Azeotrope-Like Composition of 2-Chloro-3,3,3-Trifluoropropene (HCFC-1233xf) and Hydrogen Fluoride (HF)
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example 1
[0025]60 g of 2-chloro-3,3,3-trifluoropropene (HCFO-1233xf) were mixed with 40 g of HF to form a heterogeneous azeotrope mixture. The vapor pressure of the mixture at about 25° C. was about 38 psia.
example 2
[0026]Binary compositions containing solely 2-chloro-3,3,3-trifluoropropene (HCFO-1233xf) and HF were blended to form a heterogeneous azeotrope mixtures at different compositions. The vapor pressures of the mixtures were measured at about 0, 25 and 61° C. and the following results were noticed. Table 1 shows the vapor pressure measurements of HCFO-1233xf and HF as a function of composition with varying weight percent HF at constant temperatures of about 0, 25, and 61° C. The data also showed that HCFO-1233xf / HF is a heterogeneous mixture.
TABLE 1P-T-X of HCFO-1233xf / HFPressure (Psia)Mole % HFT = 0° C.T = 25° C.T = 61° C.0.008.8722.8864.5812.7014.2135.285.6222.5014.6938.48102.438.3415.0338.4106.0846.4615.0338.35107.3455.0615.0338.45106.9567.3915.0338.45106.9576.0615.0338.4510781.7215.0338.45107.0586.2715.0838.4102.8898.3612.5129.0472.5399.309.723.1761.72100.006.8717.8252.43
[0027]The data also shows that the mixture is azeotropic or azeotrope-like since the vapor pressure of the mixtur...
example 3
[0028]The azeotropic or azeotrope-like composition of the HCFO-1233xf / HF mixture was also verified by Vapor-Liquid-Liquid equilibrium (VLLE) experiment. 63.5 g of 2-chloro-3,3,3-trifluoropropene (HCFO-1233xf) were mixed with 36.5 g of HF to form a heterogeneous mixture (visual observation) at 24° C. The vapor composition, upper liquid (HF rich), and bottom liquid (organic) were sampled. The result shows that the azeotropic composition is about 82.5±1.2 mole percent HF at 24° C.
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