Fracturing inclusion self-dissolving diversion agent and preparation method thereof

A technology of diverting agent and inclusions, applied in the field of inclusion self-dissolving diverting agent and its preparation, can solve the problems of large filtration loss of fracturing fluid, inability to form filter cake, low plugging efficiency, etc., and simplify construction operations , The effect of simple on-site construction and high blocking strength

Inactive Publication Date: 2015-07-22
RES INST OF SHAANXI YANCHANG PETROLEUM GRP
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] At present, the commonly used diverting agents are: suspension diverting agents, whose disadvantages are that it is difficult to form a large pressure difference resistance due to turbulent flow and blast hole deformation, the plugging efficiency is low, and filter cakes cannot be formed; underground cross-linking diverting agents have the disadvantages Because a small dose cannot reach the required pressure, a large dose will cause new damage. Although a filter cake can be formed, the underground reaction is unstable and cannot reach the required strength; the once-crosslinked particle diverting agent on the ground is characterized by its own strength Large, but the plugging efficiency is low, and the fracturing fluid fluid loss is large; the plugging ball diversion agent is characterized by high strength and small deformation, but it is easy to fall off, low plugging efficiency, and cannot be self-degraded

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] At a room temperature of 20°C, put 15g of guanidine collagen powder, 35g of ferric chloride, 35g of aluminum oxide, 2g of sodium bicarbonate and 2g of potassium ferricyanide in 200ml of water and stir evenly, and continue stirring to mix the slurry for 5 minutes. Afterwards, put the slurry in a drying oven at 100°C for 40 minutes to obtain agglomerated materials, and use a pulverizer to crush them into 40-50 μm powders, and then spray them at the inlet of the fluidized granulator. 1g of γ-aminopropyltriethoxysilane coupling agent is attached to the surface of 10g ammonium persulfate crystal particles of 40~60 mesh, and then the crystal particles attached to the coupling agent are fully contacted with the powder by convection, so that the powder adheres Spherical particles are formed on the surface of the crystal particles, and finally dried to obtain the diverting agent in the form of inner wrapping, with a particle size of 20 mesh.

[0023] The guanidine collagen powd...

Embodiment 2

[0025] At a room temperature of 20°C, put 15g of guanidine collagen powder, 40g of ferric chloride, 32g of aluminum oxide, 1g of sodium bicarbonate and 2g of potassium ferricyanide in 200ml of water and stir evenly, and continue stirring to mix the slurry for 5 minutes. Then put the slurry in a drying oven at 100°C and dry for 30 minutes to obtain agglomerated materials, which are crushed into 40-50 μm powder by a pulverizer, and then sprayed at the inlet of the fluidized granulator 1g γ-aminopropyltriethoxysilane coupling agent is attached to the surface of 9g ammonium persulfate crystal particles of 40~60 mesh, and then the particles and powder are fully contacted by convection, so that the powder adheres to the crystal surface, and finally dried Ready to prepare.

Embodiment 3

[0027] At a room temperature of 20°C, put 15g of guanidine collagen powder, 32g of ferric chloride, 40g of aluminum oxide, 2g of sodium bicarbonate and 1g of potassium ferricyanide in 200ml of water and stir evenly, and continue to stir and mix the slurry for 5 minutes. Afterwards, put the slurry in a drying oven at 100°C for 40 minutes to obtain agglomerated materials, and use a pulverizer to crush them into 40-50 μm powders, and then spray them at the inlet of the fluidized granulator. 1g of γ-aminopropyltriethoxysilane coupling agent is attached to the surface of 9g of ammonium persulfate crystal particles of 40~60 mesh, and then the crystal particles with the coupling agent attached to the powder are fully contacted by convection, so that the powder adheres to the The surface of the crystal particles is formed into spherical particles, and finally dried to obtain the diverting agent in the form of inner wrapping, with a particle size of 20 mesh.

[0028] The guanidine ...

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Abstract

The invention relates to an inclusion self-dissolving diverting agent for fracturing and a preparation method thereof. The diverting agent is composed of 10-15 parts of guanidine collagen powder, 30-40 parts of ferric chloride, 30-40 parts of dioxygen trioxide Aluminum, 1-2 parts of sodium bicarbonate, 8-10 parts of ammonium persulfate, 1-2 parts of potassium ferricyanide and 1 part of γ-aminopropyltriethoxysilane, the steering agent is in the form of inner wrapping , in the form of spherical particles. The preparation method is as follows: at room temperature, guanidine collagen powder, ferric chloride, aluminum oxide, sodium bicarbonate, and potassium ferricyanide are successively dissolved in water and stirred for 5 minutes according to the formula ratio, and then the solution is dried and agglomerated, and It is crushed and pulverized, and then sprayed on the surface of ammonium persulfate by gamma-aminopropyltriethoxysilane coupling agent, the prepared powder is adhered and wrapped in the outer layer of ammonium persulfate crystals to form spherical particles, and finally The particles can be dried. The diverting agent is in the form of a gel breaker inner package, which has self-dissolution ability, and does not need to add additional gel breaker degradation agent during construction.

Description

technical field [0001] The invention relates to an inclusion self-dissolving diversion agent for oil well fracturing and a preparation method thereof. Background technique [0002] Conventional fracturing fractures generally extend along the direction of the maximum horizontal principal stress. Due to the influence of injection-production well patterns, the extension length of fractures cannot be excessively increased, so the volume of conventional fracturing stimulated reservoirs is limited. In order to increase the drainage area of ​​the oil well, the diversion fracturing technology can be used to open fractures along other directions while the injection-production well pattern remains unchanged, thereby increasing the production of the oil well. The performance of the diverting agent plays a decisive role in the successful implementation of diverting fracturing. [0003] At present, the commonly used diverting agents are: suspension diverting agents, whose disadvantages ...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09K8/68C09K8/70
CPCC09K8/706C09K2208/26
Inventor 高瑞民孙晓乔红军申峰吴金桥段玉秀高志亮郭庆景丰张军涛梁小兵展转盈
Owner RES INST OF SHAANXI YANCHANG PETROLEUM GRP
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