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Rapid detection reagent and method for adsorptivity of biomass charcoal material

A technology of adsorption performance and biochar, which is applied in the direction of color/spectral characteristic measurement, etc., can solve the problems of more than 20 hours of test time, rapid determination of biochar adsorption performance, expensive instruments, etc., and achieve low production cost, The effect of stable detection reagent and fast reaction speed

Inactive Publication Date: 2016-09-07
ZHEJIANG FORESTRY ACAD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The advantages of this type of method are: accurate measurement, and can characterize the isothermal adsorption and desorption curves of carbon materials; the disadvantages are: the price of the specific surface area adsorption instrument is relatively expensive, and liquid nitrogen is needed to cool the test quartz tube during the test. For the test material to be flushed with nitrogen continuously, it takes more than 20 hours to test a sample. If the sample pretreatment time is added, the entire measurement cycle is more than 1 day. The test process is time-consuming, expensive and laborious.
However, the existing published patents do not disclose the technology for rapid determination of the adsorption performance of biochar. Therefore, how to quickly and cheaply measure the adsorption performance of biochar materials is a technology that urgently needs to be researched and solved.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] The rapid detection reagent of biochar material adsorption performance in the present embodiment is made up of ethanol, bromocresol green and water, and in every 100 grams of detection reagents, contain 60-75 gram of ethanol, 0.005-0.02 gram of bromocresol green, balance for water. The water is typically deionized water.

[0023] Table 1: Component list of rapid detection reagent for adsorption performance of 100 grams of biochar materials

[0024] serial number

Ethanol (grams)

Bromocresol Green (g)

deionized water (grams)

1

60

0.015

margin

2

72

0.013

margin

3

62

0.005

margin

4

67.5

0.019

margin

5

75

0.008

margin

6

68

0.01

margin

7

73

0.017

margin

8

70

0.02

margin

9

67

0.012

margin

10

64

0.007

margin

[0025] The rapid detection method for the adsorption performance of the biochar materi...

Embodiment 2

[0035] The rapid detection reagent for the adsorption performance of biochar materials in this example is composed of ethanol, bromocresol green and deionized water, and every 100 grams of detection reagent contains 70 grams of ethanol, 0.005 grams of bromocresol green, and the balance is deionized water .

[0036] The adsorption color chart of carbon materials with different adsorption properties is shown in Table 2. The biochar material with iodine adsorption performance of 0 to 500 mg / g and the discrimination degree of 100 mg / g can be directly compared with the sample. Colors get big results. The whole process takes no more than 6 minutes, and the whole process is as follows: 1 gram of biochar sample + 5 mL of detection reagent is ultrasonically oscillated for 3 minutes, and immediately filtered through filter paper to perform color comparison with the color comparison card and obtain the result.

[0037] Table 2 L of reagents adsorbed by carbon materials with different ad...

Embodiment 3

[0040] The rapid detection reagent for the adsorption performance of biochar materials in this example is composed of ethanol, bromocresol green and deionized water, and every 100 grams of the reagent contains 70 grams of ethanol, 0.02 grams of bromocresol green, and the balance is deionized water.

[0041] The adsorption color charts for carbon materials with different adsorption properties are shown in Table 3. When the iodine adsorption performance of biochar materials is between 0 and 1500 mg / g, the material with a discrimination degree of 200 mg / g can be obtained directly through the colorimetry of the sample. to the result. The whole process takes no more than 6 minutes, and the whole process is as follows: 1 gram of biochar sample + 5mL detection reagent is ultrasonically oscillated for 3 minutes, and immediately filtered through filter paper to compare with the color card and obtain the result.

[0042] Table 3 L of reagents adsorbed by carbon materials with different ...

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Abstract

The invention relates to a rapid detection reagent and method for adsorptivity of a biomass charcoal material. Rapid determination technology for the adsorptivity of the biomass charcoal material has not been disclosed in the prior art. The detection reagent provided by the invention has the characteristic that every 100 g of the detection reagent contains 60 to 75 g of ethanol and 0.005 to 0.02 g of bromocresol green, with the balance being water. The detection method is characterized by comprising the following steps: (1) weighing known parts of a charcoal material, mixing each part of the charcoal material with 5 mL of the detection reagent so as to obtain corresponding parts of a reaction solution, determining the values L*, a* and b* of each part of the reaction solution by using a color difference meter and preparing a colorimetric card; (2) mixing a biomass charcoal material sample with the detection reagent, carrying out ultrasonic treatment for 3 min and then carrying out filtering so as to obtain a solution; and (3) directly comparing the solution with the colorimetric card and directly estimating the adsorptivity of the biomass charcoal material sample. The rapid detection reagent is simple in composition and can realize cheap and rapid determination of the adsorptivity of the biomass charcoal material.

Description

technical field [0001] The invention relates to a rapid detection reagent and detection method for the adsorption performance of biomass carbon materials, which are specially used for rapid detection of the adsorption performance of biomass carbon materials. Background technique [0002] In contemporary society, people pay more and more attention to environmental problems. Biomass carbon materials are ideal materials for air purification, and the adsorption performance of biomass carbon materials directly determines the size of its air purification ability. The existing biomass carbon material adsorption performance There are two main categories of measurement methods. [0003] One is to use the specific surface area adsorption instrument to characterize the adsorption performance of carbon materials. The advantages of this type of method are: accurate measurement, and can characterize the isothermal adsorption and desorption curves of carbon materials; the disadvantages ar...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N21/25
CPCG01N21/25
Inventor 潘炘
Owner ZHEJIANG FORESTRY ACAD
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