Organic silicon pouring sealant, preparation method and application thereof
A technology of silicone potting glue and silicone rubber, which is applied in chemical instruments and methods, adhesives, and other chemical processes, can solve problems such as heavy metal poisoning, local curing failure, and poor adhesion, so as to avoid metal poisoning, Good operability, easy deployment effect
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Embodiment 1
[0053] A method for preparing a silicone potting compound suitable for insulating and heat-conducting circuit boards, the method comprising the following process steps:
[0054] a, preparation component A
[0055] (1) Prepare raw materials according to the following content: 15kg hydroxy silicone oil, wherein the molar fraction of methyl group is 1000g / mol, 20kg viscosity is 3000mpa s room temperature vulcanized silicone rubber, 20kg surface treatment aluminum hydroxide, 40kg aluminum oxide, 0.086 kg catalyst dibutyltin dilaurate;
[0056] (2) Put hydroxyl silicone oil and room temperature vulcanized silicone rubber into the reaction kettle, heat to 30°C and stir;
[0057] (3) Keep stirring and put the functional filler into the reaction kettle, the functional filler is a mixture of surface-treated aluminum hydroxide and aluminum oxide, seal the reaction kettle, heat and stir in vacuum for 5h;
[0058] (4) After mixing evenly, strictly calculate the required amount of cataly...
Embodiment 2
[0067] A method for preparing a silicone potting compound suitable for insulating and heat-conducting circuit boards, the method comprising the following process steps:
[0068] a, preparation component A
[0069] (1) Prepare raw materials according to the following content: 20kg hydroxysilicone oil, wherein the molar fraction of methyl group is 2000g / mol, 25kg viscosity is room temperature vulcanized silicone rubber of 3000mpa s, 60kg surface treatment aluminum hydroxide, 0.5kg chloroplatinic acid , 0.073kg catalyst n-butyl titanate;
[0070] (2) put hydroxy silicone oil and room temperature vulcanized silicone rubber into the reaction kettle, heat to 60°C and stir;
[0071] (3) Keep stirring and put the functional filler into the reactor, the functional filler is a mixture of surface-treated aluminum hydroxide and chloroplatinic acid, seal the reactor, and heat and stir in vacuum for 10 hours;
[0072] (4) After mixing evenly, strictly calculate the required amount of cata...
Embodiment 3
[0081] A method for preparing a silicone potting compound suitable for insulating and heat-conducting circuit boards, the method comprising the following process steps:
[0082] a, preparation component A
[0083] (1) Prepare raw materials according to the following content: 15kg hydroxy silicone oil, wherein the molar fraction of methyl group is 1500g / mol, 15kg room temperature vulcanized silicone rubber with a viscosity of 3000mpa s, 40kg surface treatment aluminum hydroxide, 0.01kg catalyst diisocyanate Titanium propoxide bis(ethyl acetoacetate) chelate;
[0084] (2) Put hydroxyl silicone oil and room temperature vulcanized silicone rubber into the reaction kettle, heat to 40°C and stir;
[0085] (3) keep stirring and put the functional filler into the reactor, the functional filler is surface-treated with aluminum hydroxide, seal the reactor, heat and stir in vacuum for 8 hours;
[0086] (4) After mixing evenly, strictly calculate the required amount of catalyst, put 0.0...
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