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Chemical corrosion-free liquid chromatographic column tube

A liquid chromatography column and chemical corrosion technology, applied in scientific instruments, measuring devices, instruments, etc., can solve the problems of slow analysis speed, low separation efficiency of classical liquid chromatography, complicated operation, etc., and achieve the effect of avoiding chemical corrosion

Inactive Publication Date: 2018-07-31
张敏
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The separated samples are collected by fractions and then analyzed, which makes the classical liquid chromatography not only have low separation efficiency and slow analysis speed, but also complicate the operation

Method used

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  • Chemical corrosion-free liquid chromatographic column tube
  • Chemical corrosion-free liquid chromatographic column tube
  • Chemical corrosion-free liquid chromatographic column tube

Examples

Experimental program
Comparison scheme
Effect test

Embodiment

[0019] Embodiment: A chemical corrosion-free liquid chromatography column tube, its main structure includes: mobile phase liquid storage tube 1, solvent dripping tube 2, funnel tube 3, internal thread sleeve 4, pump rack 41, micro Vacuum degassing pump 5, external threaded sleeve 6, probe base 7, sampling probe 71, base 8, tray tube 81, sample tube 9, sealing plug 10, the internal threaded sleeve 4 is fixed with a pump A shelf 41, the pump shelf 41 is clamped and fixed with a miniature vacuum degassing pump 5; the bottom of the mobile phase liquid storage tube 1 is screwed with an internal thread sleeve 4, and the top is inserted with a solvent dripping tube 2 The end of the solvent dripping tube 2 is screwed to the top of the pump shelf 41, and the top of the solvent dripping tube 2 is fixed with a funnel tube 3;

[0020] The externally threaded sleeve 6 is fixed with a probe base 7, and the probe base 7 is inserted with a sample injection probe 71; the externally threaded sl...

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PUM

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Abstract

The invention relates to a chemical corrosion-free liquid chromatographic column tube. A pump machine shelf is fixedly arranged in an inner threaded sleeve; a miniature vacuum degassing pump is clamped and fixedly arranged in the pump machine shelf; the bottom of a mobile-phase liquid storage tube is connected with the inner threaded sleeve in a screwing manner; a solvent dropping-in tube is inserted into the top of the mobile-phase liquid storage tube; the tail end of the solvent dropping-in tube is connected to the top of the pump machine shelf in the screwing manner; the top of the solventdropping-in tube is fixedly provided with a funnel tube in a running-through manner; an exploring tube seat is fixedly arranged in an outer threaded sleeve; a sample introduction exploring tube is arranged in the exploring tube seat in a socket manner. The chemical corrosion-free liquid chromatographic column tube, by adopting the technical means that a gas suction tube fitting of the miniature vacuum degassing pump is communicated with the sample introduction exploring tube, a gas exhaust tube fitting of the miniature vacuum degassing pump is communicated with the mobile-phase liquid storagetube, the inner wall of a base is fixedly provided with a tray tube, moreover, the base is screwed into the outer threaded sleeve, a sample tube is inserted into the base, the sample tube and the baseare sealed and fixed through a sealing plug and the top of the sample tube is abutted with the bottom of the exploring tube base, is used for realizing the production of the chemical corrosion-free liquid chromatographic column tube.

Description

technical field [0001] The invention relates to a chemical corrosion-free liquid chromatography column tube. Background technique [0002] Liquid chromatography is a kind of separation and analysis technique, which is characterized by using liquid as the mobile phase, and the stationary phase can have various forms, such as paper, thin plate and packed bed. In the process of chromatographic technology development. In order to distinguish the various methods, the respective nomenclature has been produced according to the form of the stationary phase, such as paper chromatography, thin-layer chromatography, and column liquid chromatography. The mobile phase of classical liquid chromatography flows through the chromatographic column slowly by gravity, so the particle size of the stationary phase cannot be too small (about 100 μm to 150 μm). The separated samples are collected by fractions and then analyzed, which makes the classical liquid chromatography not only have low sep...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N30/60
CPCG01N30/606
Inventor 张敏
Owner 张敏
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