A specific identification method for honey-roasted decoction pieces of traditional Chinese medicine

An exclusive technology for honey-roasted decoction pieces, which is applied in the field of exclusive identification of traditional Chinese medicine honey-roasted decoction pieces, and can solve the problems of deepening color and inability to achieve traditional Chinese medicine honey-roasting and other problems.

Active Publication Date: 2018-11-23
SHANDONG ACAD OF CHINESE MEDICINE
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, replacing honey with fructose syrup as an auxiliary material for honey-burning certainly cannot achieve the proper purpose of traditional Chinese medicine honey-burning
Although the fructose syrup is colorless, the color of the licorice itself will deepen during heating, and the fructose syrup is also viscous, so it is difficult to distinguish the authenticity from the real processed product with the naked eye.

Method used

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  • A specific identification method for honey-roasted decoction pieces of traditional Chinese medicine
  • A specific identification method for honey-roasted decoction pieces of traditional Chinese medicine
  • A specific identification method for honey-roasted decoction pieces of traditional Chinese medicine

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0020] The preparation method of the test solution is as follows: take 0.5g of coarse powder of licorice decoction pieces (prepared from licorice licorice and fructose syrup), add 5mL of ethanol solution with a concentration of 60%-75%, ultrasonic treatment for 10 min, filter After passing, put the filtrate in a 5mL measuring bottle, add ethanol of the same concentration to the mark, and shake well.

[0021] Preparation of honey control solution: Take 0.5g of honey, put it in a 25mL measuring bottle, add 60%-75% ethanol solution to dissolve, dilute to the mark, mix well, and use it as honey control solution.

[0022] Preparation of the reference substance solution: Take an appropriate amount of each of the glucose, fructose, and sucrose reference substances, add 60%-75% ethanol solution to make a solution containing 10 mg each of glucose, fructose, and sucrose per 1 mL, as the reference substance solution.

[0023] Thin-layer chromatography: According to the thin-layer chromat...

Embodiment 2

[0026] The preparation method of the test solution is as follows: take 0.5g of the coarse powder of Astragalus decoction pieces and honey-roasted decoction pieces, add 5mL of ethanol solution with a concentration of 60%-75% precisely, ultrasonicate for 10 min, filter, put the filtrate in a 5mL measuring bottle, add The same concentration of ethanol to the mark, shake well.

[0027] Preparation of honey control solution: Take 0.5g of honey, put it in a 25mL measuring bottle, add 60%-75% ethanol solution to dissolve, dilute to the mark, mix well, and use it as honey control solution.

[0028] Preparation of the reference substance solution: Take an appropriate amount of each of the glucose, fructose, and sucrose reference substances, add 60%-75% ethanol solution to make a solution containing 10 mg each of glucose, fructose, and sucrose per 1 mL, as the reference substance solution.

[0029] Thin-layer chromatography: According to the thin-layer chromatography test, draw 3-5 µL o...

Embodiment 3

[0032] The preparation method of the test solution is as follows: take 0.5g of the coarse powder of the decoction pieces of Peucedanum and honey-roasted decoction pieces, add 5mL of ethanol solution with a concentration of 60%-75% accurately, ultrasonically treat for 10 min, filter, and put the filtrate in a 5mL measuring bottle. Add the same concentration of ethanol to the mark and shake well.

[0033] Preparation of honey control solution: Take 0.5g of honey, put it in a 25mL measuring bottle, add 60%-75% ethanol solution to dissolve, dilute to the mark, mix well, and use it as honey control solution.

[0034] Preparation of the reference substance solution: Take an appropriate amount of each of the glucose, fructose, and sucrose reference substances, add 60%-75% ethanol solution to make a solution containing 10 mg each of glucose, fructose, and sucrose per 1 mL, as the reference substance solution.

[0035] Thin-layer chromatography: According to the thin-layer chromatograp...

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Abstract

The invention provides a specificity identification method for a traditional Chinese medicine honey-fried decoction piece. The crude product, the honey-fried product and the fake honey-fried product of the traditional Chinese medicine are identified through thin-layer chromatography, and the crude product, the honey-fried product and the fake honey-fried product of the traditional Chinese medicine are distinguished.

Description

technical field [0001] The invention relates to a specific identification method for honey-roasted decoction pieces of traditional Chinese medicine, which belongs to the technical field of traditional Chinese medicine. Background technique [0002] Clinically, Chinese herbal medicines must be processed into decoction pieces before they can be used as medicines. "Cultivation is not seen by anyone, but God knows it with the heart" is an ancient and simple pharmaceutical concept. Therefore, processing is the main factor affecting the efficacy of traditional Chinese medicines. The efficacy and properties of traditional Chinese medicines have changed after processing, such as licorice raw and cooked tonic, rhubarb raw and ripe slowly, and aconitum raw and cooked to reduce toxicity. Unable to distinguish raw products from processed products, what's more, the evaluation criteria of raw products and processed products are "same medicinal materials". However, among the various proce...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N30/90
CPCG01N30/90
Inventor 周倩戴衍朋孙立立葛秀允
Owner SHANDONG ACAD OF CHINESE MEDICINE
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