External used isolation gel aerosol solution
An aerosol and solution technology, applied in the field of external isolation gel aerosol solution, achieves the effects of not hindering skin respiration, low cost and simple preparation process
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Embodiment 1
[0027] The ratio of each component:
[0028] The ratio of monomer raw materials is: isobutylene 40%
[0029] Methyl Acrylate 60%
[0030] Catalyst: Aluminum Trichloride 0.3%
[0031] Initiator: Azobisisobutyronitrile 0.3%
[0032] Monomer concentration 40%
[0033] The balance is dimethyl carbonate.
[0034] The polymerization reaction is carried out in a tubular reactor, and the reactor is vacuumized, baked, and filled with nitrogen before use; methyl acrylate and aluminum trichloride are formulated into a complex dimethyl carbonate solution in an equimolar ratio for use, and azobis Isobutyronitrile is made into dimethyl carbonate solution for use;
[0035] The order of addition of the polymerization reaction is: dimethyl carbonate, isobutylene, methyl acrylate, aluminum chloride complex solution of methyl acrylate, and finally the solution of azobisisobutyronitrile is added, the reaction temperature is controlled at 80°C, and the reaction After 3 hours,...
Embodiment 2
[0037] The ratio of each component:
[0038] The ratio of monomer raw materials is: isobutylene 50%
[0039] Methyl Acrylate 50%
[0040] Catalyst: Aluminum Trichloride 0.9%
[0041] Initiator: Azobisisobutyronitrile 0.9%
[0042] Monomer concentration 50%
[0043] The balance is dimethyl carbonate.
[0044] The polymerization reaction is carried out in a tubular reactor, and the reactor is vacuumized, baked, and filled with nitrogen before use; methyl acrylate and aluminum trichloride are formulated into a complex dimethyl carbonate solution in an equimolar ratio for use, and azobis Isobutyronitrile is made into dimethyl carbonate solution for use;
[0045] The order of addition of the polymerization reaction is: dimethyl carbonate, isobutylene, methyl acrylate, aluminum chloride complex solution of methyl acrylate, and finally the solution of azobisisobutyronitrile is added, the reaction temperature is controlled at 50°C, and the reaction After 8 hours,...
Embodiment 3
[0047] The ratio of each component:
[0048] The ratio of monomer raw materials is: isobutylene 60%
[0049] Methyl Acrylate 40%
[0050] Catalyst: Aluminum Trichloride 1.5%
[0051] Initiator: Azobisisobutyronitrile 1.5%
[0052] Monomer concentration 60%
[0053] The balance is dimethyl carbonate.
[0054] The polymerization reaction is carried out in a tubular reactor, and the reactor is evacuated, baked, and filled with nitrogen before use; methyl acrylate and aluminum trichloride are formulated into a complex dimethyl carbonate solution in an equimolar ratio for use, and azobis Isobutyronitrile is made into dimethyl carbonate solution for use;
[0055] The order of addition of the polymerization reaction is: dimethyl carbonate, isobutylene, methyl acrylate, aluminum chloride complex solution of methyl acrylate, and finally the solution of azobisisobutyronitrile is added, the reaction temperature is controlled at 30°C, and the reaction After 12 hours,...
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