A kind of preparation method of low alkaloid burley tobacco extract
A technology of burley tobacco and alkaloids, applied in the fields of tobacco, tobacco processing, food science, etc., can solve the problems of inapplicable low yield of macroporous adsorption resin columns, unrealistic treatment, and no practical application in production, so as to avoid low yield , The method is simple, the effect of total alkaloid reduction
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Embodiment 1
[0018] Embodiment 1, a kind of preparation method of low alkaloid burley tobacco extract is characterized in that concrete steps are as follows:
[0019] (1) Take 1 kg of Burley tobacco, add 5 times the volume of water and heat and reflux twice, each time for 2 hours, to obtain the crude extract of Burley tobacco water;
[0020] (2) the crude extract of Burley tobacco in the step (1) is filtered with gauze to remove the impurities of large particles, and then the filtrate after the coarse filtration is filtered again with a filter membrane of 0.8 microns to obtain the crude extract of Burley tobacco;
[0021] (3) Select the MS-5 special macroporous adsorption resin for alkaloid extraction produced by Xingtai Minsheng Resin Technology Co., Ltd. as the macroporous resin, and activate it. The treatment process is as follows: soaking in water three times, each soaking 8-12 Take it out and soak it twice with 25% ethanol for 8-12 hours each time; take out the soaked macroporous resi...
Embodiment 2
[0024] Embodiment 2, a kind of preparation method of low alkaloid burley tobacco extract is characterized in that concrete steps are as follows:
[0025] (1) Get 1 kg of Burley tobacco, add 8 times the volume of water and heat and reflux twice, each for 3 hours, to obtain the crude extract of Burley tobacco;
[0026] (2) the crude extract of Burley tobacco in the step (1) is filtered with gauze to remove the impurities of large particles, and then the filtrate after the coarse filtration is filtered again with a filter membrane of 0.8 microns to obtain the crude extract of Burley tobacco;
[0027] (3) DLB-006 special macroporous adsorption resin for alkaloid extraction produced by Zhaoqing Jinghua Resin Chemical Co., Ltd. was selected as the macroporous resin and activated. The treatment process was as follows: soaking in water three times, each soaking 8 -12 hours; take it out and soak it twice with 30% ethanol, 8-12 hours each time; then take out the soaked macroporous resin...
Embodiment 3
[0030] Embodiment 3, a kind of preparation method of low alkaloid burley tobacco extract is characterized in that concrete steps are as follows:
[0031] (1) Take 1 kg of Burley tobacco, add 10 times the volume of water and heat and reflux twice, each time for 4 hours, to obtain the crude extract of Burley tobacco water;
[0032] (2) the crude extract of Burley tobacco in the step (1) is filtered with gauze to remove the impurities of large particles, and then the filtrate after the coarse filtration is filtered again with a filter membrane of 0.8 microns to obtain the crude extract of Burley tobacco;
[0033](3) select the DM-5 alkaloid extraction special-purpose macroporous adsorption resin produced by Nankai University Chemical Factory as the processing macroporous resin, and carry out activation treatment to it, and the treatment process is as follows: soak in water three times, each time for 8-12 hours; Take it out and soak it twice with 50% ethanol for 8-12 hours each ti...
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