Double-long-chain alkyl hydroxy sulfobetaine surfactant and oil-displacing agent
A technology of long-chain alkyl hydroxy sulfobeet and surfactant, which is applied in the fields of sulfonate preparation, drilling composition, chemical instrument and method, etc. , the reduction of recovery rate, etc.
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Embodiment 1
[0022] This embodiment provides a kind of didodecyl methyl hydroxy sultaine, which is prepared through the following steps:
[0023] Make didodecylmethyl tertiary amine and sodium trichlorodihydroxypropanesulfonate react in the presence of NaOH, the reaction medium is a mixed solution of water and isopropanol (the volume ratio of water to isopropanol is 1:1, The molar ratio of water to di-long-chain methyl tertiary amine is 30:1), the reaction temperature is 80°C, the molar ratio of sodium trichlorodihydroxypropanesulfonate to didodecyl methyl tertiary amine is 1.2:1, The molar ratio of NaOH to sodium trichlorodihydroxypropanesulfonate is 1:1.2, the reaction time is 8 hours, the unreacted didodecylmethyl tertiary amine is washed away with petroleum ether, the solvent is separated after the reaction is completed, and the product is washed with ethanol , the ethanol was distilled off to obtain the final product as a white solid.
[0024] The product was subjected to infrared an...
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