be made according to the content of this specification. This specification selects and specifically describes these embodiments in order to better explain the principles and practical applications of the utility model, so that technicians in the relevant technical field can well understand and use the utility model. The utility model is limited only by the claims and their full scope and equivalents.
Claims
1. A device for preparing 1-ethynyl-1-cyclohexanol, comprising a filter box (1), characterized in that: The bottom of the filter box (1) is fixedly connected to a stirring box (2), and the front of the filter box (1) is fixedly connected to a controller (3); A stirring assembly is arranged inside the stirring box (2), and the stirring assembly comprises a support frame (4), the support frame (4) is fixed to one side of the stirring box (2), a motor (5) is fixedly connected to one side of the support frame (4), a stirring rod (6) is fixedly connected to the output end of the motor (5), a stirring blade (7) is fixedly connected to the surface of the stirring rod (6), and a transmission member is arranged on one side of the surface of the stirring rod (6); The filter box (1) is provided with a filter assembly inside, and solids and liquids can be separated by the filter assembly.
2. The device for preparing 1-ethynyl-1-cyclohexanol according to claim 1, characterized in that: The filter assembly comprises a support rod (8), a filter plate (9) is fixedly connected to the top of the support rod (8), and collection boxes (10) are fixedly connected to both sides of the bottom of the inner cavity of the filter box (1).
3. The device for preparing 1-ethynyl-1-cyclohexanol according to claim 1, characterized in that: The transmission member comprises a first pulley (11), the first pulley (11) is fixed to one side of the surface of the stirring rod (6), a reciprocating screw (12) is movably connected to the rear side of the inner cavity of the filter box (1), a second pulley (13) is fixedly connected to one side of the surface of the reciprocating screw (12), and the second pulley (13) is connected to the first pulley (11) through a belt.
4. The device for preparing 1-ethynyl-1-cyclohexanol according to claim 3, characterized in that: The surface of the reciprocating screw (12) is threadedly connected with a threaded sleeve (14), the bottom of the threaded sleeve (14) is fixedly connected with a connecting rod (15), and the bottom of the front side of the connecting rod (15) is fixedly connected with a scraper (16).
5. The device for preparing 1-ethynyl-1-cyclohexanol according to claim 1, characterized in that: Both sides of the bottom of the front side of the filter box (1) are movably connected to a box door (17) via hinges, and a handle is fixedly connected to one side of the front side of the box door (17).
6. The device for preparing 1-ethynyl-1-cyclohexanol according to claim 4, characterized in that: The bottom of the connecting rod (15) is slidably connected to a guide plate, and the bottom of the guide plate is fixedly connected to the rear side of the top of the filter plate (9).
7. The device for preparing 1-ethynyl-1-cyclohexanol according to claim 1, characterized in that: The top of the filter box (1) is connected to a feed port (18), and the bottom of the mixing box (2) is connected to a discharge port (19), and a solenoid valve (20) is provided on the surface of the discharge port (19).
8. The device for preparing 1-ethynyl-1-cyclohexanol according to claim 1, characterized in that: The two sides of the inner wall of the mixing box (2) are fixedly connected with heating plates (21), and the number is four.