Bromobutyl rubber-based self-resealing septum and closure assembly
a technology of bromobutyl rubber and septum, applied in the field of septum, can solve problems such as less than ideal
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[0050]Comparative testing: Various septa, as detailed in Table 1 below, were tested for comparison to a septum comprising a resilient material derived from bromobutyl rubber. Each septum is coated on a single side with a fluoropolymer. The septum is placed in a retainer mechanism, which is subsequently affixed to a bottle containing tetrahydrofuran (THF). The septum is pierced with an 18 gauge needle and bottle assembly is inverted several times to simulate normal laboratory usage. The physical integrity of the pierced septa is visually evaluated.
TABLE 1Comparative testing of septa with tetrahydrofuran (THF).DiamDepthInversion testMakeSupplier(mm)(mm)Descriptionwith THFCommentBlack vitonGW43.13Single side PTFEok1face 70 ± 5° slave offRed VitonGW43.13Single side PTFEtacky surface1face 65 ± 5° slave offFKMGW43.0830.05 mm PFAtacky surface2FKMGW43.1530.25 mm PFAtacky surface2BromobutylGW42.830.25 mm PFAtacky surface2BromobutylGW42.930.05 mm PFAtacky surface2SiliconGW43.230.25 mm PFAok2S...
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