Positive pole piece, preparation method thereof and lithium ion battery
A technology of positive electrode sheet and conductive agent, applied in the field of positive electrode sheet and its preparation, can solve problems such as restricting the development of lithium ion batteries, and achieve the effect of improving specific capacity and cycle stability, high capacity advantage, and improving cycle stability
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[0055] In the second aspect of this application, the preparation method of the positive electrode sheet is provided, including the following steps:
[0056] S1: The polycrystalline active material, the first adhesive, and the first conductive agent are dissolved in the first solvent, and mixed uniform mixed by stirring to obtain a first slurry;
[0057] S2: The polycrystalline active material, the single crystal active material is dissolved in the second solvent, and mixed with stirring is mixed, and the second slurry is obtained;
[0058] S3: The single crystal active material, the second adhesive, and the second conductive agent are dissolved in the third solvent, mixed uniform mixed by stirring, to obtain a third slurry;
[0059] S4: Apply the first slurry obtained by step S1 to the surface of the current collector, forming the first material layer, applying the second slurry material obtained in step S2 to the outer surface of the first material layer, forming a transition lay...
Embodiment 1
[0072] (1) Preparation of the positive electrode plate
[0073] S1: Polycrystalline active material lini 0.8 CO 0.1 Mn 0.1 O 2 The first binder PVDF and the first conductive agent acetyxyn black are dissolved in N-methylpyrrolidone according to the mass of 97: 1: 2, and mixed with N-methylpyrrolidone, and mixed with a solid content of 40%;
[0074] S2: Polycrystalline active material lini 0.8 CO 0.1 Mn 0.1 O 2 , Single crystal active material Lini 0.8 CO 0.1 Mn 0.1 O 2 According to the volume of 1: 1 is soluble in N-methylpyrrolidone, it is mixed and mixed, and the second slurry is obtained;
[0075] S3: Lini of single crystal active materials 0.9 CO 0.05 Mn 0.05 O 2 The second adhesive PVDF and the second conductive agent acetylene black, carbon nanotubes are well dissolved in N-methylpyrrolidone according to 96.5: 1: 1.5: 1, and mixed with N-methylpyrrolidone, mixed with mixing, 50% solid content of 40%. Third slurry;
[0076] S4: The first slurry obtained by step S1 is applied ...
Embodiment 2
[0082] Based on Example 1, the difference is only: in Example 2, the polycrystalline active material Lini 0.8 CO 0.1 Mn 0.1 O 2 The mass ratio of the first binder PVDF and the first conductive agent acetylene is 96: 1: 3.
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