High-efficiency tannin germanium deposition reaction barrel

Abstract

The utility model discloses a tannin high-efficiency germanium deposition reaction barrel, and relates to the technical field of reaction barrels. Comprising a barrel body, a feeding valve is fixedly installed at the position, close to the left side, of the upper side wall of the barrel body, a stirring mechanism is fixedly installed in the middle of the upper side wall of the barrel body, and a discharging pipe is fixedly installed on the inner wall of the lower side of the barrel body on the lower side of the stirring mechanism; a conical hopper is fixedly installed between the position, close to the upper side, of the outer surface of the discharging pipe and the inner wall of the barrel body, an air distribution cavity is formed between the conical hopper and the inner wall of the lower side of the barrel body and communicates with a heating mechanism, the heating mechanism communicates with the upper side in the barrel body and is fixedly installed on the right side face of the barrel body, and a control mechanism is arranged on the right side face of the barrel body. According to the reaction kettle, materials are turned over while being stirred, so that the materials are uniformly dispersed, the reaction is more sufficient, the processing efficiency is greatly improved, meanwhile, the internal materials are conveniently and quickly heated, the heating is more uniform, the reaction is more sufficient and comprehensive, and the use is facilitated.

Description

Technical Field

[0001] The utility model relates to the technical field of reaction barrels, in particular to a tannin high-efficiency germanium precipitation reaction barrel. Background Art

[0002] When tannic acid contacts the positively charged hydrated germanium dioxide, electrical neutralization occurs and precipitation occurs; hydrated germanium dioxide chelates with the gallic acid in the tannic acid, clamping the germanium in the gallic acid to form an insoluble tannin germanium precipitate; the germanium precipitation is based on the reaction between germanium and the hydroxyl group in the tannin to form a tannin complex and precipitate. In all these germanium precipitation processes, a reaction tank is required to react.

[0003] In the prior art, conventional tannin germanium precipitation reaction barrels, during use, usually use a simple stirring mechanism to stir the raw materials in the reaction barrel, which requires a lot of time for stirring, and the upper and lower layers are layered, the dispersion effect is poor, resulting in insufficient reaction, which is not conducive to use. In addition, during use, a water jacket is often used for heating, which takes a long time to heat, and the barrel body is prone to stability, which is not conducive to use. Utility Model Content

[0004] The utility model provides a tannin high-efficiency germanium precipitation reaction barrel to solve the problems in the background technology.

[0005] To achieve the above-mentioned purpose, the utility model provides the following technical solutions: a tannin high-efficiency germanium precipitation reaction barrel, comprising a barrel body, a feeding valve is fixedly installed on the upper side wall of the barrel body near the left position, a flipping mechanism is fixedly installed on the middle position of the upper side wall of the barrel body, a discharge pipe is fixedly installed on the lower inner wall of the barrel body below the flipping mechanism, and a gate valve is arranged on the discharge pipe, a conical bucket is fixedly installed between the outer surface of the discharge pipe near the upper side and the inner wall of the barrel body, and an air distribution cavity is arranged between the conical bucket and the lower inner wall of the barrel body The air distribution cavity is connected with the heating mechanism, the heating mechanism is connected with the upper side of the barrel body, the heating mechanism is fixedly installed on the right side of the barrel body, the right side of the barrel body is provided with a control mechanism, mechanical seals are evenly fixedly installed on the four sides of the conical bucket, and transmission pipes are fixedly installed in the mechanical seals, the transmission pipe is connected with the flipping mechanism through the transmission mechanism, the lower surface of the transmission pipe is an open structure, and the lower surface of the transmission pipe is inserted in the air distribution cavity, and a stirring mechanism is provided on the transmission pipe near the upper side.

[0006] Furthermore, the flipping mechanism includes a conveying cylinder, an electric screw feeding rod, a rectangular opening and a driven screw feeding rod. The conveying cylinder is fixedly installed on the upper side wall of the barrel body, and the lower surface of the conveying cylinder is an opening structure. The electric screw feeding rod is fixedly installed on the upper side wall of the conveying cylinder. The left and right side walls of the conveying cylinder are both provided with rectangular openings near the upper side. The driven screw feeding rod is installed on the lower surface of the electric screw feeding rod, and the driven screw feeding rod is inserted in the discharge pipe.

[0007] Furthermore, the heating mechanism includes an electric heating box, a conduit, an exhaust assembly and a waterproof breathable valve. The electric heating box is fixedly installed on the right side of the barrel body. The air outlet of the electric heating box is connected to the air distribution cavity through the conduit. The electric heating box is connected to the waterproof breathable valve through the exhaust assembly. The waterproof breathable valve is embedded in the upper side wall of the barrel body.

[0008] Furthermore, the control mechanism includes a controller and a temperature sensor, the controller is fixedly installed on the right side of the barrel body, and the temperature sensor is installed on the right inner wall of the barrel body.

[0009] Furthermore, the transmission mechanism includes a driven gear and a driving gear, the driven gear is fixedly mounted on the transmission tube, the driving gear is fixedly mounted on the driven spiral feeding rod, and the driving gear and the driven gear are meshed with each other.

[0010] Furthermore, the stirring mechanism includes stirring blades and a one-way air outlet head, and the stirring blades and the one-way air outlet head are evenly installed on the transmission pipe in sequence from top to bottom.

[0011] Compared with the prior art, the utility model provides a tannin high-efficiency germanium precipitation reaction barrel, which has the following beneficial effects:

[0012] 1. The tannin high-efficiency germanium precipitation reaction barrel is equipped with a turning mechanism to turn the bottom material to the upper side of the barrel, and then the stirring mechanism is used to stir the material in the barrel. The material is turned while stirring, so that the material is evenly dispersed and the reaction is more complete, which greatly improves the processing efficiency.

[0013] 2. The tannin high-efficiency germanium precipitation reaction barrel is equipped with a heating mechanism to inject hot air into the air distribution cavity, which then flows into the transmission pipe through the air distribution cavity and is then blown into the barrel body through a one-way air outlet head, so as to quickly heat the internal material, make the heating more uniform, and make the reaction more complete and comprehensive, which is convenient for use. BRIEF DESCRIPTION OF THE DRAWINGS

[0014] Figure 1 It is a schematic diagram of the structure of the utility model;

[0015] Figure 2 It is a cross-sectional view of the utility model;

[0016] Figure 3It is a cross-sectional view of the flipping mechanism of the utility model.

[0017] In the figure: 1. barrel; 2. feeding valve; 3. flipping mechanism; 301. conveying cylinder; 302. electric screw feeding rod; 303. rectangular opening; 304. driven screw feeding rod; 4. discharge pipe; 5. gate valve; 6. conical bucket; 7. air distribution cavity; 8. heating mechanism; 801. electric heating box; 802. conduit; 803. exhaust assembly; 804. waterproof breathable valve; 9. control mechanism; 901. controller; 902. temperature sensor; 10. mechanical seal; 11. transmission pipe; 12. transmission mechanism; 121. driven gear; 122. driving gear; 13. stirring mechanism; 131. stirring blade; 132. one-way air outlet. DETAILED DESCRIPTION

[0018] The following will be combined with the drawings in the embodiments of the utility model to clearly and completely describe the technical solutions in the embodiments of the utility model. Obviously, the described embodiments are only part of the embodiments of the utility model, not all of the embodiments. Based on the embodiments in the utility model, all other embodiments obtained by ordinary technicians in this field without creative work are within the scope of protection of the utility model.

[0019] See also Figure 1-Figure 3 The utility model discloses a tannin high-efficiency germanium precipitation reaction barrel, comprising a barrel body 1, a feeding valve 2 is fixedly installed on the upper side wall of the barrel body 1 near the left position, a flipping mechanism 3 is fixedly installed on the middle position of the upper side wall of the barrel body 1, a discharge pipe 4 is fixedly installed on the lower inner wall of the barrel body 1 below the flipping mechanism 3, and a gate valve 5 is arranged on the discharge pipe 4, a conical bucket 6 is fixedly installed between the outer surface of the discharge pipe 4 near the upper side position and the inner wall of the barrel body 1, and an air distribution cavity 7 is arranged between the conical bucket 6 and the lower inner wall of the barrel body 1, and the air distribution cavity 7 and the heating mechanism 8 are connected. The heating mechanism 8 is connected to the upper side of the barrel body 1, and the heating mechanism 8 is fixedly installed on the right side of the barrel body 1. The right side of the barrel body 1 is provided with a control mechanism 9. Mechanical seals 10 are evenly fixedly installed on all sides of the conical bucket 6, and transmission pipes 11 are fixedly installed in the mechanical seals 10. The transmission pipe 11 is connected to the flipping mechanism 3 through a transmission mechanism 12. The lower surface of the transmission pipe 11 is an open structure, and the lower surface of the transmission pipe 11 is inserted in the air distribution cavity 7. A stirring mechanism 13 is provided on the transmission pipe 11 near the upper side.

[0020] Specifically, the flipping mechanism 3 includes a conveying cylinder 301, an electric screw feeding rod 302, a rectangular opening 303 and a driven screw feeding rod 304. The conveying cylinder 301 is fixedly installed on the upper side wall of the barrel body 1, and the lower surface of the conveying cylinder 301 is an open structure. The electric screw feeding rod 302 is fixedly installed on the upper side wall of the conveying cylinder 301. The left and right side walls of the conveying cylinder 301 are both provided with rectangular openings 303 near the upper side. The driven screw feeding rod 304 is installed on the lower surface of the electric screw feeding rod 302, and the driven screw feeding rod 304 is inserted into the discharge pipe 4.

[0021] In this embodiment, the electric screw feeding rod 302 rotates in the conveying cylinder 301, so that the material on the lower side of the barrel body 1 is driven by the electric screw feeding rod 302 to move upward, and then flows out through the rectangular opening 303, achieving the effect of turning the material. At the same time, the driven screw feeding rod 304 enables the discharge pipe 4 to be discharged smoothly.

[0022] Specifically, the heating mechanism 8 includes an electric heating box 801, a conduit 802, an exhaust assembly 803 and a waterproof breathable valve 804. The electric heating box 801 is fixedly installed on the right side of the barrel body 1. The air outlet of the electric heating box 801 is connected to the air distribution cavity 7 through the conduit 802. The electric heating box 801 is connected to the waterproof breathable valve 804 through the exhaust assembly 803. The waterproof breathable valve 804 is embedded in the upper side wall of the barrel body 1.

[0023] In this embodiment, the exhaust component 803 extracts the gas in the barrel body 1 through the waterproof breathable valve 804, and draws the gas into the electric heating box 801, and the electric heating box 801 heats the gas, so that the heated gas flows into the air distribution cavity 7 through the conduit 802.

[0024] Specifically, the control mechanism 9 includes a controller 901 and a temperature sensor 902 . The controller 901 is fixedly installed on the right side of the barrel body 1 , and the temperature sensor 902 is installed on the right inner wall of the barrel body 1 .

[0025] In this embodiment, the temperature sensor 902 detects the temperature inside the barrel body 1, so that the controller 901 controls the opening and closing of the heating mechanism 8.

[0026] Specifically, the transmission mechanism 12 includes a driven gear 121 and a driving gear 122 . The driven gear 121 is fixedly mounted on the transmission tube 11 , and the driving gear 122 is fixedly mounted on the driven spiral feeding rod 304 . The driving gear 122 and the driven gear 121 are meshed with each other.

[0027] In this embodiment, the driving gear 122 rotates along with the driven spiral feeding rod 304 , so that the driving gear 122 drives the driven gear 121 to rotate, and the driven gear 121 drives the transmission tube 11 to rotate.

[0028] Specifically, the stirring mechanism 13 includes a stirring blade 131 and a one-way air outlet head 132 , and the stirring blade 131 and the one-way air outlet head 132 are evenly installed on the transmission pipe 11 in sequence from top to bottom.

[0029] In this embodiment, the stirring blade 131 rotates with the transmission tube 11 to stir the material in the barrel body 1, and the one-way air outlet head 132 allows hot air to flow into the barrel body 1, and the one-way air outlet head 132 rotates with the transmission tube 11 to evenly distribute the hot air in the barrel body 1, making the heating more uniform.

[0030] When in use, tannin material is poured into the barrel 1 filled with germanium reaction raw materials through the feeding valve 2, and the electric screw feeding rod 302 in the flipping mechanism 3 rotates in the conveying cylinder 301, so that the material on the lower side of the barrel 1 is driven by the electric screw feeding rod 302 to move upward, and then flows out through the rectangular opening 303, so as to achieve the effect of flipping the material. At the same time, the electric screw feeding rod 302 drives the driven screw feeding rod 304 to rotate, and the driven screw feeding rod 304 drives the driving gear 122 in the transmission mechanism 12 to rotate, so that the driving gear 122 drives the driven gear 121 to rotate, and the driven gear 121 drives the transmission tube 11 to rotate, and the transmission tube 11 drives the stirring blade 131 in the stirring mechanism 13 to rotate, so that the material at the bottom of the barrel 1 is flipped to the upper side of the barrel 1, and then the material is flipped. At the same time, stirring is carried out to make the materials evenly dispersed and the reaction more complete, which greatly improves the processing efficiency. The temperature in the barrel body 1 is detected by the temperature sensor 902 in the control mechanism 9. When the temperature is low, the information is fed back to the controller 901. The controller 901 turns on the heating mechanism 8, and the exhaust component 803 extracts the gas in the barrel body 1 through the waterproof breathable valve 804, and draws the gas into the electric heating box 801. The gas is heated by the electric heating box 801, so that the heated gas flows into the air distribution cavity 7 through the conduit 802, and then flows into the transmission pipe 11 through the air distribution cavity 7, and then is blown into the barrel body 1 through the one-way air outlet head 132 on the transmission pipe 11, so as to quickly heat the material inside the barrel body 1, make the heating more uniform, and make the reaction more complete and comprehensive, which is convenient for use.

[0031] In summary, the tannin high-efficiency germanium precipitation reaction barrel turns the material while stirring, so that the material is evenly dispersed and the reaction is more sufficient, which greatly improves the processing efficiency. At the same time, it is convenient to quickly heat the internal material, making the heating more uniform, the reaction more sufficient and comprehensive, and easy to use.

[0032] Although the embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that various changes, modifications, substitutions and variations may be made to the embodiments without departing from the principles and spirit of the present invention, and that the scope of the present invention is defined by the appended claims and their equivalents.

Claims

1. A tannin high-efficiency germanium precipitation reaction barrel, comprising a barrel body (1), characterized in that: A feeding valve (2) is fixedly installed on the upper side wall of the barrel body (1) near the left side, a flipping mechanism (3) is fixedly installed on the middle position of the upper side wall of the barrel body (1), a discharge pipe (4) is fixedly installed on the lower inner wall of the barrel body (1) below the flipping mechanism (3), and a gate valve (5) is provided on the discharge pipe (4), a conical bucket (6) is fixedly installed between the outer surface of the discharge pipe (4) near the upper side and the inner wall of the barrel body (1), and an air distribution cavity (7) is provided between the conical bucket (6) and the lower inner wall of the barrel body (1), the air distribution cavity (7) is connected to the heating mechanism (8), and the heating mechanism (8) is connected to the barrel body (1). The barrel (1) and the drum (6) are connected to each other on the upper side thereof, the heating mechanism (8) is fixedly mounted on the right side of the barrel (1), the right side of the barrel (1) is provided with a control mechanism (9), mechanical seals (10) are evenly fixedly mounted on the four sides of the conical bucket (6), and transmission pipes (11) are fixedly mounted inside the mechanical seals (10), the transmission pipes (11) are connected to the turning mechanism (3) by transmission mechanism (12), the lower surface of the transmission pipe (11) is an open structure, and the lower surface of the transmission pipe (11) is inserted into the air distribution cavity (7), and a stirring mechanism (13) is provided on the transmission pipe (11) near the upper side.

2. A tannin high-efficiency germanium precipitation reaction barrel according to claim 1, characterized in that: The flipping mechanism (3) comprises a conveying cylinder (301), an electric screw feeding rod (302), a rectangular opening (303) and a driven screw feeding rod (304); the conveying cylinder (301) is fixedly mounted on the upper side wall of the barrel body (1); the lower surface of the conveying cylinder (301) is an open structure; the electric screw feeding rod (302) is fixedly mounted on the upper side wall of the conveying cylinder (301); the left and right side walls of the conveying cylinder (301) are both provided with rectangular openings (303) near the upper side; the driven screw feeding rod (304) is mounted on the lower surface of the electric screw feeding rod (302), and the driven screw feeding rod (304) is inserted into the discharge pipe (4).

3. A tannin high-efficiency germanium precipitation reaction barrel according to claim 1, characterized in that: The heating mechanism (8) comprises an electric heating box (801), a conduit (802), an air extraction assembly (803) and a waterproof breathable valve (804); the electric heating box (801) is fixedly mounted on the right side of the barrel body (1); the air outlet of the electric heating box (801) is connected to the air distribution cavity (7) via the conduit (802); the electric heating box (801) is connected to the waterproof breathable valve (804) via the air extraction assembly (803); and the waterproof breathable valve (804) is embedded in the upper side wall of the barrel body (1).

4. A tannin high-efficiency germanium precipitation reaction barrel according to claim 1, characterized in that: The control mechanism (9) comprises a controller (901) and a temperature sensor (902); the controller (901) is fixedly mounted on the right side of the barrel body (1); and the temperature sensor (902) is mounted on the right inner wall of the barrel body (1).

5. The tannin high-efficiency germanium precipitation reaction barrel according to claim 1, characterized in that: The transmission mechanism (12) comprises a driven gear (121) and a driving gear (122); the driven gear (121) is fixedly mounted on the transmission tube (11); the driving gear (122) is fixedly mounted on the driven spiral feeding rod (304); and the driving gear (122) and the driven gear (121) are meshed with each other.

6. The tannin high-efficiency germanium precipitation reaction barrel according to claim 1, characterized in that: The stirring mechanism (13) comprises a stirring blade (131) and a one-way air outlet head (132), and the stirring blade (131) and the one-way air outlet head (132) are evenly installed on the transmission pipe (11) in sequence from top to bottom.

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