Chlorinated alkane photo-carbonylation reaction method at cadmium compound catalysis
A technology of carbonylation reaction and chlorinated alkanes, which is applied in the direction of chemical instruments and methods, physical/chemical process catalysts, carbon monoxide or formate reaction preparation, etc., to achieve the effect of low input cost, mild reaction conditions and high added value
- Summary
- Abstract
- Description
- Claims
- Application Information
AI Technical Summary
Problems solved by technology
Method used
Image
Examples
Embodiment Construction
[0012] The specific operation steps of the method of the present invention are as follows: place a 400W high-pressure mercury lamp inside a hollow interlayer quartz photoreactor, pass circulating water into the interlayer, and simultaneously put the entire reactor into a water tank filled with water to cool the lamp Source; 5ml of methanol solution containing chlorinated alkanes substrate and catalyst is added in the quartz test tube, the quartz test tube is close to the outer wall of the photoreactor, carbon monoxide or carbon dioxide is introduced into the reaction solution, and the pressure is kept constant at room temperature after replacement and deoxygenation. 0.1MPa, start the light source to irradiate the reaction solution for 25h, the illumination of the light source is 2.6×10 -2 W / m 2 , the distance from the center of the light source to the center of the reaction solution is 3.3×10 -2 m. With n-decane as internal standard, the product was analyzed by GC and GC-MS ...
PUM
Abstract
Description
Claims
Application Information
- R&D Engineer
- R&D Manager
- IP Professional
- Industry Leading Data Capabilities
- Powerful AI technology
- Patent DNA Extraction
Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic, Popular Technical Reports.
© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap|About US| Contact US: help@patsnap.com