Method for prolonging cycle of oparation of pimelinketone device and equipment thereof
A technology of operation cycle and cyclohexanone, which is applied in chemical instruments and methods, preparation of organic compounds, preparation of carbon-based compounds, etc., can solve the problems of high investment cost and complicated process
Active Publication Date: 2010-05-19
EAST CHINA UNIV OF SCI & TECH
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Problems solved by technology
Although this method can solve the effective separation of saponification waste lye, it has the disadvantages of complicated process and high investment cost.
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[0080] The largest commercial cyclohexanone production base in my country, which was completed and put into operation in April 2005, is the transformation of the waste alkali separation system of the 80,000 tons / year cyclohexanone production unit of the Cyclohexanone Division of Sinopec Baling Petrochemical Co., Ltd. Take an example to illustrate the effect of this technology.
[0081] (1) Analysis method
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Abstract
A method lengthening the cyclohexanone device continuous running period and equipment are provided. The method can completely and effectively separate the oxidation solution waste alkali of the cyclohexanone and realize the low energy consumption, small investment and pollution, which is suitable for the stable running for long period.
Description
Technical field [0001] The invention relates to a method for extending the continuous operation period of a cyclohexanone device. More specifically, it relates to a dealkalization method for the waste alkali produced in the production process of cyclohexanone by first injecting water to enrich the alkaline substance, and then performing cyclonic separation of the alkaline water from the organic acid and ester. The invention also relates to equipment for extending the continuous operation period of the cyclohexanone device. Background technique [0002] As an important organic chemical product, cyclohexanone has a wide range of uses. Our country also imports 30-50% of domestic output of cyclohexanone every year. In the production process of cyclohexanone, the oxidation liquid produced by the oxidation process is treated with a strong alkali (3-5% sodium hydroxide) aqueous solution in the decomposition kettle to produce water, sodium hydroxide, organic sodium salt, Saponified was...
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Patent Type & Authority Patents(China)
IPC IPC(8): C07C45/33C07C49/403
Inventor 汪华林周萍白志山马吉杨强钱卓群
Owner EAST CHINA UNIV OF SCI & TECH
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