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63results about How to "Reduce process parameters" patented technology

High-Al13 aluminium trichloride polymer crystal and its prepn

The present invention relates to high-Al13 aluminum chloride polymer crystal and its preparation process. The preparation process includes the reaction of metal with hydrochloric acid or aluminum chloride solution, or the reaction of aluminum hydroxide or aluminum oxide with aluminum chloride solution, or electrolysis, electrodialysis, anionic resin exchange or distillation of aluminum chloride solution; filtering at 20-100 deg.c to eliminate residue, freeze or evaporating crystallization, solid-liquid separation, and stoving at 40-90 deg.c to obtain the high-Al13 aluminum chloride polymer crystal. The produced high-Al13 aluminum chloride polymer crystal has basicity higher than 61 %, alumina content higher than 33 %, water insolubles less than 0.3 %, key flocculating component Al13 over 90 % and thus excellent flocculating effect.
Owner:INNER MONGOLIA UNIVERSITY

Positively charged polyvinyl chloride hollow fiber nanofiltration membrane and preparation method thereof

The invention discloses a method for preparing a positively charged polyvinyl chloride (PVC) hollow fiber nanofiltration membrane. The positively charged PVC hollow fiber nanofiltration membrane has a two-layer structure consisting of a positively charged compact skin layer and an electrically neutral porous support layer; the pore diameter of micropores of the compact skin layer is 1-5nm, and the pore diameter of micropores of the porous support layer is 10-100nm; and the outer diameter of the membrane is 1.5-3.0mm, and the inner diameter of the membrane is 0.5-2mm, wherein the positively charged compact skin layer comprises main components of polyvinyl chloride and cationic copolymer; and the electrically neutral porous support layer comprises main components of polyvinyl chloride and an inorganic filler. The method for preparing the positively charged PVC hollow fiber nanofiltration membrane comprises the following steps of: co-extruding positively charged compact skin layer membrane preparing liquid and electrically neutral porous support layer membrane preparing liquid in a two-layer ring shape; and curing and forming hollow fibers by using a dry-wet spinning process. The prepared hollow fiber nanofiltration membrane has the advantages of easily controlled interception property, high strength, simple preparation process and the like, and is a high-performance, low-cost and long-life nanofiltration membrane material for water treatment.
Owner:HAINAN LITREE PURIFYING TECH CO LTD

Polyester flat microporous membrane and preparation method thereof

InactiveCN101985085AAchieve hydrophilicAchieve hydrophilizationSemi-permeable membranesCell seperators/membranes/diaphragms/spacersPolyesterMicrometer
The invention discloses a polyester flat microporous membrane and a preparation method thereof. The microporous membrane comprises the following materials in percentage by mass: 60-99.9% of polyester and 0.1-40% of modifier; or 20-40% of non-woven fabric, 60-79.9% of polyester and 0.1-30% of modifier. The preparation method is realized on the basis of a thermally induced phase separation process and comprises the following steps: mixing the polyester, the modifier and diluter into a homogeneous solution at high temperature; scraping the homogeneous solution into a liquid membrane, cooling andcuring into a membrane so as to form a precursor membrane subject to microphase separation, and extracting to obtain a flat microporous membrane. The prepared polyester flat microporous membrane is in a spongeous structure with the pore diameter of 0.05-5.0 micrometers and the porosity of 30-80%, and has the advantages of narrow pore diameter distribution, uniform pore size, easily controlled pore size, high strength, symmetrical structure and the like, thereby being a filter membrane material for water treatment and a lithium ion battery diaphragm material with high performance, low cost andlong life.
Owner:ZHEJIANG UNIV

Diene/ether copolymer-based lithium ion gel electrolyte membrane and preparation method thereof

InactiveCN102074735AEffective mass transfer quantityImprove performanceSecondary cellsCross-linkPolyethylene oxide
The invention discloses a diene / ether copolymer-based lithium ion gel electrolyte membrane and a preparation method thereof. The lithium ion electrolyte membrane provided by the invention consists of cross-linked diene / ether copolymer, lithium salt and plasticizing agent, and the preparation method of the lithium ion electrolyte membrane comprises the following steps of: firstly, adopting a blocktype diene / polyether copolymer containing a poly-butadiene or polyprene chain segment and a polyethylene oxide or polypropylene oxide chain segment to form a membrane with the assistance of a solvent; secondly, performing crosslinking to form a gel membrane under the action of ultraviolet, heating or an initiating agent; and finally, swelling and activating the gel membrane by using a plasticizing agent and lithium salt solution to obtain the lithium ion gel electrolyte membrane. The prepared lithium ion gel electrolyte membrane has a two-phase micro-phase separation structure of polyolefin and polyether, wherein a diene polymer chain segment forms a cross-linked structure to improve the strength of the membrane, and a polyether phase absorbed plasticizing agent and the lithium salt provide a lithium ion transmission channel. The electrolyte membrane provided by the invention has the characteristic of high electrical conductivity and can be strengthened by using a non-woven cloth and the like, so the electrolyte membrane is suitable to be used as an electrolyte membrane material of power lithium ion batteries.
Owner:ZHEJIANG UNIV

Method for preparing electrochemical anodic oxidation of large pipe diameter TiO2 nanometer tube

The invention discloses an electrochemical anode oxidizing method for preparing a TiO2 nanotube with large caliber, which takes preprocessed pure titanium as an anode of the electrochemical anode oxidizing reaction and a pot lead as a counter electrode. In a hydrofluoric acid and water system, phosphoric acid is added as an activating agent, the concentration of the hydrofluoric acid is 0.15 mol per liter, and the concentration of the phosphoric acid is 0.5 to 4 mol per liter; oxidation is implemented twice under the conditions with voltage of 15 to 20 V and 23 to 28 V respectively, thus obtaining a TiO2 nanotube array with large caliber surface. Without destroying the permutation and the formation of the TiO2 nanotube, the electrochemical anode oxidizing method for preparing the TiO2 nanotube with large caliber can enlarge the caliber of the TiO2 nanotube to 280 nm, and has simple and convenient operations as well as low cost.
Owner:SOUTHWEST JIAOTONG UNIV

Surface treatment method for improvement of wear-resistance of titanium or titanium alloy

The surface treatment method comprises: putting the cleaned and dried Ti or Ti alloy into thermal treatment furnace or tube furnace, leading oxygen; or putting itno quartz tube furnace, leading water vapor; heating to 500-800Deg with constant speed as 5-20Deg / s, holding for 20-60min; cooling to room temperature together. This invention changes no the material original mechanical performance, improves its wear-resistance, reduces friction factor with low cost.
Owner:SOUTHWEST JIAOTONG UNIV

Preparation method of high-temperature smoke filter ceramic material with high thermal shock resistance

The invention discloses a preparation method of a high-temperature smoke filter ceramic material with high thermal shock resistance, wherein the method takes beta-cordierite, potash feldspar, spodumene and kaolin as raw materials, takes mullite as additive and takes carbon powder, starch, silicon carbide powder, limestone, sawdust, coal slag and ceramic waste as hole-forming agent; the high-temperature smoke filter ceramic material with high porosity, high thermal shock resistance, high compression strength, excellent filter performance and controllable aperture can be prepared by ball grinding, molding and sintering processes. The source of the pore-forming agent is wide; the die pressing, cold isostatic pressing and casting molding can be adopted, so that the operation is convenient andthe production cost is low; the filter ceramic material has controllable aperture and porosity, and excellent high temperature resistance and thermal shock resistance. The technology provided by the invention solves dust filter problem of high-temperature and wet gas well and also is applied in kinds of fields such as separation and purification, sound absorption, catalyst carrier and the like.
Owner:SOUTH CHINA UNIV OF TECH

Preparation method for (para, para)-diisopropylphenyl diphenylamine product

The invention belong to the technical field of organic compound synthesis and provides a preparation method for a (para, para)-diisopropylphenyl diphenylamine product. The method includes the steps of: (A) in the presence of a montmorillonite-type supported catalyst and under the protection of nitrogen gas, mixing a polymerization inhibitor with [alpha]-olefin and diphenylamine to perform an alkylation reaction at 75-175 DEG C for 4-16 h; and (B) reducing the temperature to 45-140 DEG C, and adding an organic cosolvent and a stabilizer with stirring, and filtering the reaction liquid while hot, and performing stepwise crystallization and purification, wherein a mother liquid can be recycled. The (para, para)-diisopropylphenyl diphenylamine crystal product has stable performance and high base number, is free of the problems such as yellowing, performance reduction and the like even after long-time storage, has uniform granular size and is less than 0.2% in residual diphenylamine content. In the production process, the olefin and the catalyst can be recycled and no waste water and waste gas emission exists, so that the process is environment-friendly. The product can be widely applied in various elastomers, foam plastics and lubricant oil for achieving the effects of resisting oxidization and aging.
Owner:PETROCHINA CO LTD

Injection molding technique of microporous foamed PP (polypropylene) plastic product

The invention discloses an injection molding technique of a microporous foamed PP (polypropylene) plastic product, which comprises the following steps: preparing a PP composite material, preparing a PP foaming master batch, feeding, melting, foaming, injecting, cooling and opening the mold. By controlling the formula, injection-molding pressure and temperature, mold temperature and other key parameters in the microporous injection molding process, the invention can lower the density of the molded PP plastic product by up to 15%, and achieves the effects of light weight and production cost saving. The microporous foamed PP has uniform pore size; and the molded PP plastic product has favorable tensile strength, bending strength and impact strength.
Owner:HEFEI HUIBANG POLYMER MATERIAL CO LTD

Sliding table mechanism utilizing hydraulic cylinder and gear to realize double-speed movement

The invention discloses a sliding table mechanism utilizing a hydraulic cylinder and a gear to realize double-speed movement. The sliding table mechanism comprises a controller, a sliding table body and a sliding table mechanism, wherein the sliding table mechanism comprises a sliding table seat, a linear guide rail, a driving gear, a driving oil cylinder, a sliding table body rack and a sliding table seat rack; the controller is arranged on the sliding table seat and used for controlling the driving oil cylinder to drive the driving gear to act; the linear guide rail is arranged on the sliding table seat; the sliding table body is arranged on the linear guide rail, and the sliding table body rack is arranged on the sliding table body; the sliding table seat rack is arranged on the sliding table seat; and the driving gear is simultaneously meshed with the sliding table body rack and the sliding table seat rack. The sliding table mechanism has the following beneficial effects that the structure is relatively simpler and is convenient to machine and mount, the manufacture cost is low, and the sliding table mechanism adopting the high-precision linear guide rail is high in transmission precision; and the sliding table mechanism having the advantages of large output force, high speed, stable running, high adapting capability, strong expanding capability and high performance-cost ratio is highly competitive on the market.
Owner:LUOYANG LIWEI TECH

Preparation method of copper-based composite material

The invention relates to a method for preparing a copper-based composite material. The method uses copper powder and zirconium carbide powder as raw materials, adopts a ball mill to perform ball milling on the raw materials, and the ball milling medium is zirconium carbide balls. Pure argon and sealed. After ball milling, put the mixed powder into a graphite mold and sinter in a vacuum hot-press furnace, keeping constant temperature and applying pressure at the highest sintering temperature. After sintering, the pressure is released, and the furnace is cooled to room temperature, and the prepared material is the copper-based composite material of the present invention. The method of the invention is simple, and the prepared copper-based composite material has excellent wear resistance and easy processing performance, and is suitable for making parts in working conditions subject to impact and easy to wear.
Owner:渭南高新区火炬科技发展有限责任公司

Thermal treatment method for improving hardness of TC21 two-phase titanium alloy

The invention discloses a thermal treatment method for improving hardness of a TC21 two-phase titanium alloy and belongs to the technical field of titanium alloy thermal treatment. According to the method, by carrying out heating, heat preservation and water quenching on the TC21 two-phase titanium alloy subjected to beta forging above the phase transformation point, a whole rhombic martensitic structure is obtained, a nanoscale twin crystal alpha-phase structure is obtained by carrying out tempering treatment on the rhombic martensitic structure at 500-550 DEG C, and compared with a forging structure, the hardness of the TC21 titanium alloy is remarkably improved through the nanoscale twin crystal alpha-phase structure. As the TC21 titanium alloy has good hardenability, the whole rhombicmartensitic structure can be easily obtained. The method provided by the invention is small in number of technical parameters, high in feasibility, easy to implement, stable in performance and beneficial for industrial production of TC21.
Owner:ANHUI UNIVERSITY OF TECHNOLOGY

Breathable comfortable moisture-absorption, sweat-releasing and cooling fabric and preparation method thereof

The invention provides a preparation method of a breathable comfortable moisture-absorption, sweat-releasing and cooling fabric, wherein the preparation method comprises the following steps: carrying out activation treatment of a cotton fiber through an alkali liquid, and finishing by nano chitosan, to obtain a nano material-modified cotton fiber; modifying a superfine polyester fiber by low temperature plasma, to obtain a surface-modified superfine polyester fiber; spooling, beam-warping and sizing the nano material-modified cotton fiber, the surface-modified superfine polyester fiber and a natural bamboo fiber respectively, in an air-jet loom, respectively forming an upper layer having a twill weave with three warp yarns up and one weft yarn down as a fabric structure, forming a middle layer having a plain as a fabric structure, forming a lower layer having a twill weave with two warp yarns up and one weft yarn down as a fabric structure, taking the nano material-modified cotton fiber as a connecting line, and compositing the upper surface layer, the middle layer and the lower surface layer to form a gray fabric; and carrying out dyeing, water washing and heat setting of the gray fabric to obtain the breathable comfortable moisture-absorption, sweat-releasing and cooling fabric.
Owner:福建南平市依尔婴服饰有限公司

Hollow polyester fiber microporous membrane and preparation method thereof

The invention relates to a preparation method of a hollow polyester fiber microporous membrane, which belongs to the technical field of membrane separation. The preparation method comprises the following steps of: mixing a polyester and a diluent to form mixed liquid; performing melt blending, standing and degassing to obtain a membrane-making liquid melt; extruding the diluent serving as core liquid and the membrane-making liquid melt by using a spinning jet to prepare a hollow fiber liquid membrane; after the liquid membrane passes through an air gap, solidifying the liquid membrane in a cold bath, and performing hollow molding to prepare a hollow fiber membrane precursor; soaking the hollow fiber membrane precursor into an extractant and drying to prepare the hollow polyester fiber microporous membrane. In the hollow polyester fiber microporous membrane, the porosity is 45 to 80 percent and the average aperture is 0.05 to 5.0 mu m. The hollow polyester fiber microporous membrane has the characteristics of simple preparation process, easily-controlled membrane structure, high flux and porosity, high mechanical strength and the like, and is a high-performance and low-cost filtering membrane material for water treatment.
Owner:JIANGNAN UNIV

Method for preparing CoSb3 nanometer particle film

The invention relates to a CoSb3 thermoelectric material, in particular to a method for preparing a CoSb3 nanometer particle film. The method comprises the following steps of: firstly, weighing CoC12.6H2O powder and Sb powder according to the molar ratio of 1:3; respectively filling the powder into respective crucible; putting the crucibles and glass slide substrates into a quartz pipe; placing the quartz pipe into a horizontal pipe type furnace; vacuumizing and aerating mixed air of 95 percent of argon and 5 percent of hydrogen for multiple times and removing oxygen in the quartz pipe; raising the temperature of the tubular pipe; performing chemical vapor deposition on the glass slide substrates in a low-pressure state to acquire the CoSb3 nanometer particle film; and testing Seebeck coefficient, conductivity and heat conductivity of the CoSb3 nanometer particle film and calculating a zone time (ZT) value of the CoSb3 nanometer particle film. According to the invention, the CoSb3 nanometer particle film is synthesized by one step, the process is simple, and the diameter of the prepared CoSb3 nanometer particle is between 200 and 400nm; and moreover, the CoSb3 thermoelectric material has good conductivity and low heat conductivity, can be directly used for thermoelectricity researches, and is used for novel high-efficiency thermoelectric conversion devices.
Owner:CHANGZHOU UNIV

Polyisoprene articles and process for making the same

The invention disclosed herein relates to an improved process for making elastomeric polyisoprene articles. In particular, the process of the invention is a system which produces synthetic polyisoprene articles exhibiting tensile strength properties similar to that of solvent-based processes using natural rubber latex. The process comprises an accelerator composition at the pre-cure stage comprising a dithiocarbamate, a thiazole and a guanidine compound. In a preferred embodiment, the accelerator composition comprises zinc diethyldithiocarbamate (ZDEC), zinc 2-mercaptobenzothiazole (ZMBT) and diphenyl guanidine (DPG), in conjunction with a stabilizer, such as sodium caseinate. The invention also includes an elastomeric polyisoprene product made by the process, such as a surgeon's glove.
Owner:ALLEGIANCE CORP

Process for preparing cobaltosic oxide powder by solid-phase catalytic oxidation of cobaltous chloride

Disclosed is a process for preparing cobaltosic oxide powder through cobalt chloride solid phase catalytic oxidation, which comprises mixing cobalt chloride with catalyst proportionally, drying, disintegrating and sintering, the advantages of the process include shorter process flow, higher controllability of the processing parameters, better consistency and narrower dimension distribution.
Owner:NINGBO RONBAY LITHIUM BATTERY MATERIAL CO LTD +1

Combined sliding table driven by hydraulic cylinders and gears

The invention discloses a combined sliding table driven by hydraulic cylinders and gears. The combined sliding table comprises a controller, a sliding table body, a first sliding table mechanism, a second sliding table mechanism,..., and an Nth sliding table mechanism, wherein N is the total number of the sliding table mechanisms and is larger than or equal to three. Each sliding table mechanism comprises a drive gear, a sliding table base, a linear guide rail, a drive oil cylinder, a sliding table body rack, a sliding table base rack and a sliding table body position induction device. The sliding table bases of the sliding table mechanisms are combined together in an end butt joint manner and jointly use one sliding table body. The linear guide rails are connected. Rotation shafts are arranged in the middles of the drive gears and fixed to power output ends. The sliding table base racks are parallel to telescopic oil cylinders. Each sliding table body rack and the sliding table base rack of the adjacent sliding table mechanism can be partially crossed left and right. Due to the gear and double-rack transmission form, double amplification of the stroke and the speed of the drive oil cylinders can be achieved, conversion of drive force of two sliding bases to the sliding table body is achieved through the butt joint function, and accordingly, the cross-region operation of the sliding table body is achieved.
Owner:LUOYANG LIWEI TECH

High temperature metal boat and method of plating tin doped indium oxide transparent condutive membrane

A high-temp motel evaporator with two fins (45+ / -2)X(10+ / -3)X (24+ / -3) mm is made of the tantalum plate and annealed at 900-1200 deg.C. A method for evaporating the transparent film of Sn-doped indium oxide features that its current for evaporating is 150-200 A, the aerated oxygen is 12+ / -2 seem, its vacuum level is (0.9-1)X10 to the power -2 Pa, and its baking temp for bottom is 280+ / -20 deg.C.
Owner:SHANGHAI INST OF OPTICS & FINE MECHANICS CHINESE ACAD OF SCI

Method for preparing copper-based composite material

The invention relates to a method for preparing a copper-based composite material. Copper powder and zirconium carbide powder are used as raw materials, and ball-milled by using a ball mill, the ballgrinding medium is a zirconium carbide ball, and a high-purity argon gas is filled into a ball milling tank in the ball milling process and is sealed. After ball milling, the mixed powder is placed ina graphite mold and sintered in a vacuum hot-pressing furnace to keep constant temperature and apply pressure at the highest sintering temperature. After the sintering is finished, the pressure is released and the furnace is cooled to room temperature. The prepared material is the copper-based composite material provided by the invention. The method provided by the invention is simple, and the prepared copper-based composite material has an excellent wear resistance performance and easy processing performance, and is suitable for preparing components in the environment under impact and easy wearing conditions.
Owner:渭南高新区金石为开咨询有限公司

Positively charged polyvinyl chloride hollow fiber nanofiltration membrane and preparation method thereof

The invention discloses a method for preparing a positively charged polyvinyl chloride (PVC) hollow fiber nanofiltration membrane. The positively charged PVC hollow fiber nanofiltration membrane has a two-layer structure consisting of a positively charged compact skin layer and an electrically neutral porous support layer; the pore diameter of micropores of the compact skin layer is 1-5nm, and the pore diameter of micropores of the porous support layer is 10-100nm; and the outer diameter of the membrane is 1.5-3.0mm, and the inner diameter of the membrane is 0.5-2mm, wherein the positively charged compact skin layer comprises main components of polyvinyl chloride and cationic copolymer; and the electrically neutral porous support layer comprises main components of polyvinyl chloride and an inorganic filler. The method for preparing the positively charged PVC hollow fiber nanofiltration membrane comprises the following steps of: co-extruding positively charged compact skin layer membrane preparing liquid and electrically neutral porous support layer membrane preparing liquid in a two-layer ring shape; and curing and forming hollow fibers by using a dry-wet spinning process. The prepared hollow fiber nanofiltration membrane has the advantages of easily controlled interception property, high strength, simple preparation process and the like, and is a high-performance, low-cost and long-life nanofiltration membrane material for water treatment.
Owner:HAINAN LITREE PURIFYING TECH CO LTD

Continuous cyaniding device and technology thereof

The invention discloses a continuous cyaniding device and a technology thereof. The device is provided with a saturated water tank, a cyaniding reactor, a cyaniding stabilizer, a steam condenser, a process water receiving tank and a cyaniding vacuum buffering tank, wherein the saturated water tank is connected with the cyaniding reactor; the cyaniding reactor is connected with the cyaniding stabilizer; the bottom of the cyaniding reactor is connected with a cyaniding feeding mixer group; the top of the cyaniding stabilizer is connected with the process water receiving tank through the steam condenser; the bottom of the cyaniding stabilizer is connected with a circulating heater; the circulating heater is connected to the middle-upper part of the cyaniding stabilizer; the cyaniding vacuum buffering tank is connected with the steam condenser and the process water receiving tank. According to the continuous cyaniding device and the technology, a production process is continuously carriedout, the equipment utilization rate is high, the production capacity is great, energy sources can be saved, and automatic operation is easy to realize; technological parameters are stable, the qualityof a product is ensured relatively well, and wastes of the energy sources are avoided.
Owner:烟台国邦化工机械科技有限公司

Integrated double end electric arc spraying equipment and spraying method

The invention relates to a kind of arc spray device and spraying technology. A carrying wire plate is on the wire feeder of the device. Electric source for spraying connects to controlling box through size 1 controlling line and size 1 electric output cable. The controlling box connects to the double-spout spray gun through size 2 air-compressed tube. The wire feeder connects to the double-spout spray gun through electric cables and wire duct. Pressure of compressed air for spraying is 0.6Mpa to 0.8Mpa. The eclectic voltage for spraying is 20V to 35V .The electric current for spraying is 50A to 300A. The invention eliminates steps such as renewing painting material, adjusting technical parameter and so on .So it can save spraying time and raise working efficiency .The invention can be used to make mosaic laminating layers of different material and different performance, for example, thick base Ni3Al layer with thin mosaic WC layer .The invention has prominent advantages such as simple spray procedure, high spray efficiency, saving energy and resource and so on. The spraying method of this invention can be operated easily.
Owner:HARBIN INST OF TECH

Ion injection method of a bag-shaped injection region and manufacture method of MOS (Metal Oxide Semiconductor) transistor

The invention relates to an ion injection method of a bag-shaped injection region and a manufacture method of an MOS (Metal Oxide Semiconductor) transistor, wherein in the ion injection method for forming a bag-shaped injection region of an MOS transistor, the bag-shaped injection region is formed by twice multi-step rotations of ion injection, and the start angles of the twice multi-step rotations are different. Compared with the prior art, the invention can control the junction capacitance of the MOS transistor and ensure that the threshold voltage Vt of the manufactured MOS transistor is more smooth along with the change of Id, thereby being more beneficial to manufacturing MOS transistor in smaller sizes.
Owner:SEMICON MFG INT (SHANGHAI) CORP

Non-photosensitive polyimide passivation layer manufacturing method

The invention discloses a non-photosensitive polyimide passivation layer manufacturing method. The method comprises the following steps of providing a substrate; performing oxygen-filling plasma processing on the surface of the substrate; or growing a silicon dioxide layer or a silicon oxynitride layer on the surface of the substrate; spinning a layer of non-photosensitive polyimide onto the surface of the substrate; baking the non-photosensitive polyimide in two sections to soften the non-photosensitive polyimide; coating a photoresist and baking the photoresist to soften the photoresist; performing development; removing the photoresist by a photoresist stripping process; curing the non-photosensitive polyimide. The problem that the non-photosensitive polyimide is lifted can be solved, the production efficiency can be improved, and the danger that developing liquid corrodes metal during the development is reduced.
Owner:SHANGHAI HUAHONG GRACE SEMICON MFG CORP

Controllable preparation method of monocrystal copper nanowires

The invention relates to a preparation method of copper nanowires and in particular relates to a controllable preparation method of high-yield monocrystal copper nanowires in a liquid-phase reduction manner. The controllable preparation method comprises the steps: firstly, mixing a divalent metal copper salt solution and ethylenediamine, and heating in a water bath to form a single and stable copper ion chelate compound; mixing a strong base solution with hydrazine hydrate, and preparing a reducing agent in the water bath at the same temperature; then transferring the two mixture solutions into a reaction vessel, fully stirring to reach a uniform state, covering well, and placing in the water bath at the same temperature for heating reaction to prepare the copper nanowires; and fishing out flaky copper nanowires floating on the upper layer of the solution, washing the flaky copper nanowires with deionized water and absolute ethyl alcohol in sequence three times, and drying at room temperature under an Ar gas protection condition to prepare the copper nanowires. The controllable preparation method provided by the invention has the advantages of simple process, low cost and high yield, and the prepared copper nanowires are of monocrystal structures, and have relatively smooth surfaces, uniform radial thickness, and controllable and more uniform length and diameter.
Owner:CHANGZHOU UNIV

Lyophobic matrix sustained-release tablet for pH independence drugs and preparation method thereof

The invention discloses a lyophobic matrix sustained-release tablet for pH independence drugs and a preparation method thereof. The sustained-release tablet is prepared from the following raw materials: a main drug, a wax matrix material, a local pH regulating agent, an adhesive, a filler, a lubricating agent and a glidant, wherein the local pH regulating agent is selected from calcium hydrogen phosphate dihydrate, disodium hydrogen phosphate or calcium silicate. The preparation method of the lyophobic matrix sustained-release tablet comprises the following steps: heating and melting the wax matrix material; uniformly mixing the main drug, the local pH regulating agent, the adhesive and the filler; melting and pelletizing the matrix material and the uniformly mixed materials; screening when the mixture is hot, granulating the mixture, performing standing to cool the mixture, adding the lubricating agent and the glidant into the mixture, and performing tableting to obtain the lyophobicmatrix sustained-release tablets. According to the lyophobic matrix sustained-release tablet, the local pH regulating agent is added into the existing prescription of diclofenac sodium sustained-release tablets, the pH value of a micro-environment can be maintained to promote solubility of drugs, and release in vitro of pH independence drugs can be improved.
Owner:CHINA PHARM UNIV

Method for directly growing hemimorphite zinc silicate on glass substrate

The invention belongs to the technical field of inorganic synthesis, and particularly relates to a method for directly growing hemimorphite zinc silicate on a glass substrate. The method comprises the following steps that zinc chloride and hexadecyl trimethyl ammonium bromide are taken to be dissolved by distilled water separately and then mixed; ammonium hydroxide is added, stirring is conducted, and then suspension liquid is obtained; a clean glass slide is prepared to serve as a substrate and then put into the suspension liquid; the suspension liquid is put in an autoclave, and heat preservation is conducted; after heat preservation is finished, the glass slide is taken out; the glass slide is put into a sintering furnace to be sintered, and then hemimorphite zinc silicate can be obtained. According to the method, hemimorphite zinc silicate can be prepared by supplying silicon by the substrate without needing to add additional a silicone-containing compound raw material, simpleness and convenience are achieved, and operation and control are easy.
Owner:KUNMING UNIV OF SCI & TECH
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