Preparation method of wood-organic-inorganic hybridized nano composite material based on doped nano POSS (Polyhedral Oligomeric Silsesquioxane)
A nanocomposite material and nanotechnology, applied in the field of wood composite material preparation, can solve the problems of poor mechanical properties, low impact toughness and poor thermal stability of wood-inorganic (nano) composite materials
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specific Embodiment approach 1
[0033] Specific embodiment one: the preparation method of the wood-organic-inorganic hybrid nanocomposite material based on nano POSS doping in this embodiment is carried out according to the following steps:
[0034] 1. Weigh 1 mass part of the functional monomer and the toughening agent and mix them uniformly, the mass of the toughening agent is 1% to 150% of the mass of the functional monomer to obtain a monomer solution;
[0035]2. Weigh 0.1% to 10% POSS (with organic amine functional groups) of the monomer solution mass obtained in step 1, then dry the POSS for 24 hours at 105°C and 0.01MPa under vacuum drying conditions, and then dehydrate the POSS with tetrahydrofuran The dried POSS is dissolved to obtain a POSS tetrahydrofuran solution with a POSS mass concentration of 1% to 20%, and the POSS tetrahydrofuran solution is added to the monomer solution in step 1, and stirred evenly to obtain a transparent monomer solution in which nano-POSS is dissolved;
[0036] Three, t...
specific Embodiment approach 2
[0049] Embodiment 2: This embodiment differs from Embodiment 1 in that the mass of the toughening agent in step 1 is 50% of the mass of the functional monomer. Others are the same as in the first embodiment.
specific Embodiment approach 3
[0050] Embodiment 3: The difference between this embodiment and Embodiment 1 is that in Step 2, 5% POSS by weight of the monomer solution obtained in Step 1 is weighed. Others are the same as in the first embodiment.
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