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A sunscreen agent with high content of titanium dioxide or zinc oxide and its preparation method

A technology of titanium dioxide and zinc oxide, applied in cosmetic preparations, skin care preparations, cosmetics, etc., can solve the problems of emulsion breaking, easy phase inversion, sticky skin feeling of sunscreen cosmetics, etc., and achieve refreshing skin feeling and low irritation Effect

Active Publication Date: 2021-09-07
HUANAN IND TECH RES INST OF ZHEJIANG UNIV +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] (1) The amount of titanium dioxide and zinc oxide should not be too high
Because hydrophobically modified nano-scale titanium dioxide or zinc oxide has a water-in-oil interfacial activity tendency, if the amount used is too high, it is very easy to phase inversion, so that the phase inversion of the oil-in-water system becomes a water-in-oil system, or direct demulsification and stratification , greatly reducing the system stability
[0005] (2) Using high content or high molecular weight emulsifiers for emulsification will lead to bad skin feeling
For the same reason, due to the strong water-in-oil tendency of hydrophobically modified titanium dioxide or zinc oxide particles, it is necessary to use a large number of emulsifiers with high HLB value or high molecular weight to overcome this tendency, and these emulsifiers are often very sticky. The skin feel of the whole oil-in-water sunscreen cosmetics becomes sticky, and even if a large amount of such emulsifiers are used, it is still very easy to phase invert or break when using high content of titanium dioxide or zinc oxide

Method used

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  • A sunscreen agent with high content of titanium dioxide or zinc oxide and its preparation method
  • A sunscreen agent with high content of titanium dioxide or zinc oxide and its preparation method
  • A sunscreen agent with high content of titanium dioxide or zinc oxide and its preparation method

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Embodiment 10

[0028] The present embodiment provides a kind of preparation method of the sunscreen agent of high-content titanium dioxide or zinc oxide, and described method comprises the following steps:

[0029] (1) Take 20 parts of titanium dioxide or zinc oxide treated with triethoxyoctylsilane and disperse it into the oil phase under high-speed stirring to make a slurry. The oil phase contains the following components by weight: isononanoic acid isononyl In the mixed oil phase composed of 10 parts of triglyceride (ethylhexanoate), 10 parts of tri(ethylhexanoate), 15 parts of polydimethylsiloxane, 1 part of polyhydroxystearic acid, and 4 parts of jojoba seed oil;

[0030] (2) Get 2 parts of acrylic acid (esters) / beheneth-25 methacrylate copolymer and join in the mixed water phase of water and phenoxyethanol, then neutralize with sodium hydroxide, make the water phase Viscosity rises;

[0031] (3) Under the homogeneous condition, slowly add the powder slurry into the thickened water pha...

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Abstract

The invention provides a sunscreen agent with a high content of titanium dioxide or zinc oxide, comprising the following components in parts by weight: 5-20 parts of hydrophobically modified titanium dioxide or zinc oxide, acrylic acid (ester) / beheneth-25 0.2-2 parts of methacrylate copolymer, 0.05-2 parts of alkali agent, and 0.3-1 part of preservative. The hydrophobic inorganic sunscreen particle content in the sunscreen agent of the present invention is relatively high, can easily reach a high SPF value, and has a refreshing skin feel; because the use of emulsifiers is exempted, it will have a more refreshing skin feel and lower irritation, Sunscreen cosmetics suitable for sensitive skin.

Description

technical field [0001] In the field of cosmetics, the invention particularly relates to a sunscreen agent with high content of titanium dioxide or zinc oxide and a preparation method thereof. Background technique [0002] Titanium dioxide and zinc oxide of inorganic sunscreens are insoluble particles, which are dispersed in the water phase of cosmetics, and agglomeration will occur during application on the skin, thereby greatly reducing the sunscreen effect. Therefore, titanium dioxide or zinc oxide used in sunscreen cosmetics generally adopts hydrophobically modified nano-sized particles, which are then dispersed in the oil phase of the cosmetics. However, to prepare oil-in-water sunscreen cosmetics with a refreshing skin feel, an emulsifier is generally used to emulsify the powder slurry of titanium dioxide or zinc oxide to achieve the effect of evenly dispersing titanium dioxide or zinc oxide in the cosmetics, so that it can be evenly dipped in when applied. Pick. [0...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): A61K8/27A61K8/29A61K8/31A61K8/37A61K8/58A61K8/891A61K8/92A61Q17/04A61Q19/00
CPCA61K8/27A61K8/29A61K8/31A61K8/37A61K8/585A61K8/891A61K8/922A61Q17/04A61Q19/005
Inventor 钟晓明何杨鹏高雪山
Owner HUANAN IND TECH RES INST OF ZHEJIANG UNIV
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