Nasal spray for treating apoplexy and preparation method thereof
A technology of nasal spray and musk, which is applied in the field of Chinese patent medicine, can solve the problems of unclear and difficult pathogenesis and treatment mechanism, and achieve the effects of avoiding the first-pass effect, fast drug absorption and strong effect
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example 1
[0103] Prescription: Musk 3g, Shichangpu 40g, Borneol 5g, Pig Tooth Soap 30g.
[0104] Preparation method:
[0105] 1. Extract the active ingredients in musk, calamus and pig tooth soap respectively:
[0106] Extraction of musk: take musk and add 10 times the concentration of 60% ethanol for ultrasonic extraction 3 times, each time for 5 minutes, filter, combine the filtrate, evaporate the ethanol, and set aside; add 10 times water to extract musk residue 2 times, each time 1 hour, filtered, and the filtrate was concentrated to 50ml for later use.
[0107] Extraction of Shichangpu: Take Shichangpu and add 6 times the amount of water to distill for 6 hours, and collect the volatile oil for later use.
[0108] Extraction of pig tooth soap: Take pig tooth soap and add 6 times the amount of 60% ethanol to reflux and extract 3 times, each time for 2 hours, filter, combine the filtrate, recover ethanol under reduced pressure and concentrate to a relative density of 1.15 (65°C) for...
example 2
[0112] Prescription: Musk 41g, Shichangpu 245g, Borneol 41g, Pig Tooth Soap 165g.
[0113] Preparation method:
[0114] 1. Extract the active ingredients in musk, calamus and pig tooth soap respectively:
[0115] Extraction of musk: take musk and add 6-10 times the amount of 60-95% ethanol to ultrasonically extract 3 times, each time for 5 minutes, filter, combine the filtrate, evaporate the ethanol, and set aside; add 6-10 times the amount of water to extract the musk residue 2 times, each time for 1 hour, filtered, and the filtrate was concentrated to 80ml for later use.
[0116] Extraction of Shichangpu: Take Shichangpu and add 6 times the amount of water to distill for 6 hours, and collect the volatile oil for later use.
[0117] Extraction of pig tooth soap: Take pig tooth soap and add 6 times the amount of 60% ethanol to reflux and extract 3 times, each time for 2 hours, filter, combine the filtrate, recover ethanol under reduced pressure and concentrate to a relative ...
example 3
[0121] Prescription: Musk 30g, Shichangpu 200g, Borneol 40g, Pig Tooth Soap 200g.
[0122] Preparation method:
[0123] 1. Extract the active ingredients in musk, calamus and pig tooth soap respectively:
[0124] Extraction of musk: take musk and add 8 times the concentration of 80% ethanol to ultrasonically extract 3 times, each time for 5 minutes, filter, combine the filtrate, evaporate the ethanol, and set aside; add 8 times water to the musk residue and extract 2 times, each time 1 hour, filtered, and the filtrate was concentrated to 70ml for later use.
[0125] Extraction of Shichangpu: Take Shichangpu and add 6 times the amount of water to distill for 6 hours, and collect the volatile oil for later use.
[0126] Extraction of pig tooth soap: take pig tooth soap and add 6 times concentration of 60% ethanol to reflux extraction for 3 times, each time for 2 hours, filter, combine filtrates, recover ethanol under reduced pressure and concentrate to a relative density of 1....
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