Method of nuclear magnetic resonant rock sample analyzer label sample recipe
A nuclear magnetic resonance and analyzer technology, which is applied in the preparation of nuclear magnetic resonance rock sample porosity standard samples and the field of standard sample formulations for nuclear magnetic resonance rock sample analyzers, can solve problems such as inability to achieve accurate quantitative corrections
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Embodiment 1
[0031] A method for the standard sample formulation of a nuclear magnetic resonance rock sample analyzer is:
[0032] Step 1: Dissolve 2 grams of copper sulfate in 500 grams of deionized water to form X solution, control the concentration of copper sulfate to 0.4%, and fully dissolve it for later use;
[0033] Step 2: Dissolve 2 grams of copper sulfate in 500 grams of heavy water to form Y liquid, control the concentration of copper sulfate to 0.4%, and fully dissolve it for later use;
[0034] Step 3: Using a digital titrator, take 0.015 ml of liquid X and 9.985 ml of liquid Y to keep the total volume at a constant value of 10 ml, and control the volume ratio of liquid X to the sum of liquid X and liquid Y between 0.05% and 50%. , fully mixed to become 1% standard sample;
[0035] Take 0.15 ml of liquid X and 9.85 ml of liquid Y to keep the total volume at a constant value of 10 ml. The volume ratio of liquid X and liquid Y is 1.5%, and they are fully mixed to form a 10% sta...
Embodiment 2
[0037] Step 1: Dissolve 3 grams of chromium acetylacetonate in 500 grams of isooctane to form X liquid, control the concentration of chromium acetylacetonate to 0.6%, and fully dissolve it for later use;
[0038] Step 2: Dissolving 3 grams of chromium acetylacetonate in 500 grams of tetrabromomethane to form Y solution, controlling the concentration of chromium acetylacetonate to be 0.6%, and fully dissolving it for later use;
[0039] Step 3: Using a digital titrator, take 0.015 ml of liquid X and 9.985 ml of liquid Y to keep the total volume at a constant value of 10 ml, and control the volume ratio of liquid X to the sum of liquid X and liquid Y between 0.05% and 50%. , fully mixed to become a 3% standard sample;
[0040] Take 0.15 ml of liquid X and 9.85 ml of liquid Y to keep the total volume at a constant value of 10 ml. The volume ratio of liquid X and liquid Y is 1.5%, and they are fully mixed to form a 30% standard sample.
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