A kind of unsaturated fatty acid solid-phase microextraction method
An unsaturated fatty acid and extraction technology, applied in the field of analytical chemistry, can solve the problems of indistinguishable, qualitative and quantitative analysis effects, etc., and achieve the effects of simple method, improved separation, and ingenious process
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[0032] 1. Preparation of mucopolysaccharide functionalized monolithic column:
[0033] 1) Cleaning of PTFE tube empty column: connect the PTFE tube with an inner diameter of 750 μm to the liquid phase pump, wash it with chromatographically pure methanol at a flow rate of 0.5mL / min for 10 min, remove the residual organic impurities on the inner wall of the tube, and then pass nitrogen gas, and dried in an oven at 60 °C for 10 min.
[0034]2) Rapid polycondensation in the tube: Mix 8 mg sodium hyaluronate, 550 mg 1 g / mL urea solution, 450 mg formaldehyde solution, and 100 mg 0.2 mol / L hydrochloric acid solution evenly, and oscillate rapidly for 1 to 2 min, and then dissolve the mixture Quickly fill the cleaned and dried PTFE tube (or PEEK tube), seal both ends and immerse in a water bath at 70 °C for 10 min at a constant temperature; after the reaction is completed, use water as the mobile phase and rinse the PTFE tube on the liquid chromatography pump Keep the monolithic colum...
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