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Method for inspecting Chinese-medicinal preparation Kaiyinwan

A quality inspection method and technology of traditional Chinese medicine preparations, applied in the direction of measuring devices, preparation of test samples, instruments, etc., can solve problems such as the complexity of traditional Chinese medicine ingredients, and achieve the effect of improving the accuracy of content detection

Active Publication Date: 2008-11-12
XIAN BEILIN PHARMA
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the composition of traditional Chinese medicine is relatively complex and contains many unknown ingredients
At present, there is no report of a detection method that can effectively control the product quality of traditional Chinese medicine preparations for the treatment of eye diseases, myopia and visual fatigue, and can be operated conveniently.

Method used

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  • Method for inspecting Chinese-medicinal preparation Kaiyinwan

Examples

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Effect test

Embodiment 1

[0014] Honeysuckle, Forsythia, Scrophulariaceae, Banlangen, Radix Paeoniae Rubra, Scutellaria baicalensis, mulberry leaves, chrysanthemum, Peucedanum, bitter almond (fire single), burdock, Alisma, fat sea, silkworm (stir-fried with bran), cicada slough, wood Butterfly sixteen herbs, crushed into fine powder, sieved, and mixed; for every 100g of powder, add 35-50g of refined honey and an appropriate amount of water, make pills, dry, and coat with activated carbon to make honeyed water pills. The detection methods include: The following steps:

[0015] (1) Take 5g of honeydew pills of this product, grind them; add 4g of diatomaceous earth, grind well; add 40ml of methanol, ultrasonicate for 30 minutes, filter, evaporate the filtrate to dryness, add 20ml of water to dissolve the residue, and adjust the pH value with dilute hydrochloric acid To about 2, shake and extract twice with ethyl acetate, 20ml each time, combine the extracts, evaporate to dryness; add 1ml methanol to the r...

Embodiment 2

[0023] Honeysuckle, Forsythia, Scrophulariaceae, Banlangen, Radix Paeoniae Rubra, Scutellaria baicalensis, mulberry leaves, chrysanthemum, Peucedanum, bitter almond (fire single), burdock, Alisma, fat sea, silkworm (stir-fried with bran), cicada slough, wood Butterfly sixteen herbs are crushed into fine powder, sieved, and mixed; every 100g of powder or 110g~130g of refined honey is added to make large honeyed pills. The detection method includes the following steps:

[0024] (1) Take 8g of large honeyed pills, cut them into pieces, add 4g of diatomaceous earth, grind well; add 40ml of methanol, ultrasonicate for 30 minutes, filter, evaporate the filtrate to dryness, add 20ml of water to dissolve the residue, and adjust the pH value to About 2, shake and extract twice with ethyl acetate, 20ml each time, combine the extracts, evaporate to dryness; add 1ml methanol to the residue to dissolve, and use it as the test solution; take another baicalin reference substance, add methanol...

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Abstract

A method for detecting quality of Chinese medicine preparation for curing laryngeal disease utilizes proper solvent and optimum prepared test sample to carry out effective qualitative analysis on radix scutellariae glucoside and great burdock glucoside. The method for detecting content of Chinese herbaceous peony glucoside is also disclosed.

Description

1. Technical field: [0001] The invention relates to a quality detection method, in particular to a quality detection method of a traditional Chinese medicine preparation, Jinsang Kaiyin Pills, which belongs to the field of traditional Chinese medicines. 2. Background technology: [0002] The compound traditional Chinese medicine preparation made of honeysuckle, forsythia, isatidis, scutellaria baicalensis, etc. Jinsang Kaiyin pills, honeysuckle and forsythia evacuate wind-heat, clear away heat and detoxify, reduce swelling and relieve throat, and are the king medicine. Banlangen and Scutellaria baicalensis clear away heat and relieve fire, cool blood and detoxify, relieve swelling and sore throat; Mulberry leaves, chrysanthemum, fat sea, burdock, cicada slough clear away wind and heat, reduce phlegm and detoxify, reduce swelling and relieve throat; Peucedanum, silkworm, bitter almond clear heat Resolving phlegm, dispelling stagnation and relieving sore throat, these ten flav...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): G01N30/90G01N1/28G01N30/02
Inventor 黄小华付彬张浩雒西萍
Owner XIAN BEILIN PHARMA
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