Method and device for temperature calibration by means of benzoic acid freezing point temperature level ground
A technology of benzoic acid and freezing point, which is applied in the field of measurement, can solve the problems that the uniformity and fluctuation of the temperature field have a great influence on the calibration results, the temperature field of the constant temperature bath has a great influence on the calibration results, and mercury is not easy to handle mercury vapor, etc. Achieve good stability and reproducibility, improve temperature field accuracy, and eliminate uniformity
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Embodiment 1
[0036] The method that utilizes benzoic acid freezing point temperature plateau to carry out temperature calibration at 122 ℃, comprises the following steps:
[0037] (1) Production of benzoic acid freezing point bottle:
[0038] The inner wall of the benzoic acid freezing point container is washed successively with organic solvent, lye, dilute nitric acid, and three times of purified water, and dried; the benzoic acid with a purity of 99.98% purified by physical sublimation is put into the above-mentioned container and vacuumized Then close the container. After the benzoic acid freezing point bottle is made, it can be used repeatedly, the number of times is more than 300 times, and the service life is more than 1 year.
[0039] After the above-mentioned purified benzoic acid is loaded into the benzoic acid freezing point container, it is the benzoic acid freezing point bottle.
[0040] (2) Temperature calibration:
[0041] Place the benzoic acid freezing point container in...
Embodiment 2
[0049] In the equipment utilizing benzoic acid freezing point temperature plateau for temperature calibration of the present invention, the volume of benzoic acid freezing point bottle 5 is about 300mL, and the depth of thermometer well 2 is 200mm. It needs to be washed with organic solvent, dilute nitric acid, and three times of purified water in sequence, and dried in a drying oven. Put in benzoic acid with a purity of 99.8% after being purified by methods such as physical sublimation. After vacuuming, the container is sealed.
[0050]The temperature control range of the benzoic acid freezing point reproduction storage device 6 is from room temperature to 250°C, the temperature uniformity is ≤0.01°C, and the temperature fluctuation is ≤±0.01°C / 10min. With programmable program temperature control function, with temperature fluctuation display, continuous working time display, upper and lower limit temperature setting, temperature arrival buzzer alarm and other functions, equi...
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