Surface treatment process and titanium nail for bone setting
A technology for surface treatment and titanium nails, which is applied in the field of surface treatment and titanium nails for bone setting, which can solve the problems of difficulty in removing nails, inability to remove them, and pain of patients
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Examples
Embodiment 1
[0033] 1) Soak the titanium nail sample with one or more of absolute ethanol, acetone or metal surface degreaser, and then perform ultrasonic cleaning to remove the stain on the surface of the sample;
[0034] 2) Select 40-mesh sand, and then continue to sandblast the surface of the titanium nail sample under an air pressure of 0.2Mpa for 2 minutes. After completion, put it in pure water to clean and dry.
[0035] 3) Set the temperature of the cold trap of the lyophilizer at -20°C and pre-cool for 1 hour;
[0036] 4) Put the titanium nail sample into the vacuum chamber of the freeze dryer to seal it before pumping air, and wait for the temperature of the cold trap of the freeze dryer to drop to -45°C;
[0037] 5) Start timing when the air is evacuated to an internal vacuum of 14Pa, and last for 12 hours;
[0038] 6) Take out the titanium nail sample after finishing;
[0039] 7) Prepare hyaluronic acid solution;
[0040] 8) Make the prepared hyaluronic acid solution wet part...
Embodiment 2
[0046] In this embodiment, the size of the sand particles in step 2) of the first embodiment is selected as 100 mesh, and the rest of the conditions are the same as those of the first embodiment.
Embodiment 3
[0048] In this embodiment, the air pressure in step 2) of the first embodiment is selected as 0.8Mpa, and other conditions are the same as those of the first embodiment.
[0049] Comparing Examples 1, 2, and 3 comprehensively, the larger the number of sand grains and the greater the air pressure, the more porous structures are produced on the surface of the titanium nails, and the larger the porous pore size, the sandblasting process is selected in operability. The surface is very simple and easy to implement, but the porous structure formed is uneven, and the hyaluronic acid attached to the surface is easy to fall off, so it is impossible to achieve a very good nail removal effect. Moreover, the pore diameter on the surface of the titanium nail made by the sandblasting process is relatively large, and it is mainly used in the case of a relatively large size of the titanium nail.
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