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Method for concurrently detecting 23 ester compounds in cigarette water-base adhesive

A technology of ester compounds and tobacco water-based glue, which is applied in the field of tobacco analysis, can solve the problems of unseen simultaneous detection, and achieve the effects of wide application, good repeatability, and high sensitivity

Active Publication Date: 2014-01-01
CHINA TOBACCO HUNAN INDAL CORP
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

After reviewing the relevant literature, there is no research report on the simultaneous detection of acetates, acrylates, methacrylates and phthalates in water-based adhesives for cigarettes by gas chromatography-mass spectrometry

Method used

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  • Method for concurrently detecting 23 ester compounds in cigarette water-base adhesive
  • Method for concurrently detecting 23 ester compounds in cigarette water-base adhesive
  • Method for concurrently detecting 23 ester compounds in cigarette water-base adhesive

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Embodiment 1

[0033] 1. Instruments, reagents and materials

[0034] Instrument: Agilent 7890A-5975C gas chromatograph (Agilent Company), equipped with automatic sampler and EI source; COS-11B constant temperature oscillator (Shanghai Bilang Instrument Co., Ltd.); Sartorius BS124S electronic balance (sensitivity 0.0001g); Milli-Q50 ultrapure water device (Millipore, USA); TGL-16M high-speed refrigerated centrifuge (Xiangyi Centrifuge Instrument Co., Ltd.).

[0035]Reagents: Isopropyl acetate (IA), Propyl acetate (PA), Butyl acetate (NBA), Methyl acrylate (MA), Ethyl acrylate (EA), Butyl acrylate (BA), Methyl methacrylate (MMA), ethyl methacrylate (EMA), butyl methacrylate (BMA), dimethyl phthalate (DMP), diethyl phthalate (DEP), diene phthalate Propyl phthalate (DAP), di-n-butyl phthalate (DBP), diisobutyl phthalate (DIBP), bis(4-methyl-2-pentyl) phthalate (BMPP) , Di(2-ethoxy)ethyl phthalate (DEEP), Dipentyl phthalate (DPP), Dihexyl phthalate (DHXP), Bis(2-phthalate) Butoxy) ethyl ester...

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Abstract

The present invention discloses a method for concurrently detecting 23 ester compounds in a cigarette water-base adhesive. The method comprises that: standard solutions of various ester compounds are detected through a gas chromatograph-mass spectrometer, and a standard curve is drawn by using an internal standard method; and a cigarette water-base adhesive sample is extracted through liquid-liquid extraction to obtain the solution requiring detection, the solution requiring detection is detected through the gas chromatograph-mass spectrometer, and contents of various ester compounds in the solution requiring detection are calculated according to the standard curve. According to the method, rapid, accurate and concurrent detection of 23 ester compounds in a cigarette water-base adhesive is achieved, and advantages of high sensitivity, good repeatability and the like are provided.

Description

technical field [0001] The invention relates to a method for simultaneously detecting 23 kinds of ester compounds in tobacco water-based glue, belonging to the technical field of tobacco analysis. Background technique [0002] Water-based glue is a viscous mixed emulsion that is neutral or weakly acidic at room temperature with a water-soluble or water-dispersible solvent as the medium. Compared with organic solvent-based adhesives, water-based adhesives have the advantages of no solvent release, non-flammability, safe use, and low cost. They have been widely used in packaging and printing, wood processing, cigarette manufacturing, and papermaking industries. Tobacco water-based glue is the water-based glue used in the cigarette manufacturing process, mainly including water-based glue for cigarettes and water-based glue for packaging. [0003] Affected by production raw materials, polymerization conditions, additives, etc., some harmful compounds remain in water-based adhes...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N30/88
Inventor 龚淑果吴名剑范湘红蒋腊梅钟科军刘锋
Owner CHINA TOBACCO HUNAN INDAL CORP
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