625results about How to "Increase nucleation rate" patented technology

A coated medical device have a drug and a nucleating agent thereon. Also provided are methods of increasing or decreasing the size of drug particles on a coated substrate through the use of nucleating agents to thereby increase or decrease the release rate of the drug from the coated substrate.

The invention proposes an added material manufacturing method under a vibration condition. In an arc wire feeding added material manufacturing or laser powder feeding melting added material manufacturing process, mechanical vibration with a certain frequency is synchronously introduced, so that parts are located in a micro vibrating state; and the mechanical vibration acts on a micro liquid-state molten bath formed in the added material manufacturing process to refine grains, so that the structure becomes more uniform, and such phenomenon as air holes, inclusions and incomplete fusion is reduced or even eliminated. Meanwhile, the vibration acts on metal just condensed, so that the stress generated by vibration and residual stress generated in the added material manufacturing process are superposed to generate local plastic deformation to achieve the purpose of reducing residual stress and deformation of added material manufacturing parts, and the added material manufacturing parts under vibration condition are more excellent in performances.

The invention provides a method and a device for preparing high-performance aluminum-base composite material under the action of the pulsed magnetic field with the in situ crystallization method, belonging to the technical field of material preparation. The method comprises the following steps: smelting to synthesize compound material melt at the temperature of 10-200 DEG C higher than the compound material melt liquidus temperature and pouring the compound material melt into a specially-designed crystallizer to make the compound material melt solidify under the action of the pulsed magnetic field. The pulsed magnetic field has the key parameters of the pulse width of 1-500 ms and the amplitude strength of 0.1-50T. The pulsed electromagnetic force is applied to the process of solidifying the compound material melt under the action of the pulsed magnetic field so as to refine the matrix structure and the particle reinforced phase of the compound material at the same time, control the growth of the particle reinforced phase in cluster, increase the bonding strength of the interface of the particle reinforced phase and the matrix and obviously improve the performance of the composite material.

The invention relates to a quality improving method for horizontal continuous casting blanks by applying complex field and the device, belonging to the technical field of preparation of metal material, in particular to the technology of applying complex electromagnetic field and ultrasonic field in the continuous casting process of metal casting blanks. The device is characterized in that a generator of inert gas is arranged at the center of the bottom of a holding furnace; a generator of traveling wave magnetic field is arranged on the side of the holding furnace; a power ultrasonic device is arranged on the holding furnace close to the water port; a restriction electromagnetic coil is arranged on the outer side of a crystallizer. The device has the advantages that: firstly, the production technology is simple, the operation is easy, and the efficiency is high; secondly; the disadvantages of easy broken in rolling and drawing process of casting blank due to more impurity and pores is solved; thirdly, the solidification structure of the casting blanks is uniform, the crystal grain is fine, and the casting blanks can be rolled directly at casting state. The quality improving method and the device are mainly used for the field of metal continuous casting.

The invention discloses an ageing heat treatment method for a low-purity Al-Zn-Mg-Cu alloy. The method includes the steps that the low-purity aluminum alloy is treated in a solution mode at the temperature of 465 DEG C-480 EDG C for 1-2 h, then first-level ageing is carried out at the temperature of 90 DEG C-120 DEG C for 15-26 h, and air cooling is carried out; the alloy is treated in a regression mode at the temperature of 150 DEG C-210 DEG C for 2-120 min, and intragranular precipitates are redissoluted into a matrix through water cooling; natural ageing (RT) is carried out for 2-120 h, ageing is carried out at the temperature of 50 DEG C-120 DEG C for 2-90 h, and air cooling is carried out. The low-purity Al-Zn-Mg-Cu alloy comprises, by mass ratio, 5.8-7.5% of Zn, 0.2-0.6% of Mn, 1.7-2.5% of Mg, 1.2-2.0% of Cu, 0.08-0.25% of Cr or 0.05-0.15% of Zr, 0.1-0.6% of Fe, 0.1-0.6% of Si, and balance Al. By means of the four-level ageing technology, the low-purity Al-Zn-Mg-Cu alloy obtains highly-dispersed G.P. region granules and a few eta phase intragranular tissues and therefore has ultra-high strength, good plasticity and fatigue damage resistance.

The invention relates to a multielement seeding combustion explosion type rainfall-increasing and anti-hail rocket. In the rocket, one end of a safety system (2) is connected with a flame bullet seeding catalyst system (1), the other end is connected with the front end of a solid motor (3); the back end of the motor (3) sticks to an empennage; four catalyst seeding holes are evenly distributed in the middle part of a nozzle (5), a plurality of flame bullets (12) are sleeved together to be arranged in a shell (15), safety fuses (16) are arranged in the centre bores of the flame bullets (12), a propelling medicine (13) is filled to one end of each flame bullet (12); a cladding medicine block(9) is filled in the threaded connection section capsule of the shell (15), an ignition medicine package (8) is arranged in the counter bore of the cladding medicine block(9), and the ignition wire of the ignition medicine package passes through the centre bore of the nozzle (5). The invention adopts the flame bullet burning mode that catalyst is burnt and seeded continuously and a plurality of flame bullets are thrown along the parent trajectory, for seeding the catalyst, thus requiring that the flame bullets are thrown reliably and the burning is stable. The flame bullets of the invention adopt casting moulding for structure design, the technology is easy and stable, and the flame bullets are easy for the batch production.

The invention discloses titanium alloy and an annular titanium alloy forge piece forming method. The chemical element content of the titanium alloy comprises, by weight, 7.50%-7.80% of A1, 1.00%-2.00% of Mo, 2.60%-2.80% of Zr, 2.60%-2.80% of Sn, 0.50%-1.50% of W, 0.10%-0.25% of Si, no more than 0.15% of Fe, no more than 0.10% of Cu, no more than 0.10% of Cr, no more than 0.10% of C, no more than 0.15% of O, no more than 0.04% of N, no more than 0.012% of H, and the balance Ti. The annular titanium alloy forge piece forming method comprises the following steps that after the titanium alloy is fed, and blanking is conducted at the temperature 30 DEG C below the phase transformation point; forming is conducted at the temperature 20 DEG C above the phase transformation point, and water cooling is conducted till the allay reaches the indoor temperature; double annealing is conducted on the materials obtained through the above two steps. The annular titanium alloy forge piece has the high-temperature tensile strength which can meet the use conditions and is large in affluence measure at the temperature ranging from 500 DEG C to 550 DEG C and can replace TC 25 to be used for manufacturing compressor parts and the like.

The present invention relates to high-performance high-speed steel, and particularly to a high-hardness high-wear-resistant powder metallurgy high-speed steel which is manufactured according to a power metallurgy method and contains Al. The high-speed steel is composed of C, Si, Cr, Mo, V, W, Nb, Mn, Co, Al, Fe and impurities. The high-speed steel manufactured according to the technical solution has the following advantages: more than 67.5HRC of quenching-tempering hardness, better red hardness and wear resistance, stronger bending strength and lower cost.

The invention belongs to the field of the preparation of metal materials, and particularly relates to an auxiliary semi-continuous casting crystallizer for a low-frequency pulsed magnetic field of magnesium alloy and application thereof. The top of a casing of the crystallizer is provided with an upper cover of the crystallizer, the casing of the crystallizer and the position of a center hole of the upper cover of the crystallizer are provided with an inner sleeve of the crystallizer, a cooling water tank is formed between the casing of the crystallizer and the upper cover of the crystallizer, an excitation coil is arranged in the cooling water tank, the outer side of the casing of the crystallizer is provided with a water inlet communicated with the cooling water tank, and a secondary cooling water spraying hole communicated with the cooling water tank is arranged on the inner sleeve of the crystallizer. The casing and the upper cover of the crystallizer are made of stainless steel, and the inner sleeve of the crystallizer is made of a 4XXX family of aluminum alloy; and moreover, an upper opening of the inner sleeve of the crystallizer is higher than the upper surface of the upper cover, and a horn shape is formed between the upper opening and a lower opening. The auxiliary semi-continuous casting crystallizer for the low-frequency pulsed magnetic field of the magnesium alloyis used for the semi-continuous casting of the magnesium alloy, the forced convection of a melt is generated by utilizing pulsed electromagnetic force generated by the auxiliary semi-continuous casting crystallizer for the low-frequency pulsed magnetic field of the magnesium alloy to act on the melt of the magnesium alloy inside the crystallizer, bulky dendritic crystals are fragmented, the nucleation rate is increased, and the thinning effect of the crystal grains of a semi-continuous cast rod of the magnesium alloy is obvious.

The invention relates to steel for 600MPa-grade high-strength engineering machines and a production method thereof, belonging to the technical field of steel for the engineering machines. The steel comprises the following chemical components by weight percent: C: 0.06-0.09%, Si: 0.15-0.25%, Mn: 1.4-1.6%, P: not more than 0.020%, S: not more than 0.010%, Alt: 0.020-0.060%, Nb: 0.040-0.060%, Ti: 0.09-0.12% and the balance of Fe and inevitable impurities. The steel has no expensive elements such as Mo, V and the like, 2 frames are adopted for rough rolling, and 6 frames are used for finish rolling, thereby carrying out controlled rolling; and 20-group laminar cooling is used for strictly controlling the cooling, and internal stress is eliminated by adopting a temperature-holding pit for slow cooling after being offline, thereby being capable of stably producing a hot rolled coil with excellent toughness and low cost, which has the thickness being 5-16mm, the yield strength being more than 600MPa, the V type Charpy impact energy at -20 DEG C being not less than 40J and is applicable to the field of the engineering machines and the like.

The nano composite catalyst is prepared with silver iodide, magnesium, aluminum, copper iodide, sliver iodate or other superfine particle, combustible component, adhesive, curing agent, plasticizer, cross-linking agent, anti-aging agent, speed regulator, etc. and through kneading, deairing and curing. In combustion or explosion, the nano composite catalyst produces composite AgI-NaCl-AgCl-KCl-CuI-NH4I kernels, which possess great specific surface area, high activity, and structure and crystal lattice constant similar to those of ice crystal. The catalyst has high kernel forming rate, fast kernel forming speed, excellent physical and chemical performance, less environmental pollution and easy maintenance and transportation, and is safe and efficient composite catalyst for rain making, preventing hail, eliminating cloud, and other weather modifications.

The invention discloses a preparation method of a graphene alloy nanocomposite and an SLM (Selective Laser Melting) forming process. According to the preparation method, turbid liquid is prepared through the ultrasonic vibration of anhydrous ethanol, so that the graphene is uniformly dispersed in the anhydrous ethanol, the graphene is uniformly dispersed, then after the graphene anhydrous ethanolturbid liquid is mixed with high-temperature alloy in proportion, the graphene and partial residue are distributed in the grain boundary and crystals by participating in the interfacial reaction, so that the strength and toughness of a formed part are improved, and the hot cracking tendency is reduced; the addition of graphene changes the organization form of the material; and in the SLM forming process, the graphene in the graphene high temperature alloy nanocomposite is used as a heterogeneous nucleating agent, and increases the nucleation rate in the solidification crystallization process.The graphene high temperature alloy nanocomposite is prepared by the dielectric barrier discharge plasma-assisted ball milling technique. The plasma enhances the activity of powder, so that columnar crystals preferentially growing change to isometric crystals, grains are refined and the performances are improved.

An apparatus for preparing the semi-solid molten body of iron and steel is composed of a special container for molten iron or steel, temp regulator, stirrer and bottom vibrator. The linear layer of said special container contains nucleation promoter. Its method includes pouring the molten iron or steel at the temp which is 5-10 deg.C, higher than the temp of liquid-phase line into said special container, and stirring or vibrating for 1-10 min.

The invention discloses a preparation method of aluminium-lithium intermediate alloys, which comprises the following steps: preparing a lithium metal liquid; sending the lithium metal liquid and an aluminium metal liquid into a smelting furnace of a semicontinuous casting machine for mixing; and sending the mixed metal liquid into a crystallizer of the semicontinuous casting machine for casting ingots, wherein the magnetic density in the crystallizer is 0.01-0.05T and the casting temperature is 700-900 DEG C when casting the ingots. The lithium metal liquid and the aluminium metal liquid are together sent into the smelting furnace of the semicontinuous casting machine for mixing, and then an aluminium-lithium intermediate alloy is pulled out from the crystallizer of the semicontinuous casting machine. Under the action of a magnetic field of the crystallizer, low-frequency shock and stable circumfluence of the mixed liquid occur in, a better mixing function can be performed to the lithium metal liquid and the aluminium metal liquid, the nucleation rate is effectively improved, and the aluminium-lithium intermediate alloy with stable quality can be prepared.

The invention provides a method for preparing perfluoropolyether through carrying out ring opening polymerization on tetrafluoro oxetane and the perfluoropolyether thereby. According to the method, the ring opening polymerization of the tetrafluoro oxetane is initiated by using fluoride salt as an initiator and a perfluoropolyether chemical compound F-(OCF2CF2CF2)n-CF2CF3 is collected through controlling the vacuum degree and the distillation temperature, where the n=2-30. The invention provides a method for applying the perfluoropolyether material to a fingerprint-proof membrane for touch screens at the same time. According the method, a buffer layer is formed on a glass substrate after being subjected to O2 glow discharge bombardment and a perfluoropolyether membrane is formed on the upper surface of the buffer layer, wherein the buffer layer is a PECVD (Plasma Enhanced Chemical Vapor Deposition)-deposited SiO2 film. A good adhesive force is provided between the SiO2 buffer layer and the glass substrate through depositing the SiO2 buffer layer by utilizing PECVD, so that the adhesive force between the perfluoropolyether fingerprint-proof membrane and the glass substrate is increased to a certain extent.

The invention discloses a method for controlling electroslag melting casting by an added transient magnetic field. The method includes adding a transient magnetic field to a melting end of an electroslag remelting mother electrode, a liquid slag tank and a metal melting tank so that the transient magnetic field acts on large metal molten drops which are generated by initial melting at the tail end of the electrode and are converging to become big; under joint action of alternating lorentz force and pressure waves generated by the transient magnetic field, dispersing the metal molten drops in a burst manner into small metal molten drop groups, and randomly dispersing the small metal molten drop groups into the liquid slag tank to sufficiently contact with liquid slag after passing the liquid slag tank; after washing, enabling included foreign substances and impurities in the small metal molten drops to enter the liquid slag quickly, slowly settling and converging the foreign substances and impurities into the metal melting tank below the liquid slag tank, and finally crystallizing and solidifying to form solidified cast ingots. The invention further provides an electroslag melting casting device. By adding the transient magnetic field during electroslag melting casting and fining the molten drops by the aid of unique electromagnetic effect of the transient magnetic field, the purposes of improving refining efficiency, fining crystalline grains and reducing segregation of cast ingots are achieved, and industrial application value is realized.

The invention discloses a 420MPa normalizing super-thick steel plate, and a preparation method thereof. The 420MPa normalizing super-thick steel plate comprises following chemical components, by mass, 0.14 to 0.16% of C, 0.30 to 0.40% of Si, 1.0 to 1.60% of Mn, 0.015 to 0.025% of Als, 0.005 to 0.025% of Nb, 0.065 to 0.10% of V, 0.010 to 0.02% of Ti, 0.2 to 0.45% of Ni, 0.05 to 0.30% of Cu, P less than 0.01% , S less than 0.005%, and the balance Fe and unavoidable impurities. The preparation method comprises following steps: continuous casting steel slab, which contains the above chemical components and possesses a thickness of 400mm, is subjected to two stages of rolling without water cooling, is discharged rapidly, and is subjected to stacking slow-cooling for 72h or more; and after steel plate shot blasting, the steel plate is obtained by normalizing plus accelerated cooling heat treatment process. The normalizing 100-120mm steel plate prepared by the preparation method possesses excellent strength and toughness; yield strength is more than 420MPa; and the normalizing 100 -120mm steel plate can be used for preparation of key force support elements of buildings, bridges and tower structures with large span frameworks.

The invention relates to a titanium alloy surface multi-element laser alloyed layer and a preparation method thereof. The preparation method comprises the following steps: by using titanium alloy as a base material, applying mixed powder of B4C, graphite, Ti powder and rare-earth oxides Y2O3 used as a coating material onto the titanium alloy surface, and carrying out laser scanning while blowing nitrogen gas to perform alloying, wherein the coating material comprises the following components in percentage by mass: 10-90% of B4C, 10-90% of graphite powder, 0-50% of Ti powder and 0-4% of Y2O3.In an open N2 environment, the B4C and graphite powder are subjected to boron-carbon-nitrogen multi-element composite laser alloying on the titanium alloy surface to prepare the high-hardness wear-resistant composite ceramic coating. The simultaneous addition of the Ti powder and rare-earth oxides Y2O3 is beneficial to enhancing the microhardness and wear resistance of the alloyed layer; and the proper amount of Ti can promote the in-situ reaction in the alloyed layer, and the Y2O3 can refine the structure, thereby enhancing the comprehensive mechanical properties of the coating.

The invention discloses a quasicrystal-strengthened Mg-6Zn-3Y alloy with an ultrafine solidification texture and a preparation method thereof. The quasicrystal-strengthened Mg-6Zn-3Y alloy consists of the following chemical components in percentage by weight: 87.0 to 93.0 percent of Mg, 3.0 to 10.0 percent of Zn and 0.5 to 3.0 percent of Y. The Mg-6Zn-3Y alloy with the ultrafine solidification texture, which contains nanoscale granular quasicrystals, is prepared from normal-pressure as-cast Mg-Zn-Y alloy material under GPa-level ultrahigh pressure as solidification pressure, temperature and solidification cooling rate are controlled. The as-cast texture is characterized in that: the granular quasicrystals are evenly and dispersely distributed on the ultrafine Alpha-Mg matrix, wherein the secondary dendrite arm spacing between Alpha-Mg dendrites is 7Mu m to 10Mu m, the diameter of the granular quasicrystal is 50nm to 100nm, and the volume of the granular quasicrystals accounts for 25 to 35 percent of the total volume of the alloy. The invention adopts a cubic press, solidification process parameters are controlled, i.e., the solidification pressure is 6GPa, the solidification temperature is 1300DEG C, and the solidification rate is 300K/S. Theultrafin quasicrystal-strengthened Mg-6Zn-3Y alloy has high mechanical properties and good thermal stability.