Temperature-sensitive color-changing shape-memory material indicating deformation temperature and preparation method thereof
A technology of temperature-sensitive discoloration and deformation temperature, which is applied in the field of temperature-sensitive color-changing shape memory materials and their preparation, and can solve problems such as inaccurate temperature
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Embodiment 1
[0043] Put polycaprolactone (PCL) into the internal mixer at 70°C, rotate at 30rpm, and banbury for 5 minutes; add 5% of the mass of the masterbatch as a temperature-sensitive discoloration agent green pigment 335C; then add 15% of the mass of the masterbatch as inorganic filler agent, such as titanium dioxide, calcium carbonate, barium sulfate, carbon black or clay, etc., in this embodiment, the filler is calcium carbonate, banburying for 5 minutes; take it out, vulcanize the vulcanization test piece under the condition of temperature 100 ℃, pressure 10MPa After 10 minutes, a temperature-sensitive color-changing shape-memory material indicating the deformation temperature was prepared.
[0044] When the temperature starts to rise from room temperature, the material prepared by this formula is green; when the temperature is 60-65 ° C, the material changes from green to the original color of the material, indicating that the material can begin to deform; after the fixed shape is...
Embodiment 2~ Embodiment 5
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[0050]The temperature-sensitive color-changing shape memory material indicating the deformation temperature prepared by the method provided by the present invention is used in the injured part when it is used in human medical treatment, such as spine correction, ankle injury correction, tenosynovitis correction, mouse hand treatment, etc. Orthotics, braces, and braces of flexible materials that require temperatures to reach their shape-deformation temperature in order to deform and hold. The temperature-sensitive color-changing shape-memory material for indicating deformation temperature prepared by the method provided by the invention is mainly used for indicating the deformation temperature of shape-memory medical devices deformed by temperature at 60-68°C. The advantage is that there is no need for temperature indicating equipment required in the deformation process of the shape memory material, and the color change of the shap...
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