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Cu-based MOF material preparation device

A preparation device and reaction technology, which is applied to mixers with rotating stirring devices, transportation and packaging, mixers, etc., can solve the problems of inconvenient pressure adjustment in reactors, and achieve the goals of improving convenience, ensuring sealing, and improving safety Effect

Inactive Publication Date: 2020-07-24
江苏元捷环境科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

[0004] The purpose of the present invention is to solve the disadvantage of inconvenient adjustment of reactor pressure in the prior art, and the proposed Cu-based MOF material preparation device

Method used

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  • Cu-based MOF material preparation device
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  • Cu-based MOF material preparation device

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Embodiment Construction

[0022] The following will clearly and completely describe the technical solutions in the embodiments of the present invention with reference to the accompanying drawings in the embodiments of the present invention. Obviously, the described embodiments are only some, not all, embodiments of the present invention.

[0023] refer to Figure 1-4 , Cu-based MOF material preparation device, comprising a reaction shell 1, a first support shell 10 is connected to one side of the outer wall of the reaction shell 1 by bolts, and a second support shell is connected to one side of the outer wall of one end of the reaction shell 1 by bolts Body 13, and the top outer wall of the second support shell 13 and the bottom outer wall of the first support shell 10 are connected with the same water conduit 12 by bolts, and the bottom inner walls on both sides of the first support shell 10 are connected with supports by bolts rod 17, and the same vertically arranged limit slide bar 15 is connected b...

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Abstract

The invention belongs to the field of metal organic frameworks, and particularly relates to a Cu-based MOF material preparation device. In view of the problem that the pressure of a reaction kettle isinconvenient to adjust in the prior art, proposed now is the following scheme: the Cu-based MOF material preparation device comprises a reaction shell, a first supporting shell is fixedly mounted onthe outer wall of one side of the reaction shell, a second supporting shell is fixedly mounted on the outer wall of one side of one end of the reaction shell, the same water guide pipe is fixedly mounted on the outer wall of the top of the second supporting shell and the outer wall of the bottom of the first supporting shell, and supporting rods are fixedly mounted on the inner walls of the bottoms of the two sides of the first supporting shell correspondingly. In the present invention, a spring, a first stirring rod and a second stirring rod are arranged in the Cu-based MOF material preparation device, in the process in which a first rotating motor drives a rotating rod to rotate and stir, the first stirring rod and the second stirring rod can continuously shake up and down under the influence of gravity, and then the mixing reaction effect of reaction materials is further improved.

Description

technical field [0001] The invention relates to the technical field of metal organic frameworks, in particular to a Cu-based MOF material preparation device. Background technique [0002] Metal-organic frameworks (MOFs) are a new type of porous adsorption material, which is the frontier and hotspot of current chemical research. MOF has a high specific surface area and a uniform pore structure, and can be controlled by selecting appropriate metals and ligands. design and synthesis, or modification of the framework by modification of pore size and pore walls. [0003] Traditional CuBTC preparation equipment basically uses high-pressure reactor-type equipment, but due to the narrow physical space, the internal pressure is unstable and uncontrollable during the heating process, which is greatly affected by the heating rate and heat transfer rate. Therefore, It is necessary to design a Cu-based MOF material preparation device with easy-to-adjust pressure. Contents of the inven...

Claims

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Application Information

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IPC IPC(8): B01J19/18B01J19/00B01F7/00B01J20/22B01J20/30C08G83/00
CPCB01J19/18B01J19/0053B01J19/0073B01J20/226C08G83/008B01F27/118
Inventor 王栋
Owner 江苏元捷环境科技有限公司
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