Methods of treating a subterranean formation with a treatment fluid having surfactant effective to increase the thermal stability of the fluid
a technology of hydrocarbonbearing subterranean formation and treatment fluid, which is applied in the direction of fluid removal, insulation, borehole/well accessories, etc., can solve the problems of subterranean formation rock that is subjected to hydraulic treatment literally cracking apart or breaking under strain, and fractures that tend to be squeezed closed
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example 1
[0066] In Example 1, Sample 1 was a borate-crosslinked HPG gel prepared without any of the surfactant blend, and Sample 2 contained 1 gal / Mgal of the surfactant blend.
[0067] Experiments on Samples 1 and 2 were conducted using a Nordman Model 50 viscometer according to a modified API2 test procedure as the sample was rapidly heated from room temperature to 240° F. in about 20 minutes and then held at 240° F. Viscosity was frequently measured at a shear rate of 81 / sec over a period of more than 3 hours.
[0068] The results of these experiments on Sample 1 and Sample 2 shown in the graph of FIG. 1 demonstrate an unexpectedly improved thermal stability of a borate crosslinked HPG gel with 1 gal / Mgal of the surfactant blend compared to an otherwise identical treatment fluid without any of the surfactant blend. In other words, the improved thermal stability is observed compared to an otherwise substantially identical treatment fluid without any of the surfactant.
example 2
[0069] In Example 2, experiments were conducted to study the effect of varying the concentration of the surfactant in the borate-crosslinked HPG gel. Sample 2 contained 1 gal / Mgal of the surfactant blend. Sample 3 contained 2 gal / Mgal of the surfactant blend. Sample 4 contained 3 gal / Mgal of the surfactant blend.
[0070] Experiments on Samples 2, 3, and 4 were conducted using a Nordman Model 50 viscometer according to a modified API2 test procedure as the sample was rapidly heated from room temperature to 285° F. (140° C.) in about 20 minutes and then held at 285° F. (140° C.). Viscosity was frequently measured at a shear rate of 81 / sec over a period of more than 3 hours.
[0071] The results shown in the graph of FIG. 2 demonstrate that increased surfactant concentrations unexpectedly improve the thermal stability of a borate-crosslinked HPG gel.
example 3
[0072] In this Example, four gel samples of the borate-crosslinked, 50 lb / Mgal HPG in 4% KCl water at a pH of about 10.5 were prepared containing varying amounts of the surfactant blend and sodium thiosulfate, as shown in Table 1:
TABLE 1Sample #Gal / Mgal surfactant blendLb / Mgal sodium thiosulfate500630701831
[0073] Samples 5, 6, 7, and 8 were evaluated on a Nordman Model 50 viscometer using a modified API2 test procedure as the sample was rapidly heated from room temperature to 285° F. (140° C.) in about 20 minutes and then held at 285° F. (140° C.). Viscosity was frequently measured at a shear rate of 81 / sec over a period of about 1.5 hours.
[0074] The results shown in the graph of FIG. 3 demonstrate an unexpected synergistic relationship between a surfactant and sodium thiosulfate for improving the thermal stability of a borate crosslinked HPG gel.
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