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Chromatographic peak end point adjusting method and chromatographic work station having chromatographic peak end point adjusting function

An adjustment method and workstation technology, applied in the field of chromatography, can solve the problem of inaccurate identification of the end point, and achieve the effect of accurate, fast and definite determination

Active Publication Date: 2015-06-24
达耐科学有限公司
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Problems solved by technology

[0006] The purpose of the present invention is to: solve the technical problem of inaccurate identification of the end point of the spectral peak by only using the method of slope threshold judgment in the prior art to identify the starting point and end point of the spectral peak, and provide a method for adjusting the end point of the spectral peak

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  • Chromatographic peak end point adjusting method and chromatographic work station having chromatographic peak end point adjusting function
  • Chromatographic peak end point adjusting method and chromatographic work station having chromatographic peak end point adjusting function
  • Chromatographic peak end point adjusting method and chromatographic work station having chromatographic peak end point adjusting function

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Embodiment Construction

[0038] The specific implementation manners of the present invention will be further described in detail below in conjunction with the accompanying drawings.

[0039] refer to Figure 4 , shows a method flowchart of an embodiment of a method for adjusting the end point of a spectral peak in the present invention, including the following steps:

[0040] Step S401, determining the middle point of the spectrum peak;

[0041] In this step, firstly, the middle point of the spectral peak is found by using the slope threshold judgment method in the prior art. In this embodiment, the middle point of the spectrum peak is selected as the apex of the spectrum peak.

[0042] As another example, the middle point of the spectral peak may also be an inflection point of the spectral peak or any point between the apex of the spectral peak and the inflection point of the spectral peak as the middle point.

[0043] As another example, the determination of the middle point of the spectral peak ...

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Abstract

The present invention discloses a chromatographic peak end point adjusting method and a chromatographic work station having the chromatographic peak end point adjusting function. The chromatographic peak end point adjusting method comprises: determining a chromatographic peak middle point; sequentially judging whether the slope value of the data point in the data group and behind the chromatographic peak middle point is subjected to symbol change, and adopting the last data point before the symbol change or the first data point after the symbol change as the chromatographic peak end point if the symbol change exists; if the symbol change does not exist, searching a first data group having the data point average slope absolute value of less than the preset slope threshold, and adopting any one data point in the group as a first data point; searching a second data group having the data point average slope absolute value of more than the preset slope threshold and positioned behind the first data group, and adopting any one data point in the group as a second data point; and searching all data points having the slope absolute value of less than the preset slope threshold and positioned between the first data point and the second data point, and determining the lowest data point as the chromatographic peak end point. According to the present invention, the chromatographic peak end point can be quickly and accurately determined.

Description

technical field [0001] The invention relates to the technical field of chromatography, in particular to a method for adjusting the end point of a spectrum peak and a chromatography workstation with the function of adjusting the end point of a spectrum peak. Background technique [0002] At present, all chromatographic devices in the industry are equipped with chromatographic workstations. The chromatographic workstation is equivalent to a host computer. On the one hand, it completes the control of the lower computer (that is, the chromatographic device), and on the other hand, it analyzes and processes the chromatographic data collected by the lower computer to achieve Quantitative analysis of the sample to be tested. Chromatographic devices include liquid chromatography, high performance liquid chromatography and ultra-high performance liquid chromatography. [0003] The quantitative analysis of the sample to be tested mainly depends on the peak area or peak height of the ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N30/86G01N35/00
Inventor 王灿王悦王铁军李维森
Owner 达耐科学有限公司
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