Method for judging heavy metal detection type of portable X-ray fluorescence spectrometry

A technology of fluorescence spectroscopy and heavy metals, which is applied in the evaluation field of rapid detection data of heavy metal content in soil, can solve the problems of incompleteness, standardization, imperfect methods and complex sample composition, etc.

Inactive Publication Date: 2017-05-24
HUATIAN ENG & TECH CORP MCC +1
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Problems solved by technology

Through the miniaturization of the instrument, the application of portable X-ray fluorescence spectrometry (PXRF) detection in the monitoring of heavy metal pollution in soil is in the ascendant, but the method is not yet perfect
Compared with alloys and plastics, the sample composition of soil is more complex, and the physical state of the sample and the matrix composed of elements other than the analyzed elements have great interference on the

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  • Method for judging heavy metal detection type of portable X-ray fluorescence spectrometry
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  • Method for judging heavy metal detection type of portable X-ray fluorescence spectrometry

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Embodiment Construction

[0026] The present invention will be further described below in conjunction with the accompanying drawings.

[0027] A kind of portable X-ray fluorescence spectrometry heavy metal detection type judgment method of the present invention comprises the following steps: step (1): use portable X-ray fluorescence spectrometry and standard method to measure the heavy metal content in the soil respectively and obtain rapid measurement value and standard method measurement value;

[0028] Step (2): Calculate the evaluation parameters according to the rapid measurement value of the heavy metal content obtained in step (1) and the measurement value of the standard method. If the calculated evaluation parameters are within the predetermined threshold range, it is determined that the heavy metal is within the detection range , it can be directly detected by portable X-ray fluorescence spectrometry; if the calculated evaluation parameters are not within the predetermined threshold range, it...

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Abstract

The invention discloses a method for judging the heavy metal detection type of a portable X-ray fluorescence spectrometry, wherein the method is mainly designed to judge the metal detection type when heavy metals in soil are detected by using PXRF. The method comprises the following steps: (1) respectively using the portable X-ray fluorescence spectrometry and a standard method for measuring the content of the heavy metals in the soil to obtain a rapid measurement value and a standard method measurement value; (2) calculating evaluation parameters according to the rapid measurement value and the standard method measurement value of the heavy metals obtained in step (1), if the calculated evaluation parameters are in a predetermined threshold range, determining that the heavy metals can be detected directly by the portable X-ray fluorescence spectrometry within a detection range; if the calculated evaluation parameters are not in the predetermined threshold range, determining that the heavy metals cannot be detected directly by the portable X-ray fluorescence spectrometry beyond the detection range.

Description

technical field [0001] The invention relates to the fields of agriculture and environment, in particular to an evaluation method for rapid detection data of heavy metal content in soil. Background technique [0002] Soil is the material basis for sustainable economic and social development, and it is related to the health of the people and the construction of ecological civilization. Heavy metals are major soil pollutants, and their hazards are well known due to their toxicity, non-biodegradability and persistence. Heavy metals can also be absorbed by plants and enter the food chain, thereby endangering human health. Therefore, rapid and effective detection of heavy metals in soil is of great significance for timely understanding of land pollution status, evaluation of remediation effects and risk assessment. [0003] However, although traditional standard soil heavy metal detection and analysis methods such as atomic absorption (AAS), atomic fluorescence (AFS), and plasma...

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Application Information

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IPC IPC(8): G01N23/223
CPCG01N23/223G01N2223/076
Inventor 冉景詹茂华程寒飞李明项萌朱巧红
Owner HUATIAN ENG & TECH CORP MCC
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