The invention relates to the technical field of
nickel-based
powder, in particular to a preparation method and a preparation device of nano
nickel-based
powder, and the preparation method comprises the following steps: A, uniformly mixing
nickel salt, a
reducing agent, an additive and a
solvent, and adjusting the pH value to 8-12 to obtain a precursor solution; b, the precursor solution is subjected to a reaction for 10-60 s and 10-60 min in a
nucleation temperature section and a growth temperature section in sequence respectively, and then is frozen for 5-20 min in a freezing temperature section, and a nano nickel-based particle mixture is obtained; wherein the temperature of the
nucleation temperature section is higher than that of the growth temperature section, and the temperature of the growth temperature section is higher than that of the freezing temperature section; and C, sequentially separating, washing and
drying the nano nickel-based particle mixture to obtain the nano nickel-based
powder. According to the preparation method of the nano nickel-based powder and the preparation device of the nano nickel-based powder, on the premise that the production cost is reduced, it is guaranteed that the size uniformity,
dispersity and morphology of the nano nickel-based powder are controllable.