Photosensitive compositions and compounds used therein
A technology of photosensitive composition and photosensitive material, which is applied in the field of photosensitive composition and the compounds used in it, can solve the problems of poor adhesion strength and increased defects, and achieve the effect of small possibility and improvement of pattern adhesion strength
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Embodiment 1
[0105] 10 mol of 3-glycidyloxypropyltrimethoxysilane (KBM-403 produced by Shinetsu, Co., Ltd.) was diluted in propylene glycol monomethyl ether acetate. The solution was kept at 50°C, and 10 mol of N-methallylamine (Aldrich) was added slowly to allow the reaction to proceed. After the obtained solution was subjected to column separation, the solvent was removed by using vacuum distillation to obtain a compound represented by the following formula 5:
[0106] [Formula 5]
[0107]
[0108] pass 1 H-NMR confirmed structure: 5.17, 5.15, 5.83 (-CH=CH 2 ),2.27(CH 3 ), 2.0(-OH), 3.55(-OCH 3 )
Embodiment 2
[0110]Except that 3-glycidyloxypropyltriethoxysilane (KBE-403 produced by Shinetsu, Co., Ltd.) was used instead of 3-glycidyloxypropyltrimethoxy in Synthesis Example 1 Synthesis Example 2 was the same as Synthesis Example 1 except for silane (KBM-403 produced by Shinetsu, Co., Ltd.). Thus, a compound represented by the following formula 6 was obtained:
[0111] [Formula 6]
[0112]
[0113] pass 1 H-NMR confirmed structure: 5.17, 5.15, 5.83 (-CH=CH 2 ),2.27(CH 3 ),2.0(-OH),1.22,3.83(-OCH 2 CH 3 )
Embodiment 3
[0115] Synthesis Example 3 was the same as Synthesis Example 1 except that N-ethylallylamine (Aldrich) was used instead of N-methallylamine (Aldrich) in Synthesis Example 1. Thus, a compound represented by the following formula 7 was obtained:
[0116] [Formula 7]
[0117]
[0118] pass 1 H-NMR confirmed structure: 5.17, 5.15, 5.83 (-CH=CH 2 ),2.40,2.62(-CH 2 CH 3 ), 2.0(-OH), 3.55(-OCH 3 )
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