Fracturing inclusion self-dissolving diversion agent and preparation method thereof
A technology of diverting agent and inclusions, applied in the field of inclusion self-dissolving diverting agent and its preparation, can solve the problems of large filtration loss of fracturing fluid, inability to form filter cake, low plugging efficiency, etc., and simplify construction operations , The effect of simple on-site construction and high blocking strength
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Embodiment 1
[0022] At a room temperature of 20°C, put 15g of guanidine collagen powder, 35g of ferric chloride, 35g of aluminum oxide, 2g of sodium bicarbonate and 2g of potassium ferricyanide in 200ml of water and stir evenly, and continue stirring to mix the slurry for 5 minutes. Afterwards, put the slurry in a drying oven at 100°C for 40 minutes to obtain agglomerated materials, and use a pulverizer to crush them into 40-50 μm powders, and then spray them at the inlet of the fluidized granulator. 1g of γ-aminopropyltriethoxysilane coupling agent is attached to the surface of 10g ammonium persulfate crystal particles of 40~60 mesh, and then the crystal particles attached to the coupling agent are fully contacted with the powder by convection, so that the powder adheres Spherical particles are formed on the surface of the crystal particles, and finally dried to obtain the diverting agent in the form of inner wrapping, with a particle size of 20 mesh.
[0023] The guanidine collagen powd...
Embodiment 2
[0025] At a room temperature of 20°C, put 15g of guanidine collagen powder, 40g of ferric chloride, 32g of aluminum oxide, 1g of sodium bicarbonate and 2g of potassium ferricyanide in 200ml of water and stir evenly, and continue stirring to mix the slurry for 5 minutes. Then put the slurry in a drying oven at 100°C and dry for 30 minutes to obtain agglomerated materials, which are crushed into 40-50 μm powder by a pulverizer, and then sprayed at the inlet of the fluidized granulator 1g γ-aminopropyltriethoxysilane coupling agent is attached to the surface of 9g ammonium persulfate crystal particles of 40~60 mesh, and then the particles and powder are fully contacted by convection, so that the powder adheres to the crystal surface, and finally dried Ready to prepare.
Embodiment 3
[0027] At a room temperature of 20°C, put 15g of guanidine collagen powder, 32g of ferric chloride, 40g of aluminum oxide, 2g of sodium bicarbonate and 1g of potassium ferricyanide in 200ml of water and stir evenly, and continue to stir and mix the slurry for 5 minutes. Afterwards, put the slurry in a drying oven at 100°C for 40 minutes to obtain agglomerated materials, and use a pulverizer to crush them into 40-50 μm powders, and then spray them at the inlet of the fluidized granulator. 1g of γ-aminopropyltriethoxysilane coupling agent is attached to the surface of 9g of ammonium persulfate crystal particles of 40~60 mesh, and then the crystal particles with the coupling agent attached to the powder are fully contacted by convection, so that the powder adheres to the The surface of the crystal particles is formed into spherical particles, and finally dried to obtain the diverting agent in the form of inner wrapping, with a particle size of 20 mesh.
[0028] The guanidine ...
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