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40results about How to "Uniform method" patented technology

Preparation method of spherical nickel hydroxide anode material coated with gamma-hydroxy cobalt oxide

The invention relates to a preparation method of a spherical nickel hydroxide anode material coated with gamma-hydroxy cobalt oxide, comprising the following steps: heating cobalt hydroxide coated spherical nickel hydroxide which is utilized as a precursor, and spraying an alkali metal hydroxide aqueous solution; evenly mixing the precursor with the alkali metal hydroxide aqueous solution; introducing oxygen to oxidize the cobalt hydroxide to convert the cobalt hydroxide into high-valency gamma-hydroxy cobalt oxide; and during oxidation, combining mechanical agitation and ultrasonic agitation to prevent the spherical nickel hydroxide anode material coated with gamma-hydroxy cobalt oxide from gathering and cause alkali metal ions to be embedded into a crystal lattice with the laminated structure of the gamma-hydroxy cobalt oxide. After oxidation reaction is over, a lithium hydroxide alkaline solution at certain temperature is added into an oxidation reaction pot to carry out heat preservation on the spherical nickel hydroxide anode material coated with gamma-hydroxy cobalt oxide; when heat preservation is carried out, mechanical agitation and ultrasonic agitation are adopted to cause the lithium ions to be embedded into the laminated structure of the gamma-hydroxy cobalt oxide; and the obtained spherical nickel hydroxide anode material coated with gamma-hydroxy cobalt oxide is screened by an ultrasonic sieve shaker after being washed and dried.
Owner:JIANGMEN CHANCSUN UMICORE IND

Ice slurry concentrating, equalizing, storing and dispatching tank device

The invention discloses an ice slurry concentrating, equalizing, storing and dispatching tank device, and discloses a high-concentration ice slurry concentrating, storing and dispatching tank device. The device comprises at least one ice slurry making machine and an ice concentrating, storing and dispatching tank, wherein an ice lifter, a damping grille and an ice slurry water inlet pipe are arranged in the dispatching tank; an inlet of the ice slurry water inlet pipe is formed in the bottom of a tank body of the dispatching tank; an ice discharge submerged pump is arranged in the damping grille; the ice lifter comprises a gear motor; the upper end of the rotating shaft is connected with the gear motor; the lower end of a rotating shaft is connected with an ice discharge device; an ice discharge opening is formed in the position of the tank body of the ice concentrating, storing and dispatching tank; a top ice outlet of the ice slurry making machine is communicated with the inlet of the ice slurry water inlet pipe through an ice slurry delivery pipeline; and a water outlet in the bottom of the dispatching tank is communicated with a bottom water return opening of the ice making machine through a circulating pipeline with an ice-making circulation pump and a flow meter. According to the ice slurry concentrating, equalizing, storing and dispatching tank device, efficient ice making of the ice slurry making machine is kept, and continuous ice making and ice storage are realized.
Owner:王飞波

Gradient nano-coating used for thermal barrier coating anti-corrosion function and preparation method thereof

InactiveCN103058654AOvercoming differences in thermal expansion coefficientsThe method is simple and easyTotal thicknessThermal barrier coating
The invention discloses a gradient nano-coating used for a thermal barrier coating anti-corrosion function and a preparation method thereof. A substrate is steeped and lifted in pure sol and mixed sol of yttria stabilization zirconia (YSZ) and Al 2O3. A gradient coating structure with proportion of the YSZ and the Al2O3 changed from inside to outside is obtained in a prepared mode. The gradient nano-coating is composed of particles with the particle diameter of 10 to 100nm. The total thickness of the coating is 0.5 to 5 micrometers. According to the novel gradient coating structure, the facts that anti-corrosion property of the Al2O3 is kept and meanwhile a phenomenon of coating exfoliation due to difference of thermal expansion coefficients between the YSZ and the Al2O3 materials is overcome are hopeful to be achieved, the gradient nano-coating structure is prepared through a mixed sol steeping and lifting method, and then high temperature roasting is conducted. A composition weight ratio of the YSZ to the Al2O3 in the mixed sol changes between 9 to 1 and 1 to 9. The particles contained by the YSZ sol are in a monoclinic crystal shape. Temperature of the high temperature roasting is 500 to 800 DEG C. The preparation method is simple and convenient to achieve, and practical. The coating prepared is even in structure.
Owner:SHANGHAI UNIV

Method for preparing chloramphenicol molecularly imprinted polymeric microspheres

The invention discloses a method for preparing chloramphenicol molecularly imprinted polymeric microspheres, and relates to a method for preparing polymeric microspheres. The method solves the problems that a molecularly imprinted polymer obtained by adopting a mass polymerization method has irregular particles and is easy to agglomerate. The method comprises the following steps of: 1, dissolving methacrylic acid and chloramphenicol into acetonitrile, adding ethylene glycol dimethacrylate and zaodiisobutyronitrile after the oscillation to obtain a mixture, performing ultrasonic treatment on the mixture, and then sealing the mixture after nitrogen aeration and oxygen removal; 2, performing heating polymerization on the sealed mixture for hours, cooling and centrifugating the mixture, and then naturally drying a precipitate; and 3, removing the chloramphenicol from the precipitate, washing the precipitate with methanol for 5h, and drying the precipitate to obtain the chloramphenicol molecularly imprinted polymeric microspheres. The chloramphenicol molecularly imprinted polymeric microspheres obtained by the method have regular particle shapes, uniform size, and no agglomeration phenomenon, and increase the specific surface area of the chloramphenicol molecularly imprinted polymeric microspheres, thereby improving the adsorptivity.
Owner:BEIJING PURKINJE GENERAL INSTR

Manufacturing method of screen printed plate of edge sealing frame of liquid-crystal display

The invention discloses a manufacturing method of a screen printed plate of an edge sealing frame of a liquid-crystal display, comprising the following steps: designing the patterns of the whole screen printed plate as rectangular patterns which are matched with a glass substrate to be processed; arranging a rectangular layout area for multiple patterns of the edge sealing frame on the middle parts of the rectangular patterns in a row and column form; and respectively arranging U-shaped auxiliary lines of which the opening face outwards on the two ends of the patterns of the edge sealing frame in each row and each column, wherein the U-shaped auxiliary lines are located between the outer edge of the rectangular layout area and the outer edges of the patterns of the whole screen printed plate, the whole width of each U-shaped auxiliary line is the same as the widths of the patterns of the edge sealing frames in corresponding rows or corresponding columns, and the widths of the lines of the U-shaped auxiliary line is the same as the widths of the lines of the patterns of the edge sealing frame. According to the method, the U-shaped auxiliary lines are arranged at the four sides of the layout area, the U-shaped auxiliary lines are similar to the local shapes of the patterns of the edge sealing frame, and the density of the U-shaped auxiliary lines is the same, so that the influence of the thickness uniformity of the boxes caused by edge effect is maximally eliminated, the rainbow problem caused by the influence is solved, and the quality of the product is improved.
Owner:HEBEI JIYA ELECTRONICS

Method for preparing chloramphenicol molecularly imprinted polymeric microspheres

The invention discloses a method for preparing chloramphenicol molecularly imprinted polymeric microspheres, and relates to a method for preparing polymeric microspheres. The method solves the problems that a molecularly imprinted polymer obtained by adopting a mass polymerization method has irregular particles and is easy to agglomerate. The method comprises the following steps of: 1, dissolvingmethacrylic acid and chloramphenicol into acetonitrile, adding ethylene glycol dimethacrylate and zaodiisobutyronitrile after the oscillation to obtain a mixture, performing ultrasonic treatment on the mixture, and then sealing the mixture after nitrogen aeration and oxygen removal; 2, performing heating polymerization on the sealed mixture for hours, cooling and centrifugating the mixture, and then naturally drying a precipitate; and 3, removing the chloramphenicol from the precipitate, washing the precipitate with methanol for 5h, and drying the precipitate to obtain the chloramphenicol molecularly imprinted polymeric microspheres. The chloramphenicol molecularly imprinted polymeric microspheres obtained by the method have regular particle shapes, uniform size, and no agglomeration phenomenon, and increase the specific surface area of the chloramphenicol molecularly imprinted polymeric microspheres, thereby improving the adsorptivity.
Owner:BEIJING PURKINJE GENERAL INSTR

Apparatus and method for uniformly mixing ice powder and sand or soil

The present invention provides an apparatus and a method for uniformly mixing ice powder and sand or soil. The apparatus comprises an adjustable-speed rotator, a stainless steel container, a filter screen, an atomizing nozzle, a vent hole, a protective cover, a constant flow pump, a water cup and a mass balance. The bottom of the stainless steel container body is connected with the adjustable-speed rotator through the card slot, and the filter screen is arranged in the upper groove of the stainless steel container body; the atomizing nozzle is arranged in the middle of the upper cover; the outer part of the atomizing nozzle is provided with a protective cover; and the atomizing nozzle is connected with the constant flow pump outlet, and the constant flow pump inlet is connected with a water cup on the mass balance through the pipeline. According to the apparatus provided by the present invention, micron-sized atomized water droplets are obtained through the atomizing nozzle; if liquidnitrogen is poured into the stainless steel container, the water droplets will fall into liquid nitrogen to become ice powder; and sand and soil within the desired particle size range can be obtainedby using the filter screen. According to the apparatus provided by the present invention, ice powder or atomized water droplets are prepared and sand or soil of a desired particle size is screened inthe rotating stainless steel container, and uniform mixing of ice powder or atomized water droplets with sand or soil is realized.
Owner:DALIAN UNIV OF TECH +1

Preparation method and application of three-dimensional polydopamine

The invention relates to a preparation method and application of three-dimensional polydopamine, and belongs to the technical field of functional materials. According to the preparation method, dopamine hydrochloride and metal iron salt are used as raw materials, and the three-dimensional polydopamine is prepared by utilizing a self-polymerization and self-assembly. The three-dimensional polydopamine prepared by the method has the advantages of simple method, adjustable size and morphology and the like, and the requirement of environmental protection is met by taking a common water / alcohol system as a reaction solvent. The preparation method of the three-dimensional polydopamine material provided by the invention can promote further development of related research of polydopamine. The three-dimensional polydopamine prepared by the method disclosed by the invention has an excellent photo-thermal conversion effect, and compared with traditional optical materials, the material shows excellent biocompatibility and photo-thermal conversion rate, and plays a role in promoting the research of a photo-thermal agent. The three-dimensional polydopamine material prepared by the method can beused for photothermal therapy of tumors, so that the three-dimensional polydopamine material has a good medical application prospect.
Owner:TSINGHUA UNIV

A kind of preparation method of wafer level vanadium dioxide thin film

The invention provides a preparation method of a wafer-level vanadium dioxide film. The preparation method comprises the following steps of S1, providing a metal vanadium film with uniform growth; andS2, under the condition that the temperature is 450-650 DEG C and oxygen-free, oxidizing the metal vanadium film by using water vapor to obtain a monoclinic phase vanadium dioxide film. The preparation method can be used for preparing the vanadium dioxide thin film with the excellent performance of the wafer level size, is uniform and compact, and can achieve the resistance change of three to four orders of magnitudes in the phase change process. According to the preparation method, the water vapor is used as a mild oxidizing agent, a self-adjusting oxidation mechanism can be realized in thegrowth process when the vanadium dioxide film is prepared, so that a stable positive tetravalent monoclinic phase vanadium dioxide film can be prepared. According to the preparation method, the growthtemperature zone prepared by the vanadium dioxide film is greatly expanded, and the vanadium dioxide film can be efficiently prepared within the range of 450-650 DEG C; and the method is simple and easy to implement and high in repeatability, and the whole film growth process is non-toxic, environment-friendly and low in cost.
Owner:UNIV OF SCI & TECH OF CHINA

A method for manufacturing a screen printing plate of a liquid crystal display sealing frame

The invention discloses a manufacturing method of a screen printed plate of an edge sealing frame of a liquid-crystal display, comprising the following steps: designing the patterns of the whole screen printed plate as rectangular patterns which are matched with a glass substrate to be processed; arranging a rectangular layout area for multiple patterns of the edge sealing frame on the middle parts of the rectangular patterns in a row and column form; and respectively arranging U-shaped auxiliary lines of which the opening face outwards on the two ends of the patterns of the edge sealing frame in each row and each column, wherein the U-shaped auxiliary lines are located between the outer edge of the rectangular layout area and the outer edges of the patterns of the whole screen printed plate, the whole width of each U-shaped auxiliary line is the same as the widths of the patterns of the edge sealing frames in corresponding rows or corresponding columns, and the widths of the lines of the U-shaped auxiliary line is the same as the widths of the lines of the patterns of the edge sealing frame. According to the method, the U-shaped auxiliary lines are arranged at the four sides of the layout area, the U-shaped auxiliary lines are similar to the local shapes of the patterns of the edge sealing frame, and the density of the U-shaped auxiliary lines is the same, so that the influence of the thickness uniformity of the boxes caused by edge effect is maximally eliminated, the rainbow problem caused by the influence is solved, and the quality of the product is improved.
Owner:HEBEI JIYA ELECTRONICS

Preparation method and application of Bi2Ti4O11:Yb, Er up-conversion luminescence anti-counterfeiting film

The invention discloses a preparation method and application of a Bi2Ti4O11:Yb, Er up-conversion luminescence anti-counterfeiting film. HAC, DMF and TBOT solutions are uniformly mixed, bismuth nitrate, ytterbium nitrate and erbium nitrate are sequentially added, after the bismuth nitrate, the ytterbium nitrate and the erbium nitrate are fully dissolved, a mixture is evaporated to dryness to obtain gray black powder, the powder is annealed, TPU, THF and DMF are dissolved to obtain a uniform transparent solution with viscosity, and Bi2Ti4O11:Yb, Er powder is added under a stirring condition and is fully dissolved to obtain an electrostatic spinning precursor solution. The precursor solution is transferred into an electrostatic field, an electrostatic spinning process is performed, and a spinning product is obtained on a collecting plate. The collecting plate is put into a drying oven to be dried. Finally, the film is white and transparent under a fluorescent lamp, and no light emitting phenomenon exists. However, under the excitation of a 980 nm laser, the film shows excellent up-conversion luminescence performance. By adjusting the doping proportion of the ytterbium nitrate and the erbium nitrate, the anti-counterfeiting film with red, yellow and green up-conversion luminescence properties can be obtained.
Owner:SHAANXI UNIV OF SCI & TECH

Picc venous catheter intelligent control operation instrument for chemotherapy of leukemia patients

The invention discloses a PICC (peripherally inserted central catheter) intelligent control operation instrument for chemotherapy on leukemia patients, and belongs to the technical field of medical apparatus and instruments. The PICC intelligent control operation instrument comprises a movable operation device, an automatic puncture device, a positioning and navigation device, a main control monitoring device and an auxiliary fixing device. The movable operation device comprises a base desk, a first mechanical arm, a second mechanical arm and a third mechanical arm, the automatic puncture device comprises a first electric telescopic rod, an angle controller, a puncture support plate, a cannula sheath clamp head, a needle clamp head and a catheter clamp head, the positioning and navigation device comprises a connector, a positioning and navigation mechanism, a second electric telescopic rod and an ultrasonic probe, the main control monitoring device comprises a hose, a display screen, a control desk, an ultrasonic generator, an electrocardiogram instrument and an EKG (electrocardiogram) positioning assembly, and the auxiliary fixing device comprises an automatic pulse pressure device, a base plate and a grip strength fixing mechanism. The PICC intelligent control operation instrument has the advantages of simplicity and convenience in use, speediness and high accuracy.
Owner:张建英
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