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Method for manufacturing injectable water-swelling gingival retraction paste

A technology of water absorption swelling and manufacturing method, applied in the field of biomedical materials, can solve the problems of unfavorable clinical wide application and high price, and achieve the effects of good stability, convenient operation and good cost performance.

Inactive Publication Date: 2012-06-06
ANHUI MEDICAL UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The wireless gingival retraction technology has the advantages of positive clinical effect, time saving, easy operation, no bleeding, no need for anesthesia, and less damage, but its price is expensive, which is dozens of times that of the gingival retraction cord. It is not suitable for my country's national conditions and is not conducive to widespread clinical application.

Method used

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  • Method for manufacturing injectable water-swelling gingival retraction paste
  • Method for manufacturing injectable water-swelling gingival retraction paste
  • Method for manufacturing injectable water-swelling gingival retraction paste

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0020] The preparation method of injectable water-absorbent swellable gingival retraction paste comprises the following steps: use an analytical electronic mass balance to measure 2 g of polyvinylpyrrolidone (PVP), measure 20 mL of 15% aluminum chloride solution in a graduated cylinder, mix the two , placed in a 70°C water bath to fully dissolve. After 30 minutes, slowly add 30g of kaolin measured by an analytical electronic mass balance, 2g of cross-linked polyvinylpyrrolidone (PVPP), put it into a digital constant temperature stirrer, stir well, the temperature is 70°C, the speed is 100r / s, stir The injectable water-absorbing swellable gingiva removal paste was obtained in 30 minutes. The appearance of the injectable water-absorbing swellable gingiva-removal paste was milky white, ooze-like semi-solid, and the specific structure and appearance, see Figure 5 ;Under a certain pressure, it can be molded by injection, has a certain viscoelasticity, can maintain the stability of...

Embodiment 2

[0024] Use an analytical electronic mass balance to measure 1 g of polyvinylpyrrolidone (PVP), and a measuring cylinder to measure 20 mL of 10% aluminum chloride solution. After mixing the two, place them in a water bath at 70 °C to fully dissolve them. After 30 minutes, slowly add 25g of kaolin measured by an analytical electronic mass balance, 2g of cross-linked polyvinylpyrrolidone (PVPP), put it into a digital constant temperature stirrer, stir well, the temperature is 70°C, the speed is 100r / s, stir 30min. Obtain an injectable water-swellable gingival retraction paste. Using method is the same as embodiment 1.

Embodiment 3

[0026] Measure 3g of polyvinylpyrrolidone (PVP) with an analytical electronic mass balance, and measure 20mL of 15% aluminum chloride solution with a graduated cylinder. After mixing the two, place them in a water bath at 70°C to fully dissolve them. After 30 minutes, slowly add 20g of kaolin measured by an analytical electronic mass balance, 3g of cross-linked polyvinylpyrrolidone (PVPP), put it into a digital constant temperature stirrer, stir well, the temperature is 70°C, the speed is 100r / s, stir 30min. Obtain an injectable water-swellable gingival retraction paste. Using method is the same as embodiment 1.

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Abstract

The invention relates to a method for manufacturing injectable water-swelling gingival retraction paste. The method comprises the following specific operations of: preparing and mixing 1-3g of polyvinylpyrrolidone (PVP) and 20mL of aluminium chloride solution with concentration of 15%, and putting in a water bath at a temperature 70 DEG C for 30min to sufficiently dissolve; slowly adding 20-30g of kaolin and 2-3g of cross-linked polyvinylpyrrolidone (PVPP), putting in a numerical constant temperature stirrer, and sufficiently stirring at a temperature 70 DEG C under a revolving speed 100r / s to obtain the injectable water-swelling gingival retraction paste. The method for manufacturing injectable water-swelling gingival retraction paste has simple operation, good controllability, environmentally friendly and high yield; the materials used are pharmaceutical substances with high biocompatibility, the injectable water-swelling gingival retraction paste is an ideal material for implementing gingival retraction technology; the gingival retraction material obtained through the method has the advantages of convenient operation, time-saving and no wound and the like; when compared with similar products abroad, the injectable water-swelling gingival retraction paste has high price performance ratio; the problem that similar products abroad are collapsed when meeting water is overcome, with good stability in oral cavity saliva environment, the injectable water-swelling gingival retraction paste is not collapsed, and the injectable water-swelling gingival retraction paste can swell.

Description

technical field [0001] The invention belongs to biomedical material technology, and is used for a preparation method of materials that need to push away gingival margins in clinical oral cavity. Background technique [0002] In oral clinical fixed restoration, when the restoration edge involves the gingival margin or subgingival, improving the suitability of the crown edge and reducing its stimulation to the periodontal tissue is the key to the success of the restoration. Using gingival retraction technology is conducive to preparing good tooth margins and reducing damage to the gingiva during tooth preparation. It can also improve the accuracy of impressions, thereby increasing the success rate of restorations. [0003] The initial gingival retraction material used was homemade cotton thread with or without epinephrine. Later, specialized companies produced finished products, such as braided gingival retraction cords, double-strand twisted gingival retraction cords; drug-f...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): A61K6/00
Inventor 徐晓华李全利祝小鹏宁天云刘巍
Owner ANHUI MEDICAL UNIV
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