The application relates to the technical field of atomic
gas chamber manufacturing, in particular to a vacuum heating reduction preparation
system of
alkali metal elements. The vacuum heating reduction preparation
system of
alkali metal elements comprises a reaction container, a glass vacuum device, a first heating piece, a second heating piece and a
temperature control device. The glass vacuum device comprises a glass
diffusion pump and a mechanical pump, one side of the glass
diffusion pump is connected with the reaction container, and the other side is connected with the mechanical pump. The first heating piece is used for heating the
mixed materials in the reaction container, and the second heating piece is used for baking and degassing the reaction container. The
temperature control device is electrically connected with the first heating piece and the second heating piece. The glass
diffusion pump is used as a main pump, which is beneficial to removing the gas in the
system before the reaction and the gas generated during the reduction reaction, improves the ultimate vacuum degree of the system, and obviously enhances the
alkali metal vapor
corrosion resistance of the glass vacuum device compared with the
metal vacuum device. After long-term use, the vacuum degree of the system is reduced little, and the high-purity alkali
metal elements meeting the vacuum filling of the
atomic clock atomic
gas chamber can be stably prepared.