Electrochemical method for detecting anthracene of polycyclic aromatic hydrocarbon

An anthracene and electrochemical technology of polycyclic aromatic hydrocarbons, applied in the direction of material electrochemical variables, can solve the problems of high cost and complex preparation of immunomodified electrodes, and achieve the effects of low detection limit, low material price and short detection cycle

Inactive Publication Date: 2013-04-17
UNIV OF JINAN
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Problems solved by technology

However, the preparation of immunomodified electrodes is too complicated and the cost is high

Method used

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  • Electrochemical method for detecting anthracene of polycyclic aromatic hydrocarbon
  • Electrochemical method for detecting anthracene of polycyclic aromatic hydrocarbon
  • Electrochemical method for detecting anthracene of polycyclic aromatic hydrocarbon

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Embodiment 1

[0035] An electrochemical method for detecting polycyclic aromatic hydrocarbon anthracene, using the probe Alizarin Red (ARS) to modify the mesoporous material SBA15 electrochemically modified electrode, the modified electrode is prepared from the mesoporous material ARS-SBA15 and glassy carbon electrode, used for Detection of anthracene content in aqueous solution.

[0036] 1 Synthesis of mesoporous material SBA15: For the synthesis of SBA15, dissolve 4g Pluronic P123 in 30g deionized water, add 120g 2mol / L HCl, stir at 40°C to obtain a transparent solution, add 8.5g TEOS, and keep stirring at 40°C for 20h. Then continue aging at 100°C for 2-3 days, filter, wash and dry. Finally, the temperature was raised to 500°C at a rate of 1°C / min, and the SBA15 sample was obtained after calcination for 4-6 hours.

[0037] 2 Alizarin red probe (ARS) modified mesoporous material (SBA15), the steps are as follows: weigh 0.5g of ARS and dissolve it in an appropriate amount of dry DMF, add ...

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Abstract

The invention relates to the technical field of assay determination of anthracene of polycyclic aromatic hydrocarbon, and in particular relates to an electrochemical method for performing quantitative determination on anthracene content in a water system by taking alizarin red as a probe for modifying a mesoporous material. The material synthesis of a functional modified electrode taking the probe for modifying the mesoporous material is simple and convenient; the modified electrode is simple and convenient to manufacture; the material cost is low; the electrode is easy to update, good in reproducibility and non-toxic, and does not cause environment pollution; and the determining method reduces the interference of coexist substances effectively, and is good in selectivity and high in sensitivity.

Description

technical field [0001] The invention relates to the technical field of anthracene analysis and determination of polycyclic aromatic hydrocarbons, in particular to an electrochemical method for modifying mesoporous materials using alizarin red as a probe and quantitatively detecting the anthracene content in a water system. Background technique [0002] As coal and petroleum are widely used in industrial production, transportation and daily life, the resulting polycyclic aromatic hydrocarbons have strong teratogenicity, carcinogenicity and mutagenicity, so they have become organic pollutants of common concern to all countries in the world. Anthracene widely exists in the wastewater discharged from the production of textiles, pharmaceuticals, papermaking, dyes and other industries, and has serious toxic effects on humans, animals, and plants. s concern. [0003] With the development of science and technology, various methods and instruments for detecting aromatic hydrocarbons...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N27/48G01N27/30
Inventor 周长利徐帅刘珊卫茂超
Owner UNIV OF JINAN
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