A kind of salt bridge production method used in low temperature environment
A low-temperature environment and production method technology, applied in the direction of material electrochemical variables, can solve the problems of residual bubbles, easy solidification, and affecting experimental results, etc., and achieve the effect of moderate gelation speed, stable chemical properties, and good solubility
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Embodiment 1
[0029] The salt bridge used under the low temperature environment has the ratio of raw materials in parts by weight, saturated potassium nitrate solution: soluble starch: density of 1.34g / cm 3 The ratio of dilute sulfuric acid is 8:7:4.
[0030] 1. First measure 8 grams of saturated KNO 3 The solution is placed in a 30mL small beaker, and the density is 1.34g / cm 3 Slowly pour 4 grams of dilute sulfuric acid into the saturated KNO 3 In a small beaker of the solution, stir well with a glass rod. Then measure 7 grams of soluble starch, pour into the saturated KNO 3 In a small beaker of the solution, stir it with a glass rod for a few seconds until it is uniform and presents a cloudy floating state.
[0031] 2. Make sure that the bottom of the beaker is dry and put it on the preheated muffle furnace, and then stir it with a glass rod for 1-2 minutes, so that the turbid floating starch is heated to a translucent beige paste, stop stirring, and turn off the power of the muffle f...
Embodiment 2
[0036] The salt bridge used under the low temperature environment has the ratio of raw materials in parts by weight, saturated potassium nitrate solution: soluble starch: density of 1.34g / cm 3 The ratio of dilute sulfuric acid is 10:10:2.
[0037] The preparation steps are as in Example 1.
[0038] Cut the prepared salt bridge to a length of 100mm as required, press figure 1 The connection method is connected, and placed in different environments at 0 ° C ~ -18 ° C for 12 hours, according to the process, the current 6A is discharged to 1.75V / single cell, and then 0.18C 2 A limited voltage 2.5V / single cell constant current and constant voltage charging for 12 hours. Process the measured positive and negative electrode potentials, and compare them with the previous punching method, such as image 3 shown.
[0039] From Example 2, image 3The results of the test show that the test results of the salt bridge prepared by this method are basically consistent with the discharge ...
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