428 results about "Vacuum induction melting" patented technology

The invention belongs to the technical field of metal material forming, and relates to a high-strength plastic titanium-based composite material annular part and a preparation method and application thereof. The preparation method comprises the following steps: firstly, uniformly mixing titanium alloy powder and reinforced phase powder, then preparing an annular blank according to the technological process of smelting, plasma rotating electrode atomization, degassing seal welding, hot isostatic pressing and ring rolling, and finally, annealing the annular blank to prepare the target annular part. According to the method, the titanium-based composite material powder is prepared by replacing a traditional laboratory small-batch ball milling method with a large-batch mixing method, a vacuum induction melting rod manufacturing method and a plasma rotating electrode atomization method, a reinforced phase can be introduced into a titanium matrix crystal and uniformly distributed, and the method is suitable for industrial large-batch production requirements; the titanium-based composite material annular part is prepared through the technology of powder metallurgy blank making and thermal deformation, and the effects of shortening the machining period and improving the material utilization rate and the forming rate are achieved through the precise size of powder metallurgy forming and the high efficiency of special-shaped ring rolling.

The invention discloses an electric engine assembly integral forming process based on precision integral casting, which comprises the following steps: designing a split type precision mold through computer aided design software, and carrying out nitriding treatment to improve the performance; selecting a specific aluminum alloy raw material, performing vacuum induction melting and refining, and injecting the aluminum alloy raw material into a preheated and sprayed mold cavity in a low-pressure casting manner; and demolding after air cooling and water cooling are combined, then after-treatment procedures such as deburring and heat treatment are conducted, and finally detection and assembly are conducted. A conformal cooling water channel design and an ultrasonic-assisted smelting technology are adopted in the process innovation, and the casting process is monitored in real time. According to the process, manufacturing procedures are reduced, compared with a traditional mode, the production efficiency is improved by 30%-50%, the cost is reduced by 20%-30%, the assembling problem is effectively avoided, the sealing performance and reliability of the electric engine are improved, the service life of the electric engine is prolonged, high integration is achieved, and the modern industrial requirement is met.

The invention relates to the technical field of metal processing, and discloses a production method of an ER2209 austenite ferrite duplex stainless steel welding wire, the ER2209 austenite ferrite duplex stainless steel welding wire comprises an adopted vacuum induction melting furnace and a liquid storage tank, the outer side of the vacuum induction melting furnace is provided with a protective shell, one side of the liquid storage tank is fixedly connected with a conveying pump, and the other side of the liquid storage tank is fixedly connected with a vacuum pump. A cooling assembly is arranged in the protective shell. The preparation method comprises the following steps that S1, raw materials are prepared and smelted; s2, cooling the vacuum induction melting furnace; s3, forging is conducted; s4, hot rolling and solution treatment; s5, acid pickling and surface treatment; s6, cold drawing and intermediate annealing; s7, surface copper plating and finish drawing; and S8, winding and packaging. In the acid pickling process of the wire rod, the oxidation degree of the wire rod is detected, meanwhile, the concentration of the acid pickling solution is adjusted according to the actual situation, and the situation that the surface of the wire rod is excessively corroded or is not thoroughly cleaned due to the fact that the concentration of the acid pickling solution is improper is prevented.

The invention provides a directional solidification preparation method of a degradable high-hardness zinc alloy material. The preparation method of the zinc alloy material comprises the machining processes of vacuum induction melting, vacuum directional solidification melting and the like, through the preparation method, growth of Zn + Mg2Zn11 trilobal eutectic and Zn + MgZn2 spiral eutectic is regulated and controlled, microscopic structures are arranged in the specific direction, fine and uniform structure morphology is formed, and the corrosion resistance and the mechanical property of the alloy are improved. The Zn-Mg series alloy prepared by the preparation method disclosed by the invention shows excellent microhardness (181.19 to 243.10 HV). Besides, the corrosion rate of the ideal degradable bone implant is within the range of 0.1 mm / y to 0.5 mm / y, and the corrosion rate of the degradable medical Zn-Mg alloy bone implant material is within the range of 0.0316 mm / y to 0.2280 mm / y, so that the requirement on the corrosion rate in the bone repair process is met; and after the Cu element is added on the basis of Zn-3% Mg, the microhardness of the Zn-3% Mg-Cu-Cu alloy material is improved to about 200HV, and the advantages in the aspect of mechanical support are improved.

The invention discloses a pickling-free cold heading Kovar alloy wire production process which comprises the following steps: S1, raw material preparation: preparing the following raw materials in percentage by mass: 41.5% of Ni, 0.5% of Co, less than or equal to 0.03% of C, less than or equal to 0.05% of Mn, less than or equal to 0.05% of Si, less than or equal to 0.02% of P, less than or equal to 0.02% of S and the balance of Fe; mixing the materials, and carrying out vacuum induction melting and electroslag remelting to prepare an alloy ingot; the alloy cast ingot is subjected to hot rolling treatment to form a hot-rolled wire rod with the diameter being 12.0-16.0 mm; s2, peeling treatment is conducted, specifically, surface layer defects of the hot-rolled wire rod in the step S1 are removed through a peeling machine; s3, dry-type drawing treatment is conducted, specifically, the hot-rolled wire rod treated in the step S2 is subjected to dry-type drawing through a dry-type drawing die to form an alloy wire; s4, intermediate annealing treatment is conducted, specifically, the alloy wire in the step S3 is placed in an annealing furnace, sufficient hydrogen is input into the annealing furnace, intermediate annealing is conducted under the hydrogen protection atmosphere, the annealing temperature is 950-1100 DEG C, and the annealing walking speed is 3-5 m / min; the surface quality and the size consistency of the wire can be improved, meanwhile, the defects of environmental pollution, hydrogen embrittlement and the like are reduced, and the use requirements of high-end precise cold heading parts are met.

The invention belongs to the technical field of high-temperature alloy heat treatment, and discloses a method for improving the hot working performance of a nickel-based high-temperature alloy for a molten salt reactor by combining pre-deformation and homogenization. The method comprises the steps that raw materials of the nickel-based superalloy for the molten salt reactor to be improved are sequentially subjected to vacuum induction melting, pouring and electroslag remelting refining treatment, and an electroslag remelting refined alloy cast ingot is obtained; the electroslag remelting refined alloy cast ingot is sequentially subjected to heating, heat preservation and pre-deformation treatment and is air-cooled to the room temperature, and a pre-deformed cast ingot is obtained; and the pre-deformed cast ingot is subjected to homogenization treatment and air cooling to the room temperature, and the method is completed. The method is a novel heat treatment process combining pre-deformation and high-temperature homogenization, the hot working performance of the alloy is optimized, the high-temperature alloy uniform in structure and excellent in mechanical property is obtained, and application in the field of high-temperature molten salt energy systems is met.

The invention belongs to the technical field of vacuum centrifugal casting and vacuum induction melting, and particularly relates to a complex thin-wall casting vacuum induction remelting pouring temperature gradient control device and method, and the device comprises a calculation system, a temperature measurement mechanism, a rapid induction remelting mechanism and a bottom pouring crucible; the calculation system is used for achieving simulation calculation of rapid induction remelting and bottom pouring of the alloy ingot, and the temperature measuring mechanism outputting target remelting characteristic parameters is used for measuring temperature changes and temperature gradient distribution of the top, the middle and the bottom of the alloy ingot in the remelting process in real time. The rapid induction remelting mechanism is used for melting the alloy ingots and achieving the melting sequence of the alloy ingots from top to bottom and from outside to inside. By means of the high-temperature alloy remelting device, the problem that in the high-temperature alloy remelting process, due to the fact that the temperature gradient is disordered, alloy is completely melted or part of alloy liquid flows out from the bottom firstly is effectively solved, and casting defects are reduced.

The invention discloses a smelting method of a large-size Fe-based high-temperature alloy for a gas turbine. The smelting method comprises the following two steps: casting a metal raw material into a 710mm electrode bar through a vacuum induction furnace, and then feeding the electrode bar into a consumable electrode vacuum furnace for remelting to produce a 810mm steel ingot. According to the method, the vacuum induction melting and vacuum consumable remelting (VIM and VAR) combined process is adopted for smelting, so that the burning loss of the Ti element can be effectively controlled to ensure that the content of the Ti element reaches the standard, excessive generation of Ti-series carbonitride can be avoided, and the negative influence on the purity of the molten steel is fundamentally avoided.

The present application relates to high-temperature alloy smelting technical field, specifically relates to a kind of high-aluminum titanium cast nickel-based high-temperature alloy purification smelting method.The pure smelting method, step one, low calcium nickel alloy preparation;Step two, pure smelting: batching and furnace charging, melting period, refining period, alloying period, calcium treatment purification period and casting period;Pure smelting process is carried out in vacuum induction melting furnace, 2 / 3 low calcium nickel alloy is directly loaded into magnesium oxide crucible when furnace charging, and the remaining 1 / 3 low calcium nickel alloy is added in calcium treatment purification period.The present application prepares a kind of component accurately controllable "low calcium nickel alloy" as master alloy by pre-preparation, is added in key smelting stage, solves the problem of calcium element direct addition, realizes the deep deoxidation denitrogenation desulfurization of alloy melt, significantly reduces the oxygen, nitrogen, sulfur impurity content in alloy, to improve the purity and comprehensive mechanical properties of alloy.

The invention discloses a method for reducing impurity element sulfur in cast high-temperature alloy return scraps, and belongs to the technical field of metal material smelting. The method comprises the following steps: carrying out vacuum induction melting on pretreated cast high-temperature alloy return scraps of the same mark to obtain a return scrap alloy induction ingot; surface oxide skin of the obtained return scrap alloy induction ingot is removed, a primary shrinkage cavity in the upper end is cut off, then the return scrap alloy induction ingot and an auxiliary electrode are coaxially welded, and a consumable electrode is obtained; and after the consumable electrode is baked, electroslag remelting is conducted under the protective atmosphere, and an electroslag ingot is obtained. On the basis of vacuum induction melting, the protective atmosphere electroslag remelting technology is further adopted for conducting deep purification melting treatment on the return scrap alloy ingot, the content of the impurity element S in the return scrap alloy ingot can be reduced to 0.5 ppm or below, and the content of the impurity element S in the return scrap alloy ingot reaches the level lower than the content of the element S in a new material; and the high-temperature oxidation resistance and corrosion resistance of the alloy can be obviously improved, and the fatigue, durability and other mechanical properties of the alloy are improved.

The invention provides a preparation method of a GH706 high-temperature alloy large-size bar billet, which comprises the following five steps: (1) a GH706 high-temperature alloy ingot prepared by a triple smelting process of vacuum induction melting, protective atmosphere electroslag remelting and vacuum consumable remelting comprises the following chemical components in percentage by weight: 0.025%-0.060% of C, 14.50%-17.50% of Cr, 39.00%-44.00% of Ni, 1.50%-2.00% of Ti, 2.50%-3.30% of Nb + Ta, 0.15%-0.50% of Al and the balance of Fe and inevitable impurities; the balance is Fe and other micro trace elements; (2) high-temperature homogenization treatment; (3) cogging and forging: carrying out high-temperature cogging and forging on the cast ingot for 2-3 heating numbers, wherein the forging modes are upsetting and drawing-out; (4) intermediate billet forging: performing medium-temperature multi-heating-number upsetting and octagonal drawing on the intermediate billet subjected to cogging forging; according to the preparation method of the GH706 high-temperature alloy large-size bar billet, the technical problem that the structure uniformity is difficult to control due to end face cracking, low forging yield and severe temperature rise in the cogging process of a large-size cast ingot is solved, and the preparation method has high application value in industrial actual production.

The invention discloses a vacuum induction melting furnace for alloy melting, and relates to the technical field of melting furnaces. The vacuum induction smelting furnace for alloy smelting comprises a smelting furnace body, a heating unit, a crucible, a bottom support, a mold base, a vacuum control unit, a feeding unit, a discharging control unit and a proportional control mechanism. According to the smelting furnace, the feeding unit is additionally arranged on the smelting furnace main body, the feeding unit is convenient for storing various raw materials and controlling discharging, the tedious operation of opening the furnace for adding the raw materials for many times is avoided, time and labor are saved, alloy smelting can be continuously and stably carried out, the discharging amount of the two raw materials is controlled through the design of the discharging control unit and the proportion control mechanism, and the smelting efficiency is improved. Quantitative supply is achieved, the discharging proportion of the two raw materials is accurately controlled through the proportion control mechanism, operation is easy and convenient, errors are not prone to occurring, the requirement for accurate proportion of different alloy components can be met, and stability and consistency of alloy quality are guaranteed.

A vacuum induction melting (VIM) furnace and method of using. A VIM is configured for use with metal-containing carbon powders. In operation, the metal-containing carbon powders are formed into a pellet so as to minimize or eliminate ejection of material during introduction of the pellet into the VIM processor. The VIM processor may be substituted or used in combination with a vacuum arc melt processing apparatus, an electron beam melt furnace, an ion plating furnace, a plasma flame source, a smelter, a traditional metal-metal melt furnace, or any equivalent. Pelletizing can be accomplished through use of a press or through application of any pelletizing technique and / or use of any apparatus that is able to generate pellets that have sufficient mass to avoid ejection from a VIM processor.

The invention discloses a preparation device of a titanium hydrogen storage alloy for solid hydrogen storage, which comprises a vacuum induction melting system and an ultrasonic generation system, the vacuum induction melting system comprises a vacuum chamber, a melting mechanism and a heatable mold which are arranged in the vacuum chamber, and a vacuum pump communicated with the vacuum chamber; the ultrasonic generation system comprises an ultrasonic generator, an amplitude-change pole and an ultrasonic probe which are connected in sequence, one end of the ultrasonic probe extends into the vacuum chamber, and a mobile positioning system for controlling the position of the ultrasonic probe is arranged on the vacuum induction melting system; the invention further discloses a preparation method of the titanium hydrogen storage alloy for solid hydrogen storage. According to the device, the ultrasonic generation system is arranged, ultrasonic waves are applied in the raw material smelting process, segregation of the Ti element is effectively restrained, meanwhile, dendritic crystal arms are broken in the alloy solidification process, more nucleation sites are formed to refine grains, and the device is suitable for preparing the titanium hydrogen storage alloy for solid hydrogen storage.

The invention provides a micron-sized beryllium powder preparation method based on a gas atomization method, and particularly relates to the technical field of metal powder material preparation. The preparation method provided by the invention comprises the following steps: (1) melting raw materials, namely putting a high-purity beryllium ingot with the purity of more than or equal to 99.9% into a vacuum induction melting furnace, vacuumizing until the pressure is less than or equal to 1 * 10 <-3 > Pa, filling inert gas, heating to 1300-1400 DEG C, and keeping the temperature for 10-30 minutes until the superheat degree of beryllium liquid reaches 50-100 DEG C; (2) gas atomization treatment: spraying beryllium liquid through a supersonic nozzle, crushing liquid beryllium into fine liquid drops by using atomized gas, and solidifying the fine liquid drops into powder; (3) multiple layers of cyclone separators connected in series are arranged, parameters are adjusted step by step, and powder with different particle sizes is sequentially collected in a graded mode; and the powder with the target particle size is sealed and packaged after vacuum drying. According to the method, secondary screening can be effectively avoided, continuous production can be achieved, and the obtained micron-sized beryllium powder is controllable in particle size, high in sphericity degree and low in oxygen content.

The application belongs to the field of high-entropy alloys, and particularly relates to a preparation method of an ultra-high strength and plasticity product Fe50Mn30Co10Cr10 alloy. Firstly, a cast slab is prepared through vacuum induction melting, then the cast slab is subjected to multi-pass hot rolling with a reduction ratio of 70% to 75%, and after pickling, the cast slab is subjected to multi-pass warm rolling with a reduction ratio of 80%, and finally, high-temperature short-time annealing is carried out at 1050 to 1150 DEG C to obtain a final annealing plate. In the application, the phase transformation behavior in the alloy deformation process is inhibited by controlling the hot rolling and warm rolling temperatures, and the rolling plasticity of the material is improved. Meanwhile, by optimizing the annealing process, the grains are refined as much as possible, and a certain dislocation density is retained, and the strength and plasticity of the alloy are improved through the comprehensive action of multiple strengthening mechanisms. The prepared Fe50Mn30Co10Cr10 alloy has a tensile strength of 1050 to 1280 MPa, an elongation of 35% to 58%, and a strength and plasticity product of 40 to 73 GPa.

The invention belongs to the field of ultra-pure smelting processes of high-performance Cr-Ni-W series high-strength steel, and particularly relates to an ultra-pure smelting method of high-performance Cr-Ni-W shaft steel and the high-performance Cr-Ni-W shaft steel. According to the method, vacuum induction melting is adopted, furnace charge is heated and melted in a magnetic induction mode, the whole melting process is completed in vacuum, and no slag participates in the metallurgy process. The smelting mode has a good effect of removing gas and non-ferrous metal impurities, and alloy elements are basically not burnt. In the vacuum consumable remelting process, inclusion particles float to the surface of a molten pool and are gradually adsorbed by the wall of a crucible under the action of an electric arc, so that the inclusion content in the alloy can be further reduced, and the purity of a cast ingot is improved; and meanwhile, reasonable cooperation of current and voltage, melting speed and cooling is adopted in the melting process, and the component and structure uniformity of Cr-Ni-W series high-strength steel finished product cast ingots is guaranteed.

The invention discloses a novel desulfurization process in a vacuum induction melting process. According to the technical scheme, the method comprises the steps that an alloy material is dissolved and clarified, after the pressure of a furnace chamber is smaller than 10 Pa, the temperature of molten steel is increased to 60-150 DEG C above the alloy melting point for refining, and sampling is conducted every 10-30 min in the refining process till the content of oxygen and nitrogen in the molten steel is smaller than 20 ppm; then, the temperature of the molten steel is maintained to be 60-80 DEG C above the alloy melting point, after a furnace chamber is filled with argon to 10000 Pa, 0.5-5% of a Ca element additive is added into the molten steel, and the high binding force of the Ca element and the S element is utilized; the invention has the following beneficial effects: the desulfurization characteristics of Ca element and rare earth element are used; the sulfur element in the molten steel is removed in the mode that Ca is firstly used for desulfurization and then rare earth elements are used for desulfurization, and the content of the S element in the molten steel can be reduced to 10 ppm or below.

The invention discloses an amorphous nanocrystalline magnetic material production method, which relates to the technical field of amorphous nanocrystalline, and comprises the following operation steps: S1, material preparation; s2, alloy smelting, wherein the prepared raw materials are added into a vacuum induction smelting furnace according to a specific proportion; s3, single-roller rapid quenching strip manufacturing is conducted, specifically, smelted alloy liquid flows out through a nozzle at the bottom of the vacuum induction smelting furnace and is sprayed to the surface of a copper roller rotating at a high speed, and the alloy liquid is solidified into a thin strip; s4, nano-crystallization treatment: putting the prepared amorphous ribbon into a vacuum annealing furnace for annealing treatment; s5, magnetic field heat treatment, wherein after annealing treatment, the thin strip is placed in a high-intensity magnetic field environment to be subjected to heat treatment again; and S6, forming processing: winding the thin strip into an inductance coil by using a winding device. According to the production method of the amorphous and nanocrystalline magnetic material, the operation steps are simpler, the production efficiency of amorphous and nanocrystalline is higher, and the quality of the material is better.

The application belongs to the technical field of metal material forming, and relates to a high-strength plastic titanium-based composite material ring-shaped piece and a preparation method and application thereof. The preparation method comprises the following steps: uniformly mixing titanium alloy powder and reinforcing phase powder, preparing a ring-shaped blank according to a process flow of "melting -> plasma rotating electrode atomization -> degassing and sealing welding -> hot isostatic pressing -> ring rolling", and finally performing annealing treatment on the ring-shaped blank to obtain a target ring-shaped piece. The application replaces the traditional laboratory small-batch ball milling method for preparing titanium-based composite material powder by using "large-batch mixing + vacuum induction melting rod preparation + plasma rotating electrode atomization method", so that the reinforcing phase can be introduced into the titanium matrix crystal and uniformly distributed, and the application is suitable for industrialized mass production requirements. The titanium-based composite material ring-shaped piece is prepared through the "powder metallurgy blank preparation + hot deformation" process, the size accuracy of powder metallurgy forming and the high efficiency of special-shaped ring rolling are utilized to achieve the effects of reducing the processing period, improving the material utilization rate and the forming rate.

The invention discloses a PdAgCuMt alloy and a three-dimensional nano material prepared on the basis of the PdAgCuMt alloy. The PdAgCuMt alloy comprises the following alloy components: 38-42 wt% of Pd, 26-30 wt% of Ag, 28-32 wt% of Cu, 1-2 wt% of Mt (Mt is a combination of any two of three elements of In, Zn and Al) and inevitable impurities. The alloy is prepared according to the proportion and then placed in a vacuum induction melting furnace, an alloy blank is prepared after refining, and bulk materials, bars, wires and strips with nanocrystalline can be prepared on the basis of the alloy blank through forging, rolling, drawing, heat treatment and other processes. The alloy can be used for manufacturing a metal three-dimensional nano material, the grain size of the metal three-dimensional nano material ranges from 3 nm to 10 nm, and the metal three-dimensional nano material has the characteristics of high strength, high hardness, high elasticity, high corrosion resistance and precise resistance.

The invention relates to the technical field of intermediate alloy metal materials, and provides a low-nitrogen vanadium-aluminum intermediate alloy and a preparation method thereof, and the low-nitrogen vanadium-aluminum intermediate alloy comprises the following components: 40-68 wt% of V, 0.001-0.003 wt% of N, and the balance of Al and inevitable impurities. The preparation method comprises the following steps: uniformly mixing raw materials of vanadium pentoxide powder and aluminum shots, charging the mixture into a furnace, carrying out exothermic smelting outside the furnace to obtain a vanadium-aluminum intermediate alloy semi-finished product, uniformly mixing potassium fluotitanate and nano carbon powder, putting the mixture as a grate-layer material at the bottom of a corundum crucible, charging the vanadium-aluminum intermediate alloy semi-finished product and the aluminum shots, and carrying out vacuum induction smelting, and the low-nitrogen vanadium-aluminum intermediate alloy is obtained. According to the preparation method provided by the invention, not only is the content of impurity nitrogen in the produced vanadium-aluminum intermediate alloy low, but also the production cost required by nitrogen removal is low.

The invention provides a corrosion-resistant iron-based amorphous material suitable for ultrahigh-speed laser cladding and a preparation method of the corrosion-resistant iron-based amorphous material. The corrosion-resistant iron-based amorphous material is characterized in that an iron-based amorphous coating comprises the following components in percentage by weight: 27-29 wt% of Cr, 2-3 wt% of Co, 1-3 wt% of Nb, 3-5 wt% of Mo, 5-8 wt% of Ce, 3.6-3.8 wt% of B, 4.3-4.5 wt% of Si, 0.7-0.9 wt% of C and the balance of Fe. Amorphous alloy powder is prepared by combining vacuum induction melting with a gas atomization powder preparation technology, a coating is prepared on the surface of a base body by adopting an ultra-high-speed laser cladding technology, the coating has high amorphous content and excellent corrosion resistance, and meanwhile, low porosity (llt) is achieved through the ultra-high-speed laser cladding technology; the coating has the advantages of high hardness (greater than or equal to 800HV) and strong bonding strength (greater than or equal to 70MPa), prolongs the service life of maritime work equipment in a marine environment, is suitable for industrial popularization, is suitable for surface protection of marine equipment, chemical equipment and other severe environments, and has the advantages of efficient process, environmental protection, low cost and strong corrosion resistance.

The present invention relates to a fabrication method for cobalt wire for a self-powered neutron-sensitive element. The cobalt wire fabrication method comprises the following steps: (1) cobalt powder reduction treatment; (2) mixing and compression molding; (3) vacuum induction melting; (4) forging, rotary swaging, and drawing; and (5) electrolytic polishing and annealing. Adopting the method described above allows for the fabrication of cobalt wire with a diameter of 1.00 mm-2.00 mm and having a purity greater than or equal to 99.95%, and the content of radiation-intolerant impurity elements (boron, cadmium, chromium, copper, and silicon) present in the cobalt wire is less than or equal to 30 ppm per element. The cobalt wire has an ovality precision of + / -0.003 mm, with a surface roughness less than or equal to Ra1.6 μm, a tensile strength greater than or equal to 900 MPa, and an elongation greater than or equal to 6%.

The invention discloses a preparation method of a novel low-alloy steel solid welding wire. The preparation method comprises the following steps of S1, raw material smelting, S2, a hot working stage, S3, a cold working stage, S4, surface treatment and S5, quality detection. During raw material selection, C-Mn-Si is adopted as a basic alloy, the content of C is 0.06-0.12%, the content of Mn is 1.2-1.6%, then a Ti-B microalloy is added, the hardenability is improved, the O / N content is limited at the same time, then a two-stage refining process combining vacuum induction melting and electroslag remelting is adopted, the melting temperature, time and refining slag system components are regulated and controlled, and the hardness of the alloy is improved. The method comprises the following steps: preparing a copper plating solution through equipment, deeply removing harmful impurities such as S and P, promoting floating and size refinement of inclusions by applying an electromagnetic stirring technology, remarkably improving the purity of a metal matrix, thereby improving the purity of raw material smelting, proportioning the copper plating solution through the equipment, setting the parameters of the copper plating equipment to be 10-15A / dm in current density and 2-3mu m in plating thickness, and carrying out a copper plating process on a welding wire.

The application relates to the technical field of aluminum bronze material, in particular to a high-hardness aluminum bronze material and a preparation method thereof. The application comprises the following steps S1: raw materials are put into a vacuum induction melting furnace, smelting is carried out at 1250-1350 DEG C, alloy liquid is obtained; the alloy liquid is continuously cast at 1150-1300 DEG C, a cast ingot is obtained; the cast ingot is extruded to form an aluminum bronze material; step S2: after the aluminum bronze material is polished, polished, cleaned and dried, a primer material is synchronously fed to a dry aluminum bronze material in a magnetic field assisted laser cladding mode to obtain a primer layer; step S3: a wear-resistant material is synchronously fed to the primer layer in a magnetic field assisted laser cladding mode to obtain a wear-resistant layer, and tempering is carried out to obtain the high-hardness aluminum bronze material.

The invention discloses a V-Ti-Ni shape memory alloy with high elasticity modulus and high hardness and a preparation method of the V-Ti-Ni shape memory alloy. The preparation method comprises the steps of raw material proportioning, V-Ni pre-alloy smelting, vacuum induction smelting and argon protection pouring, multi-pass hot forging and hot rolling and fine cold drawing, and particularly, 7-9 at% of vanadium element is introduced, so that the diameter phi of the prepared V-Ti-Ni shape memory alloy wire is 0.10-0.50 mm. According to the V-Ti-Ni shape memory alloy prepared through the method, the elasticity modulus at the room temperature reaches 100-110 GPa, the microhardness is 320-360 HV, the phase transition temperature regulation and control range of the NiTi-based shape memory alloy is widened, and the structural rigidity, abrasive resistance, plasticity and cycle stability of the V-Ti-Ni shape memory alloy material are remarkably improved. The V-Ti-Ni shape memory alloy prepared through the method is mature in process route, can be produced in batches and is suitable for precise elastic components in medical instruments, micro electro mechanical systems, thermal actuators and spaceflight structures.

The invention relates to a preparation method of a nickel-based alloy for a high-temperature ultrahigh-pressure reaction kettle, which comprises the following steps of: preparing a high-quality and high-purity nickel-based high-temperature alloy ingot by adopting a triple smelting process of (1) vacuum induction melting, (2) electroslag remelting and (3) vacuum consumable remelting; (4) homogenizing heat treatment is conducted, specifically, heat preservation is conducted for 24-48 h at the temperature of 1100- 5) hot working: keeping the temperature of the cast ingot at 980-1150 DEG C for 2-6 hours, and forging the cast ingot into a finished forge piece; and (6) heat treatment is conducted, specifically, after solution treatment is conducted on the forged piece at the temperature of 920-1050 DEG C, stabilization treatment is conducted at the temperature of 810-860 DEG C, heat preservation is conducted for 8-12 h at the temperature of 720-760 DEG C, then furnace cooling is conducted to the temperature of 620-650 DEG C, heat preservation is conducted for 8-12 h, by the adoption of the method, the purity and quality of the alloy cast ingot can be remarkably improved, precipitation of harmful phases is reduced, the structure performance of the alloy forged piece is optimized, the reliability and using performance of the alloy forged piece for the reaction kettle are improved, and the reaction kettle can be used for a long time under the high-temperature and ultrahigh-pressure complex working conditions.

The present invention discloses a copper-iron-chromium-nickel quaternary alloy planar sputtering target and a preparation method thereof. The preparation method comprises at least a vacuum induction melting and casting step: copper, iron, chromium, and nickel raw materials are placed in a vacuum induction melting furnace according to a preset mass ratio to form a shaped target material, wherein the shaped target material has a relative density of not less than 99%. Since the shaped target material is melted in the vacuum induction melting furnace, the copper, iron, chromium, and nickel raw materials disclosed in the present invention can be fully fused in the vacuum induction melting furnace. Moreover, since the copper-iron alloy has good electrical and thermal conductivity, high mechanical strength, and wear resistance, the addition of chromium can further improve the corrosion resistance and mechanical properties of the alloy. The addition of nickel can fully cooperate with chromium to transform the metallographic structure from a single-phase ferrite to a two-phase structure of austenite and ferrite, thereby effectively improving the corrosion resistance and mechanical properties of the alloy target material.