Composition for sealing semiconductor, semiconductor device, and process for producing semiconductor device
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[0201]A polyethyleneimine aqueous solution 1 (PEI, manufactured by BASF SE, weight-average molecular weight: 25,000, 250 mg / 100 mL, pH: 10.52, cationic functional group equivalent weight: 309) was made to contact the interlayer dielectric layer obtained in the above process (hereinafter, also referred as “low-k”) using a commercially available spraying bottle (AIR-BOY, manufactured by Carl Roth GmbH) by a spraying method (solution contact time: 20 sec, spraying distance: 10 cm). Next, water was made to contact the interlayer dielectric layer using a similar spraying bottle by a spraying method (contact time with ultrapure water: 10 sec, spraying distance: 10 cm). After drying by air blowing, a resin layer was formed on the interlayer dielectric layer. After being stored in a constant-temperature and constant-humidity environment of 23° C. and 55% for 15 hours or longer, the sample (low-k / PEI) was subjected to the following evaluation.
[0202]The water used in the above process was ult...
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