The invention discloses a 
mass titration device with a 
titration protective component and a 
titration method. The device comprises a balance scale, a titration 
bottle, a base, a polished opening conical 
bottle and a connecting 
pipe, wherein the balance scale is used for weighing the titration 
bottle and the base; the titration bottle comprises a bottle body, and a cock cavity is arranged below the bottle body, is connected with a leakage 
pipe and a casing 
pipe sleeving the casing pipe, and is internally provided with a cock; the cock is provided with a communicating hole; when the cock rotates to the communicating part, the communicating hole communicates the bottle body and the leakage pipe; the outer side of the end head of the casing pipe is polished to form a 
polishing opening plug; the connecting pipe is connected with a filter or an 
inert gas, and is used for connecting the titration bottle with the conical bottle; the length of the leakage pipe is greater than the total length of the casing pipe and the connecting pipe which are connected with each other; the base and one end of the connecting pipe are provided with 
polishing openings matched with the 
polishing opening plug. According to the invention, the titration process can be protected, interference factors of titration can be eliminated, and the measurement is accurate.