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94results about How to "No use" patented technology

Preparation method of carbon nano material-modified polymer

The invention provides a preparation method of a carbon nano material-modified polymer. The preparation method comprises the following steps: 1) adding a thermoplastic polymer and a carbon nano material into a ball mill, wherein the ratio of the material to balls is 1:(2-5); ball-milling for 1-8 hours under the condition of 50-300 rpm to obtain a raw material, wherein the mass percentage of the carbon nano material is 0.05-15 percent of that of the polymer, grinding bodies in the ball mill are grinding balls with different sizes made of two kinds of same materials, and the mass ratio of the big balls to the small balls is 1:(1-6); 2) performing melt extrusion on the raw material by utilizing a single screw extruder or a double-screw extruder and curing to obtain a fibrous carbon nano material-modified polymer; or hot-pressing the raw material by utilizing a hot press to obtain the flaky carbon nano material-modified polymer. According to the preparation method provided by the invention, the dispersing properties of a carbon nano tube and grapheme in a polymer matrix layer in the melt spinning process are improved, and the physical and mechanical properties or the electrical conductivity or the thermal conductivity of a polymer composite material are effectively improved.
Owner:TIANJIN POLYTECHNIC UNIV

Preparation method of lyophilization sulbactam sodium material medicine

The invention belongs to the field of medicine and chemical industry. The invention relates to a preparation method of a lyophilization sulbactam sodium material medicine, which comprises the following steps of: (1) adding sodium bicarbonate into sulbactam acid suspension to obtain a lyophilization sulbactam sodium material liquid medicine; (2) filtering the liquid medicine by utilizing a filter; (3) uniformly pouring the sterile liquid medicine into a material disk of a freeze drier, setting the temperature of a baffle plate to be -40 DEG C to -10 DEG C for freezing for 1-6h, then setting the temperature of the baffle plate to be -10 DEG C to 10 DEG for keeping for 1-10h, then setting the temperature of the baffle plate to be 10 DEG C to 20 DEG C for drying 1-20h, then setting the temperature of the baffle plate to be 20-50 DEG C for drying for 1-30h, finally setting the temperature of the baffle plate to be 50-65 DEG C for drying 1-20h; and (4) grinding and uniformly mixing the lyophilization powder prepared from the step (3) to obtain the lyophilization sulbactam sodium material medicine. The products prepared by the preparation method of a lyophilization sulbactam sodium material medicine has the advantages of good clarity index and high content; and bad factors of solvent residues, clarity foreign matters, turbidity and the like prepared by utilizing a solvent method can be avoided.
Owner:SHIJAZHUANG ZHONGSHUO PHARMA CO LTD +1

Preparation method of star-shaped polyurethane elastomer toughened polylactic acid compound

ActiveCN107189386AEfficient and controllable synthesisGood mechanical propertiesPolyurethane elastomerSolvent
The invention provides a simple polylactic acid toughening modification method, in particular to a method for preparing a toughened polylactic acid compound by taking star-shaped polyurethane as a toughening modifier. The toughened polylactic acid compound with a better toughening effect is prepared by adding polyisocyanate as a crosslinking agent. The preparation method of the star-shaped polyurethane toughened polylactic acid compound comprises the following steps: adding 60 to 99 parts of polylactic acid, 1 to 40 parts of star-shaped polyurethane and 0 to 10 parts of polyisocyanate into a torque rheometer for compounding and banburying; performing a co-blending reaction at the temperature of 170 to 210 DEG C and at the rotation speed of 30 to 120 revolutions per minute for 3 to 20 minutes. The star-shaped polyurethane is prepared by adopting a simple bulk one-step method or a bulk pre-polymerizing method. The preparation method is easy to operate, is short in preparation period, is high in efficiency, and has the advantages of lowering equipment investment and production cost and overcoming the defects caused by adoption of solvents in the prior art, along with no need of catalyst, environment-friendly production process, and easiness in popularization and application.
Owner:TAIYUAN INST OF TECH

Flame-retardant, antibacterial and transparent super-amphiphobic paint and preparation method and application thereof

ActiveCN110283529ARich in practical application valueRich application valueFireproof paintsAntifouling/underwater paintsIonSolvent
The invention discloses flame-retardant, antibacterial and transparent super-amphiphobic paint and a preparation method and application thereof. The flame-retardant, antibacterial and transparent super-amphiphobic paint is prepared by the following steps: firstly preparing inorganic/organic nanoparticles modified by a nitrogen-containing positive ion silane coupling agent, and dispersing the inorganic/organic nanoparticles along with flame retardant particles and a fluorine-containing silane coupling agent in a solvent and reacting. By a spray-coating, brush-coating or dip-coating method, the paint is applied on the surface of a metallic base material, an inorganic base material or an organic polymer base material. The use amount of the coating obtained is less. It can be effectively ensured that characteristics such as color, texture, pores, air permeability, etc. of the surface of the base material are unchanged, and excellent and stable super-amphiphobic property, flame retardant property and antibacterial property can be obtained. Meanwhile, the preparation is simple, the raw materials are cheap and easily available, and no toxic organic solvent is used. The preparation condition is mild, and the preparation is carried out at normal temperature and in an ordinary state and is environmentally-friendly. The preparation cost is low. Thus, the method is suitable for large-scale production and is good for industrial application and promotion.
Owner:SICHUAN UNIV

Rosa roxburghii tratt powder rich in vitamin C and preparation method thereof

The invention discloses rosa roxburghii tratt powder rich in vitamin C and a preparation method thereof. The preparation method comprises the following steps: (1) pre-treating rosa roxburghii tratt toobtain rosa roxburghii tratt juice or concentrated juice; (2) fermenting the rosa roxburghii tratt juice by using saccharomyces cerevisiae; (3) sequentially filtering by using filter cloth and a nanofilter element ceramic membrane; (4) performing vacuum concentration treatment; and (5) drying. According to the preparation method disclosed by the invention, the saccharomyces cerevisiae is added in the preparation process of the rosa roxburghii tratt powder, and carbohydrates in the feed liquid are effectively reduced through the fermentation effect of the saccharomyces cerevisiae, so that theproportion of the vitamin C in the material is increased, and the content of the vitamin C in the rosa roxburghii tratt powder disclosed by the invention reaches 17% or above. According to the preparation method disclosed by the invention, SOD is effectively enriched, and the content can reach 10-15,000U/g; the yeast and other impurities are filtered by the ceramic membrane, high-temperature treatment is avoided, and degradation of VC is reduced; and the rosa roxburghii tratt powder prepared by the preparation method disclosed by the invention is good in fluidity, effectively inhibits the caking problem, and can be applied to industrial production.
Owner:广东青云山药业有限公司

DA reaction-based fluorine-containing polyacrylate self-repairing coating and preparation method thereof

The invention discloses a preparation method of a DA reaction-based fluorine-containing polyacrylate self-repairing coating. The method comprises the following steps: preparing a mixed monomer and aninitiator aqueous solution; separately weighing polyacrylic acid-b-hexafluorobutyl polyacrylate, deionized water, and an alkali according to the mass of the mixed monomer, adding polyacrylic acid-b-hexafluorobutyl polyacrylate, deionized water, and the alkali into a reactor together with 25-30% of the mixed monomer, introducing argon and performing heating, and adding the initiator aqueous solution to prepare a seed emulsion; dropwise adding the remaining initiator aqueous solution and mixed monomer into the seed emulsion, and carrying out a reaction to obtain a furyl-containing fluorine-containing polyacrylate soap-free emulsion; and dissolving a maleimide-based crosslinking agent in an organic solvent and then performing uniform mixing with the furyl-containing emulsion, and coating thesurface of a substrate with the mixed solution for curing to form the self-repairing coating. The preparation method of the self-repairing coating is mild, and does not use a large amount of solvents.The self-repairing coating has good water and oil repellency and good self-repairing performance, and at the same time, the applicable substrate of the coating is wide.
Owner:SHAANXI UNIV OF SCI & TECH

Method for extracting lycium barbarum polysaccharide

The invention discloses a method for extracting lycium barbarum polysaccharide. The method for extracting the lycium barbarum polysaccharide comprises the following steps: A, weighing a certain weightof lycium barbarum, performing vacuum freeze drying, crushing and passing through a sieve of 60 to 80 meshes; B, taking the sieved dried lycium barbarum powder, adding 700 to 900 ml of water into per100 g of lycium barbarum according to the material liquid ratio, and stirring uniformly; C, adding cellulase and papain, putting into ultrasonic extraction equipment and extracting enzymolysis liquid; D, filtering the enzymolysis liquid to obtain filtrate, adding absolute ethanol into the filtrate according to the ratio of 1:4, precipitating and standing at 4 DEG C for 24 hours, centrifuging for15 minutes at the centrifugal rotating speed of 5000 rpm, collecting the precipitate, performing freeze drying, crushing and passing through a 80-mesh sieve to obtain soluble polysaccharide. Enzymolysis is assisted by high-frequency ultrasonic treatment, so that the obtaining time of the lycium barbarum polysaccharide is greatly shortened, the polysaccharide extraction rate is relatively high on the premise of guaranteeing the purity of the lycium barbarum polysaccharide, treatment equipment is simple, a toxic organic solvent is not used, and industrialization is facilitated.
Owner:邱媛媛

Desulfurization gypsum powder decorating board

The invention discloses a desulfurization gypsum powder decorating board. A raw material formula of the desulfurization gypsum powder door pocket board is as follows: 60-70 percent of desulfurization gypsum powder, 8-12 percent of epoxy resins, 4.8-5.2 percent of polyvinyl chloride, 4.8-5.2 percent of foam regulating agents, 4.8-5.2 percent of activated charcoal (AC) foaming agents, 2.8-3.2 percent of stearic acid, 3.8-4.2 percent of calcium stearate and 4.8-5.2 percent of glazes. A preparation method of the desulfurization gypsum powder decorating board comprises the following steps of: (1) weighing the materials in the proportion of the raw material formula; (2) mixing and stirring the weighed materials; (3) performing extrusion molding on a mixed material by virtue of an extruding machine; (4) heating and conserving molded blank bodies; (5) manufacturing semi-finished products which are subjected to the conservation to be blank bodies by using a board pressing machine; (6) delivering the pressed blank bodies to a drying kiln for drying; (7) performing atomization and glaze spraying on the dried desulfurization gypsum powder decorating board by using the conventional method; and (8) drying the desulfurization gypsum powder decorating board onto which the glazes are sprayed. The desulfurization gypsum powder decorating board has the advantages of corrosion resistance, weather resistance and the like.
Owner:朔州市润臻新技术开发有限公司

A kind of flame retardant antibacterial transparent superamphiphobic coating and its preparation method and application

The invention discloses flame-retardant, antibacterial and transparent super-amphiphobic paint and a preparation method and application thereof. The flame-retardant, antibacterial and transparent super-amphiphobic paint is prepared by the following steps: firstly preparing inorganic / organic nanoparticles modified by a nitrogen-containing positive ion silane coupling agent, and dispersing the inorganic / organic nanoparticles along with flame retardant particles and a fluorine-containing silane coupling agent in a solvent and reacting. By a spray-coating, brush-coating or dip-coating method, the paint is applied on the surface of a metallic base material, an inorganic base material or an organic polymer base material. The use amount of the coating obtained is less. It can be effectively ensured that characteristics such as color, texture, pores, air permeability, etc. of the surface of the base material are unchanged, and excellent and stable super-amphiphobic property, flame retardant property and antibacterial property can be obtained. Meanwhile, the preparation is simple, the raw materials are cheap and easily available, and no toxic organic solvent is used. The preparation condition is mild, and the preparation is carried out at normal temperature and in an ordinary state and is environmentally-friendly. The preparation cost is low. Thus, the method is suitable for large-scale production and is good for industrial application and promotion.
Owner:SICHUAN UNIV
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