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A kind of preparation method of biomass carbon material doped with molybdenum phosphide nanoparticles with pore network structure

A biomass carbon and nanoparticle technology, applied in chemical instruments and methods, water pollutants, other chemical processes, etc., can solve the problems of cumbersome preparation process, high cost, unfavorable production and preparation, etc., and achieve simple preparation process and easy separation. , the effect of reducing the burden on the marine environment

Inactive Publication Date: 2021-04-13
QINGDAO UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

At present, most of the design and preparation of porous carbon is based on the traditional hard template method and soft template method. These methods can effectively control the morphology and pore size of carbon materials, but the preparation process is cumbersome and costly, which is not conducive to large-scale Production scale

Method used

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  • A kind of preparation method of biomass carbon material doped with molybdenum phosphide nanoparticles with pore network structure
  • A kind of preparation method of biomass carbon material doped with molybdenum phosphide nanoparticles with pore network structure
  • A kind of preparation method of biomass carbon material doped with molybdenum phosphide nanoparticles with pore network structure

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Experimental program
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Effect test

Embodiment 1

[0045] An in-situ conversion preparation method of a molybdenum phosphide-doped biomass-carbon composite material with a pore network structure is characterized in that it is prepared from Enteromorpha as a biomass carbon source, and is mainly prepared from the following raw materials in parts by weight become:

[0046] 1 part dried Enteromorpha, 1 part sodium hypochlorite, 1 part glacial acetic acid, 1 part ammonium molybdate.

[0047] The in-situ conversion preparation method of a kind of biomass carbon-based composite material of the present invention comprises the following steps:

[0048] (1) The salvaged Enteromorpha enteromorpha was rinsed with water, dried in a vacuum oven at 80°C, and set aside.

[0049] (2) Place the dried Enteromorpha in acidified sodium hypochlorite solution for decolorization, specifically, take 10g of dried Enteromorpha and soak it in 200mL acidified sodium hypochlorite solution (the solution kind contains 1.5mL of glacial acetic acid and 1.99g ...

Embodiment 2

[0053] Weigh 2mg of MoP / HPC composite material, add 1.0mL model dye solution (100mg L -1 , pH4~10), the mixture was centrifuged at 2000rpm for 2min after shaking and adsorption for 5min, and the supernatant was collected for quantitative analysis of the residual dye in the initial solution. The test was carried out on a U3900 ultraviolet-visible spectrometer, and the characterization results are as follows figure 2 shown.

Embodiment 3

[0055] Weigh 2mg of MoP / HPC composite material, add 1.0mL methylene blue solution (MB) (5~5000mgL -1 , pH 10.0) and 1.0mL Rose Bengal (RB) (5~5000mg L -1 , pH 10.0), the mixture was centrifuged at 2000rpm for 2min after shaking and adsorption for 5min, and the supernatant was collected for quantitative analysis of the residual dye in the initial solution. The test was carried out on a U3900 ultraviolet-visible spectrometer, and the characterization results are as follows image 3 shown.

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Abstract

The invention discloses a preparation method of a biomass carbon material doped with molybdenum phosphide nanoparticles with a pore network structure. The impregnated Enteromorpha is obtained by impregnating the decolorized Enteromorpha in an ammonium molybdate solution for a period of time, and the impregnated Enteromorpha Moss is heated to 350±10°C under the protection of inert gas for pre-carbonization for a period of time, and then heated to 700±10°C for carbonization to obtain oxide-doped porous carbon composite material MoO x / HPC, will MoO x / HPC and sodium hypophosphite are subjected to phosphating treatment for at least three times, wherein the phosphating treatment condition is to raise the temperature to 300±10° C. under an inert atmosphere. In the preparation method, enteromorpha is used as a carbon source, and the molybdenum phosphide-doped biomass porous carbon with a pore network structure is prepared by one-step in-situ conversion. Not only is the cost low, the reaction process is simple, green and the yield is high, it can achieve tonnage-level production, but it also helps to expand the application field and scope of natural biomass.

Description

technical field [0001] The invention belongs to the field of synthesis of inorganic nanometer materials, and in particular relates to a method for preparing a biomass carbon material doped with molybdenum phosphide nanoparticles with a pore network structure. Background technique [0002] In recent years, a variety of water pollutants caused by the rapid development of human society have received great attention, mainly including heavy metal ions, chemical toxins, petroleum derivatives, dyes and others. Among them, dye wastewater is mainly discharged by industries such as textiles, plastics, and papermaking, and the annual discharge accounts for about 20% of the total industrial wastewater. Dyes are mainly composed of complex aromatic compounds, which have potential carcinogenic and mutagenic effects, and high Chemical stability and strong resistance to biodegradation make it difficult to be degraded under natural conditions. Therefore, it is imminent to research and develo...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01J20/20C02F1/28B01J20/30C02F101/30
CPCB01J20/0259B01J20/20B01J2220/4843C02F1/283C02F2101/308
Inventor 张杨杨璐刘爱骅
Owner QINGDAO UNIV
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