Interior liner for tubes, pipes, and blood conduits
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example 1
[0040]This example describes an interior liner of the present invention useful primarily as a liner for blood conduits. It was made to require distension by a balloon catheter, to have a second circumference and to have minimal recoil. Having helically-wrapped layers of porous PTFE film applied in opposing directions, it is described in appearance by FIG. 2. It was manufactured according to the procedure described by the flow chart of FIG. 4.
[0041]To make this particular interior liner, a 3 mm inside diameter, longitudinally extruded and expanded porous PTFE tube was obtained. This tube had a wall thickness of about 0.25 mm and a fibril length of about 25 microns. The tube was fitted coaxially onto a 3 mm diameter stainless steel mandrel as described by step 1 of FIG. 4.
[0042]Next, a length of porous PTFE film was obtained that had been cut to a width of 5.1 cm. This film had a thickness of about 0.02 mm, a density of 0.2 g / cc and a fibril length of about 70 microns. Thickness was m...
example 2
[0051]This example also appears as described by FIG. 2 and was made with the same process and materials as that of Example 1, except for the following differences. The 3 mm inside diameter, longitudinally extruded and expanded tube of 0.25 mm wall thickness described by step 1, was replaced with an otherwise identical tube having a 0.10 mm wall thickness and a 30 micron fibril length. The porous PTFE film of step 2 was of 2.5 cm width rather than the 5.1 cm width. Likewise the mandrel about which the film was helically wrapped in step 2 was of 10 mm diameter rather than 12 mm diameter. The heat treatment described by step 3 was performed at 380° C. for 11 minutes rather than 12 minutes. In step 8 the larger mandrel used was of 10 mm rather than 8 mm diameter. Finally, in step 11, only about 5 kg of force was required to tension the tube to cause it to conform to the 3.2 mm diameter mandrel. The resulting interior liner was distensible at normal human blood pressures and consequently...
example 3
[0056]An example was made which was circumferentially distensible up to a second circumference; however, process step 9 intended to better resist recoil following the release of the distending force was omitted. The physical appearance of this example is also described by FIG. 2.
[0057]This example was made from the same materials and by the same method as Example 1 with the omission of step 9 of FIG. 4. The film-covered porous PTFE tube of step 8 was removed from the 8 mm diameter mandrel per step 10, after which about 8 kg tension was applied to the ends of the tube adequate to cause the tube to assume the 3.2 mm diameter of the mandrel according to step 11.
[0058]An interior liner made according to this description was subjected to heat sterilization in an air convection oven at about 145° C. for 15 minutes. Steam was not used. The inside diameter was determined to be 3.7 mm using a tapered, smooth-finished, graduated stainless steel mandrel.
[0059]Percentage recoil for the heat ste...
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Abstract
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