Plasma and enzyme combined anti-felting method for tidying wool knitted fabric

A technology of wool knitted fabric and plasma, which is applied in biochemical fiber treatment, fiber treatment, animal fiber, etc., can solve the problem of excessive damage to wool fiber, and achieve the effect of improving the anti-felting process

Inactive Publication Date: 2008-05-14
DONGHUA UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] The purpose of the present invention is to provide a wool knitted fabric anti-felting finishing method combined with plasma and biological enzymes to solve the problem of excessive damage to wool fibers in the protease finishing, and to control fiber damage through plasma pretreatment and TG enzyme Repair process to reduce the damage of protease to the interior of wool fibers; develop machine-washable wool knitted fabrics with anti-felting and low-strength damage

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] Example 1 Plasma treatment of wool knitted fabric

[0024] Process flow: wool scouring→plasma treatment

[0025] in:

[0026] 1) Wool washing: The wool knitted fabric is treated at a constant temperature of 40°C for 30 minutes in 0.5 g / L wool washing liquid at a bath ratio of 1:30. Drain lightly, dry and set aside.

[0027] 2) Plasma treatment:

[0028] Treat at 30Pa, 100W for 3min. Gas: air.

[0029] The wool knitted fabric treated by the above process has an anti-felting rate of 10.47% (untreated 17.20%), and a bursting strength of 0.276Mpa, which is 6.15% stronger than the bursting strength of 0.260Mpa after scouring.

Embodiment 2

[0030] Embodiment 2: Plasma combined with protease to treat wool knitted fabric

[0031] Process flow: wool scouring→plasma treatment→protease treatment→water washing→drying

[0032] 1) Wool washing: The wool knitted fabric is treated at a constant temperature of 40°C for 30 minutes in 0.5 g / L wool washing liquid at a bath ratio of 1:30. Drain lightly, dry and set aside.

[0033] 2) Plasma treatment:

[0034] Treat at 30Pa, 100W for 3min. Gas: air.

[0035] 3) Protease treatment:

[0036] The mass concentration of protease is 4% (o.w.f) (weight to wool), the temperature is 50° C., the time is 40 minutes, the bath ratio is 1:20, and the pH is 8.5.

[0037] 4) Washing:

[0038] Treat at 90°C for 10 minutes, and inactivate the enzyme at high temperature. Wash twice in cold water, gently absorb the water, dry at 80°C, and set aside.

[0039] The wool knitted fabric treated by the above process has an anti-felting rate of 1.79% (untreated 17.20%) and a burst...

Embodiment 3

[0040] Example 3 Plasma combined with protease and transglutaminase (TGase) to treat wool knitted fabrics

[0041] Process flow: wool scouring→plasma treatment→protease treatment→water washing→transglutaminase treatment→water washing→drying

[0042] in:

[0043] 1) Wool washing: The wool knitted fabric is treated at a constant temperature of 40°C for 30 minutes in 0.5 g / L wool washing liquid at a bath ratio of 1:30. Drain lightly, dry and set aside.

[0044] 2) Plasma treatment:

[0045] Treat at 30Pa, 100W for 3min. Gas: Air.

[0046] 3) Protease treatment:

[0047] The mass concentration of protease is 4% (o.w.f) (weight to wool), the temperature is 50° C., the time is 40 minutes, the bath ratio is 1:20, and the pH is 8.5.

[0048] 4) Washing:

[0049] Treat at 90°C for 10 minutes, and inactivate the enzyme at high temperature. Wash twice in cold water, gently absorb the water, dry at 80°C, and set aside.

[0050] 5) Transglutaminase treatment:

[0051] The mass co...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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PUM

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Abstract

The invention relates to an antifelting finish method of wool knits combining plasma and bio-enzyme, comprising the steps that: wool washing, plasma treatment, protease treatment, water washing, Transglutaminase treatment, water washing, and drying. The invention can lead wool knits to reach machine washable standard (with a felting rate less than 2 percent) while the intensity is ensured (intensity damage is less than 10 percent), and has little damage during the finish process, with safety and environmental protection performance, and is an energy-conservation and clean wool post-treatment technique.

Description

technical field [0001] The invention belongs to the field of anti-felting of wool, in particular to an anti-felting finishing method of wool knitted fabrics combined with plasma and biological enzymes. Background technique [0002] When wool products are processed and washed, the oriented scales will be rubbed to cause displacement between fibers, resulting in shrinkage, resulting in shrinkage of the product size, unclear lines, etc., which seriously affect the appearance, feel, easy care and wearing performance. At present, the domestic wool anti-felting process generally adopts a relatively mature chlorination method and a two-step method of chlorinating a resin (IWS / CSIRO Chlorine Hercosett method). These two methods are based on chlorination treatment, which are easy to absorb chlorine and turn yellow, and cause great damage to the fiber strength. Not only the wool fiber is severely eroded by chemicals, but also there are a large amount of absorbable organic halogenated ...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06M16/00D06M10/02D06M101/10
Inventor 张瑞萍蔡再生
Owner DONGHUA UNIV
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