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Electrochemical reactor for preparing oligosaccharide from marine biology functional sugars and preparation method

A technology for marine organisms and functional sugars, applied in the electrolysis process, electrolysis components, electrolysis organic production, etc., can solve the problems such as the inability to meet the requirements of oligosaccharides, the insufficient reaction of the reaction solution, and the inability to control the product concentration, and achieve strong selectivity. , Simple operation, easy to integrate control and optimized effect

Active Publication Date: 2014-12-24
ZHEJIANG CHENGXIN PHARMA & CHEM EQUIP
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] At the same time, the controllability of the current electrochemical reactor cannot meet the requirements for preparing oligosaccharides from marine biological functional sugars. For example, the high-efficiency electrochemical reactor [CN101654294A] disclosed in the Chinese patent literature includes a tank body, which is arranged in parallel in the tank body. several plates
The flow of the solution between the plates in this type of electrochemical reactor is very unsmooth, resulting in different reaction conditions between each plate, and insufficient and uneven reaction of the reaction solution, resulting in uncontrollable reaction after the reaction. The concentration of the product in the reaction solution is less controllable

Method used

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  • Electrochemical reactor for preparing oligosaccharide from marine biology functional sugars and preparation method
  • Electrochemical reactor for preparing oligosaccharide from marine biology functional sugars and preparation method
  • Electrochemical reactor for preparing oligosaccharide from marine biology functional sugars and preparation method

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Embodiment 1

[0033] Electrochemical reactor for preparation of oligosaccharides from functional sugars of marine organisms, such as Figure 1 to Figure 3 As shown, it includes a reaction tank 1 with a cavity, and two partitions 2 are fixed in the reaction tank 1, and the two partitions 2 divide the cavity into three chambers, and the three chambers are reaction chamber 1a and respectively located in In the flow chamber 1b on both sides of the reaction chamber 1a, the flow holes 2a connecting the reaction chamber 1a and the flow chamber 1b are opened on the two partitions 2, and the reaction chamber 1a is provided with a pole plate assembly, which includes two parallel set Side pole plates 3 and several inner pole plates 4 between the two side pole plates 3, there are seven inner pole plates 4 in the first embodiment; two side pole plates 3 are provided with installation holes for installing electrodes 3a, the installation hole 3a is provided with the middle part of the upper end surface of...

Embodiment 2

[0044] The structure and principle of this embodiment are basically the same as that of Embodiment 1. The difference is that the positioning structure includes a positioning plate, and a number of slots are opened on the positioning plate, and the slots are arranged at equal intervals. The lower ends of the side plates and the inner plates All are clamped in the slot, and the positioning plate is fixed on the bottom surface of the reaction tank located in the reaction chamber.

Embodiment 3

[0046] The structure and principle of this embodiment are basically the same as those of Embodiment 1, except that in step D, the adsorbed oligosaccharides are eluted with 0.07 mol / l hydrochloric acid.

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Abstract

The invention provides an electrochemical reactor for preparing oligosaccharide from marine biology functional sugars and a preparation method and belongs to the electrolysis field. The technical problem that the oligosaccharide cannot be prepared from the marine biology functional sugars through an electrochemical reaction in the prior art is solved. The electrochemical reactor comprises a reaction tank which comprises an empty chamber; two separating plates are fixed in the reaction tank; the empty chamber is divided into three chambers through the two separating plates; the three chambers comprise a reaction chamber and two flow chambers which are located on the bilateral sides of the reaction chamber respectively; each separating plate is provided with a circulation hole which is communicated with the reaction chamber and the corresponding flow chamber; a polar plate is arranged in the reaction chamber. According to the electrochemical reactor, the integration is easy to control and optimize. The preparation method for preparing the oligosaccharide from the marine biology functional sugars comprises step A, feeding; step B, reaction; step C, discharging; step D, separation and collection. According to the preparation method, the oligosaccharide can be extracted from the marine biology functional sugars.

Description

technical field [0001] The invention belongs to the field of electrolysis, and relates to an electrochemical reactor, in particular to an electrochemical reactor for preparing oligosaccharides from marine biological functional sugars; the invention also relates to a preparation of oligosaccharides from marine biological functional sugars method, belonging to the field of organic chemistry. Background technique [0002] Marine organisms are widely distributed in the ocean, so the resources are very rich. At present, there is no mature technology to prepare oligosaccharides from functional sugars of marine organisms through electrochemical reactions. [0003] At the same time, the controllability of the current electrochemical reactor cannot meet the requirements for preparing oligosaccharides from marine biological functional sugars. For example, the high-efficiency electrochemical reactor [CN101654294A] disclosed in the Chinese patent literature includes a tank body, which i...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C25B3/00C25B15/02C25B15/04
Inventor 林海波潘万贵
Owner ZHEJIANG CHENGXIN PHARMA & CHEM EQUIP
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