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A kind of preparation method of low alkaloid burley tobacco extract

A technology of burley tobacco and alkaloids, applied in the fields of tobacco, tobacco processing, food science, etc., can solve the problems of inapplicable low yield of macroporous adsorption resin columns, unrealistic treatment, and no practical application in production, so as to avoid low yield , The method is simple, the effect of total alkaloid reduction

Active Publication Date: 2018-02-02
HUBEI CHINA TOBACCO IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, it is unrealistic to process large quantities of extracts, especially in the application of Burley tobacco extracts in cigarettes, and the single batch to be processed can reach hundreds of kilograms or even tons of weight; moreover, from an economic point of view Look, the low output of macroporous adsorption resin column is also not applicable to Burley tobacco extract. Therefore, the purification of macroporous adsorption resin technology is only carried out in the laboratory research stage, but not actually applied in production.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0018] Embodiment 1, a kind of preparation method of low alkaloid burley tobacco extract is characterized in that concrete steps are as follows:

[0019] (1) Take 1 kg of Burley tobacco, add 5 times the volume of water and heat and reflux twice, each time for 2 hours, to obtain the crude extract of Burley tobacco water;

[0020] (2) the crude extract of Burley tobacco in the step (1) is filtered with gauze to remove the impurities of large particles, and then the filtrate after the coarse filtration is filtered again with a filter membrane of 0.8 microns to obtain the crude extract of Burley tobacco;

[0021] (3) Select the MS-5 special macroporous adsorption resin for alkaloid extraction produced by Xingtai Minsheng Resin Technology Co., Ltd. as the macroporous resin, and activate it. The treatment process is as follows: soaking in water three times, each soaking 8-12 Take it out and soak it twice with 25% ethanol for 8-12 hours each time; take out the soaked macroporous resi...

Embodiment 2

[0024] Embodiment 2, a kind of preparation method of low alkaloid burley tobacco extract is characterized in that concrete steps are as follows:

[0025] (1) Get 1 kg of Burley tobacco, add 8 times the volume of water and heat and reflux twice, each for 3 hours, to obtain the crude extract of Burley tobacco;

[0026] (2) the crude extract of Burley tobacco in the step (1) is filtered with gauze to remove the impurities of large particles, and then the filtrate after the coarse filtration is filtered again with a filter membrane of 0.8 microns to obtain the crude extract of Burley tobacco;

[0027] (3) DLB-006 special macroporous adsorption resin for alkaloid extraction produced by Zhaoqing Jinghua Resin Chemical Co., Ltd. was selected as the macroporous resin and activated. The treatment process was as follows: soaking in water three times, each soaking 8 -12 hours; take it out and soak it twice with 30% ethanol, 8-12 hours each time; then take out the soaked macroporous resin...

Embodiment 3

[0030] Embodiment 3, a kind of preparation method of low alkaloid burley tobacco extract is characterized in that concrete steps are as follows:

[0031] (1) Take 1 kg of Burley tobacco, add 10 times the volume of water and heat and reflux twice, each time for 4 hours, to obtain the crude extract of Burley tobacco water;

[0032] (2) the crude extract of Burley tobacco in the step (1) is filtered with gauze to remove the impurities of large particles, and then the filtrate after the coarse filtration is filtered again with a filter membrane of 0.8 microns to obtain the crude extract of Burley tobacco;

[0033](3) select the DM-5 alkaloid extraction special-purpose macroporous adsorption resin produced by Nankai University Chemical Factory as the processing macroporous resin, and carry out activation treatment to it, and the treatment process is as follows: soak in water three times, each time for 8-12 hours; Take it out and soak it twice with 50% ethanol for 8-12 hours each ti...

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Abstract

The invention provides a preparation method of low-alkaloid burley tobacco extract. According to the low-alkaloid burley tobacco extract, burley tobacco is taken and added into water of 5-10 times volume to be heated till boiling backflow is carried out two times, and burley tobacco crude extract is extracted and obtained; large-particle impurities are filtered away through gauze; then after filter liquor obtained after rough filtering is filtered again through a filtering film, the filter liquor and activated macroporous resin particles special for alkaloid extraction are mixed according to the mass ratio of (5-10):1, and stirring is carried out for 30 min to 60 min at the speed ranging from 20 turns / min to 40 turns / min; and then after gauze is adopted for filtering, a filtering film is used for filtering, concentration is carried out, and the low-alkaloid burley tobacco extract is obtained. According to the preparation method, the adsorption character of macroporous resin is utilized for reducing the content of alkaloid in the burley tobacco crude extract, and safe, low-alkaloid and high-quality tobacco flavor can be obtained.

Description

technical field [0001] The invention belongs to tobacco extracts, in particular to a method for preparing low-alkaloid burley tobacco extracts by using macroporous resin adsorption technology. technical background [0002] Burley is one type of tobacco. It belongs to the genus Nicotiana of the Solanaceae family and is a type of N. tabac-un. Because the stems and veins of Burley tobacco are milky white, it is more accurate to call it White Burley tobacco (White Burley). In the 1950s, my country began to introduce trial planting, and in the 1980s and 1990s, Hubei, Chongqing and other places had large-scale planting. However, compared with the quality of imported tobacco, domestic burley tobacco still has a large gap in sensory quality. In terms of chemical composition, the alkaloid content of domestic burley tobacco is much higher than that of imported burley tobacco, which has reached more than 6%, which is more than twice that of imported burley tobacco. Among them, the a...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): A24B15/24
CPCA24B15/24
Inventor 司辉陈一王娜谢豪李超程炳发
Owner HUBEI CHINA TOBACCO IND
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