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A method for analyzing components of electronic cigarette smoke liquid and smoke

A technology of e-cigarette liquid and analysis method, which is applied in the field of e-cigarette and tobacco analysis, can solve problems that have not been seen, and achieve the effects of wide promotion and use, good repeatability and high sensitivity

Active Publication Date: 2022-02-15
CHINA TOBACCO HUNAN INDAL CORP
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The applicant has checked the relevant literature and found no use of gas chromatography-mass spectrometry for the detection of acetol, ethyl 2-hydroxyacetate, acetic acid, dipropylene glycol, and 1,3-dihydroxyacetone in e-cigarette liquid and smoke. Tested Research Reports

Method used

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  • A method for analyzing components of electronic cigarette smoke liquid and smoke
  • A method for analyzing components of electronic cigarette smoke liquid and smoke
  • A method for analyzing components of electronic cigarette smoke liquid and smoke

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Embodiment 1

[0047] 1. Instruments, reagents and materials

[0048] Main instruments: Agilent 7890A-5975C gas chromatograph (Agilent Company), equipped with automatic sampler and EI source; COS-11B constant temperature oscillator (Shanghai Bilang Instrument Co., Ltd.); electronic balance (sensitivity 0.0001g) (Shanghai Yue Ping Scientific Instrument Manufacturing Co., Ltd.); Milli-Q 50 ultrapure water device (Millipore, USA); SM450 linear smoking machine (CERULEAN).

[0049] Reagents: Glycerin and propylene glycol are analytically pure, with a purity of ≥99%, purchased from Tianjin Damao Chemical Reagent Factory; 1,4-Butanediol, analytically pure, with a purity of ≥99%, purchased from Tianjin Guangfu Institute of Fine Chemicals; Acetol, purity ≥ 95%, purchased from AlfaAesar; 1,3-dihydroxyacetone, purity ≥ 99%, ethyl 2-hydroxyacetate, purity ≥ 99.1%, dipropylene glycol, purity ≥ 99.5%, were purchased from CHEM SERVICE.inc; acetic acid, analytically pure, purity ≥ 99.5%, purchased from Tia...

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Abstract

The invention relates to a method for analyzing components of e-cigarette smoke liquid and smoke gas. First, the standard solution of the target detection object is detected by a gas chromatography-mass spectrometer, and a standard curve is drawn by an internal standard method; Extract to obtain the test solution A, or extract the filter piece after capturing the flue gas with the extraction liquid to obtain the test solution B, after the corresponding test solution is detected by gas chromatography-mass spectrometry, calculate the test solution according to the standard curve The content of each target detection substance in the solution. By optimizing the parameter conditions of gas chromatography-mass spectrometry, the present invention can rapidly and accurately simultaneously quantitatively detect target detection substances in e-cigarette liquid and smoke, and realize rapid and accurate simultaneous determination of five target detection substances. The sensitivity of the detection method is High, good repeatability, can be widely used.

Description

technical field [0001] The invention relates to a method for analyzing electronic cigarette liquid and smoke components, belonging to the technical field of electronic cigarette and tobacco analysis Background technique [0002] At present, the existing e-cigarettes are becoming more and more common in the market, and their tastes are also diversified. The more common ones are tobacco aroma and fruit aroma. Spices, additives, etc. The main components in the e-cigarette liquid are propylene glycol and glycerin. If the purity of the propylene glycol and glycerin solvents is not up to the standard, there will be a certain amount of solvent residue, which will affect the quality of the e-cigarette liquid. Moreover, affected by environmental factors, such as light, temperature, etc., during the storage of e-cigarette liquid, propylene glycol, glycerin and other components have some slow chemical reactions among themselves or each other, and some substances will be produced. At ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N30/02
CPCG01N30/02
Inventor 龚淑果尹新强代远刚彭新辉黄建国孔波黄平
Owner CHINA TOBACCO HUNAN INDAL CORP
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