Thermal treatment process for X12CrMoWVNbN10-1-1 grain refinement

A grain refinement and process technology, which is applied in the heat treatment process field of X12CrMoWVNbN10-1-1 grain refinement, can solve the problems of increasing the concentration of carbides and nitrides, reducing energy absorption, and the impact of impact absorption, etc.

Active Publication Date: 2020-02-28
WUXI HONGDA HEAVY IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, due to the high content of alloying elements and a variety of strong carbide-forming elements, this material has very good hardenability and very stubborn structure inheritance. Therefore, after the grain is coarse, the grain size is difficult to refine, and the grain The difficulty of grain refinement is obviously more than that of martensitic heat-resistant steel such as SA336F91 and SA336F92
[0008] The existing heat treatment process for grain refinement of X12CrMoWVNbN10-1-1 steel is normalizing + high temperature tempering, high temperature normalizing + high temperature tempering, and then conventional normali...

Method used

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Examples

Experimental program
Comparison scheme
Effect test

specific Embodiment 1

[0036] Specific embodiment one: when adopting a heat treatment furnace, its concrete technological process is as follows:

[0037] 1 High temperature normalizing: 650°C, preheat for 2-3h; heat up to 790°C, keep warm for 10-15h to ensure that the workpiece is thoroughly burned; It is possible to get more spherical austenite, destroying the relationship of metallographic orientation, heat preservation at 1080°C-1110 for 6-8h, furnace cooling or air cooling; adjust the temperature between 1080-1110°C to obtain the most suitable austenitization temperature;

[0038] 2 High temperature tempering: 700°C, keep warm for 15-20h, let the carbide precipitate as much as possible, further destroy the relationship of metal orientation, air cooling;

[0039] 3 Conventional normalizing: 650°C, preheat for 2-3h; heat up to 790°C, keep warm for 10-15h, must ensure that the workpiece is thoroughly burned. Then raise the temperature with the maximum power of the heat treatment furnace, pass thro...

specific example 2

[0042] When two heat treatment normalizing high temperature furnaces are used for heat treatment process, the specific process flow is as follows:

[0043] 1 Preheating: 650°C, keep warm for 2-3h; heat up to 790°C, keep warm for 10-12h, to ensure that the workpiece is thoroughly burned;

[0044] 2 Carry out high-temperature normalizing through the first heat treatment normalizing high-temperature furnace: heat the furnace to 1080-1110 ° C in advance, keep it at this temperature for at least 2.5 hours, and then transfer the preheated and completely burnt workpiece to this furnace In the process, heat up rapidly at the maximum power, pass through the two-phase region of α+γ at the fastest possible heating rate, and then heat to 1080-1110°C for 6-8h, furnace cooling or air cooling; adjust the temperature between 1080-1110°C , to select the most suitable austenitizing temperature;

[0045] 3 High temperature tempering: 700℃, heat preservation for 15-20h, air cooling;

[0046] 4 ...

specific example 3

[0049] Specific example three: when adopting two heat treatment normalizing high-temperature furnaces as specific embodiment 2 to carry out heat treatment process, retain enough other workpieces in each heat treatment normalizing high-temperature furnace, and these workpieces are in the corresponding temperature in the furnace. Through-fired state (process and heat treatment parameters are as in Example 2).

[0050] The heat treatment process of X12CrMoWVNbN10-1-1 steel grain refinement in the prior art is normalizing + high temperature tempering, high temperature normalizing + high temperature tempering, and then conventional normalizing + high temperature tempering, complete annealing, the effect is very good Poor, the grain size can only be increased by 0.5. The reason why the effect is not ideal is that the alloy element content of X12CrMoWVNbN10-1-1 steel is relatively high, the hardenability is very good, and the hereditary structure is very stubborn. Whether it is normal...

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PUM

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Abstract

The invention provides a thermal treatment process for X12CrMoWVNbN10-1-1 grain refinement. According to the thermal treatment process, the amount of acicular austenite is decreased as much as possible by increasing the heating speed, and the amount of spherical austenite is increased, so that grain refinement is achieved, the grain size can meet the technical requirement, and the using range of X12CrMoWVNbN10-1-1 is enlarged. Fed materials are forged into workpieces, the workpieces are sequentially subjected to high-temperature normalizing, high-temperature tempering, conventional normalizingand high-temperature tempering, and then the workpiece subjected to high-temperature tempering are subjected to subsequent processing treatment. In the high-temperature normalizing process, the temperature increasing speed of the workpieces in an alpha and gamma two-stage region is increased, the workpieces can pass through the two-stage region rapidly, and the spherical austenite can be obtainedas much as possible. On one hand, the orientation relationship of crystallography is broken through to a greater extent, namely, the K--S relationship; and on the other hand, the nucleation rate of the austenite can be increased by increasing the heating speed. The high-temperature tempering process particularly comprises the steps that heat preservation is conducted for 15-20 h at the environmental temperature of 700 DEG C to enable carbides to be dissolved as many as possible to further destroy the orientation relationship of metallography, and then air cooling is conducted.

Description

technical field [0001] The invention relates to the technical field of material heat treatment, in particular to a heat treatment process for X12CrMoWVNbN10-1-1 grain refinement. Background technique [0002] The forging manufacturing industry is the basic industry of the national equipment manufacturing industry. It is also an indispensable strategic industry related to national security and the lifeline of the national economy. It is also an important component of national capabilities. The development level of large forgings is a measure of a country's comprehensive capabilities important sign. [0003] With the rapid development of electric power, petrochemical and other industries at home and abroad, some new technologies and equipment have appeared, and some new materials have been used; at the same time, new requirements have been put forward for the forging industry, which not only promotes the continuous upgrading of forging equipment , and accelerated the generati...

Claims

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Application Information

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IPC IPC(8): C22C38/02C22C38/04C22C38/44C22C38/42C22C38/46C22C38/48C22C38/54C22C38/06C21D1/28
CPCC21D1/28C22C38/001C22C38/02C22C38/04C22C38/06C22C38/42C22C38/44C22C38/46C22C38/48C22C38/54
Inventor 张瑞庆张忠明张伟东孙景会马晗珺
Owner WUXI HONGDA HEAVY IND
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