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Temperature-sensitive color-changing shape-memory material indicating deformation temperature and preparation method thereof

A technology of temperature-sensitive discoloration and deformation temperature, which is applied in the field of temperature-sensitive color-changing shape memory materials and their preparation, and can solve problems such as inaccurate temperature

Active Publication Date: 2021-07-06
青岛维思顿智能新材料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] Most of the shape memory materials in the prior art are polymer materials. In general, the deformation of shape memory materials is mostly temperature-sensitive materials. Once the temperature of the material reaches the deformation temperature of the material, the shape of the material will be However, in the process of thermal deformation of the shape memory material, the deformation temperature of the shape memory material can only be indirectly indicated by the ambient temperature of the material that causes the deformation of the shape memory material. There are differences in the temperature of the shape memory material itself, and the temperature corresponding to the shape transformation point of the shape memory material indicated in this way is not accurate

Method used

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  • Temperature-sensitive color-changing shape-memory material indicating deformation temperature and preparation method thereof
  • Temperature-sensitive color-changing shape-memory material indicating deformation temperature and preparation method thereof
  • Temperature-sensitive color-changing shape-memory material indicating deformation temperature and preparation method thereof

Examples

Experimental program
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Effect test

Embodiment 1

[0043] Put polycaprolactone (PCL) into the internal mixer at 70°C, rotate at 30rpm, and banbury for 5 minutes; add 5% of the mass of the masterbatch as a temperature-sensitive discoloration agent green pigment 335C; then add 15% of the mass of the masterbatch as inorganic filler agent, such as titanium dioxide, calcium carbonate, barium sulfate, carbon black or clay, etc., in this embodiment, the filler is calcium carbonate, banburying for 5 minutes; take it out, vulcanize the vulcanization test piece under the condition of temperature 100 ℃, pressure 10MPa After 10 minutes, a temperature-sensitive color-changing shape-memory material indicating the deformation temperature was prepared.

[0044] When the temperature starts to rise from room temperature, the material prepared by this formula is green; when the temperature is 60-65 ° C, the material changes from green to the original color of the material, indicating that the material can begin to deform; after the fixed shape is...

Embodiment 2~ Embodiment 5

[0046]

[0047]

[0048]

[0049]

[0050]The temperature-sensitive color-changing shape memory material indicating the deformation temperature prepared by the method provided by the present invention is used in the injured part when it is used in human medical treatment, such as spine correction, ankle injury correction, tenosynovitis correction, mouse hand treatment, etc. Orthotics, braces, and braces of flexible materials that require temperatures to reach their shape-deformation temperature in order to deform and hold. The temperature-sensitive color-changing shape-memory material for indicating deformation temperature prepared by the method provided by the invention is mainly used for indicating the deformation temperature of shape-memory medical devices deformed by temperature at 60-68°C. The advantage is that there is no need for temperature indicating equipment required in the deformation process of the shape memory material, and the color change of the shap...

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Abstract

Disclosed are a temperature-sensitive color-changing shape-memory material indicating deformation temperature and a preparation method thereof, belonging to the technical field of polymer materials. The material includes a masterbatch, an auxiliary material and a color-changing pigment that changes with temperature, wherein the master batch includes polycaprolactone, the amount of the auxiliary material includes a filler, and the value range of the color-changing temperature of the color-changing pigment that changes with temperature is the same as that of the master batch. The value range of the deformation temperature is the same; the addition amount of the auxiliary material is 5%-23% of the mass of the master batch, and the addition amount of the color-changing pigment that changes with temperature is 2%-10% of the mass of the master batch. The method includes putting the masterbatch into the internal mixer for the first internal mixing; adding color-changing pigments and auxiliary materials that change with the temperature in the same range as the deformation temperature of the masterbatch; putting the masterbatch into the internal mixer for the second internal mixing ; After vulcanization, the temperature-sensitive color-changing shape-memory material indicating the deformation temperature is obtained. It indicates the shape-memory material shape-change transition point by a color change at the shape-change transition point of the shape-memory material.

Description

technical field [0001] The invention relates to the technical field of polymer materials, in particular to a temperature-sensitive color-changing shape-memory material indicating deformation temperature and a preparation method thereof. Background technique [0002] Most of the shape memory materials in the prior art are polymer materials. In general, the deformation of shape memory materials is mostly temperature-sensitive materials. Once the temperature of the material reaches the deformation temperature of the material, the shape of the material will be However, in the process of thermal deformation of the shape memory material, the deformation temperature of the shape memory material can only be indirectly indicated by the ambient temperature of the material that causes the deformation of the shape memory material. There are differences in the temperature of the shape memory material itself, and the temperature corresponding to the shape transformation point of the shape...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08L67/04C08K3/26C08K5/00C08K3/013C08L23/08
CPCC08K3/26C08K5/0041C08L2201/12C08L2203/02C08K3/013C08L67/04C08L23/0815C08L23/0853
Inventor 刘卫东谭琳
Owner 青岛维思顿智能新材料有限公司
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