Anti-constipation composition
a composition and anti-constipation technology, applied in the field of anti-constipation composition, can solve the problems of poor intra-pooling effect, inability to use pges or pgfs as cathartic agents, and unknown activity of bi-cyclic tautomers as anti-constipation treatment and prevention agents,
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example 1
[0116]The biological activity of compositions due to the ratios of mono-cyclic / bi-cyclic structures when Z of general formula (I) is an oxygen atom, and a ketone is present at the C-9 position of the present invention can be seen from the following examples. The number of fluorine atoms at the C-16 position and the ratio of mono-cyclic / bi-cyclic structures are shown in Table 1.
[0117]Enteropooling tests and diarrhea tests were conducted. The results are set forth in Table 1. The dose that raise the intraintestinal content by 50% was referred to as ED50.
TABLE 1Example AExample BComparative Example ANumber of F atoms210at C-16 positionRatio of mono-4:961:1No signal derived fromcyclic / bi-cyclicbi-cyclic structure wasstructure*detected.Enteropooling0.6 μg / kg2 μg / kg320 μg / kgactivity, ED50Diarrhea in mice+: at 3 mg / kg (PO1)±: at 0.3 mg / kg (SC)−: at 10 mg / kg (PO)+: at 0.3 mg / kg (SC2)−: at 1 mg / kg (SC)*Determined by NMR measurement, in CDCl3 solution.1PO is by mouth (oral administration)2SC ...
example 2
[0118]The biological activity of the composition due to the ratios of mono-cyclic / bi-cyclic structures when Z in Formula (I) is an oxygen, a ketone is present at the C-9 position, and there is a double bond between the 5,6-carbons is shown below.
Enteropooling tests and diarrhea tests were conducted. The results are set forth below in Table 2. The dose that raise the intraintestinal content by 50% was referred to as ED50.
TABLE 2Example CExample DComparative Example CNumber of F atoms210at C-16 positionRatio of mono-4:961:1no signal derived fromcyclic / bi-cyclicbi-cyclic structure wasstructure*detected.Enteropooling0.3 μg / kg3 μg / kg220 μg / kgactivity, ED50Diarrhea in mice+: at 1 mg / kg (PO)1−: at 1 mg / kg (PO)−: at 10 mg / kg (PO)+: at 5 mg / kg (PO)*Determined by NMR measurement in CDCl3 solution.1PO is by mouth (oral administration)
Effect of the Present Invention Dissolved in Medium Chain Fatty Acid Triglyceride on Bowel Movement after Single Oral Administration to Healthy Male Volunteers
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